Functionalization of Graphene:
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| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH
2014
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| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XVIII, 406 S. Ill., graph. Darst. |
| ISBN: | 352733551X 9783527335510 |
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| 245 | 1 | 0 | |a Functionalization of Graphene |c ed. by Vasilios Georgakilas |
| 263 | |a 201405 | ||
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Record in the Search Index
| _version_ | 1809769634309603328 |
|---|---|
| adam_text |
CONTENTS
PREFACE
XIII
LIST OF CONTRIBUTORS
XV
1 AN INTRODUCTION TO CRAPHENE 1
KONSTANTINOS SPYROU AND PETRA RUDOLF
1.1 BRIEF HISTORY OF GRAPHITE 1
1.2 GRAPHENE AND GRAPHENE OXIDE 2
1.2.1 PREPARATION OF GRAPHENE FROM GRAPHENE OXIDE 3
1.2.2 ISOLATION OF PRISTINE GRAPHENE MONOLAYERS 5
1.2.3 LARGE SCALE PRODUCTION OF GO BY LANGMUIR-BLODGETT METHODS 6
1.2.4 OTHER METHODS OF GRAPHENE PRODUCTION 6
1.3 CHARACTERIZATION OF GRAPHENE 9
1.3.1 MICROSCOPIC OBSERVATION 9
1.3.2 RAMAN SPECTROSCOPY 11
1.3.3 THERMOGRAVIMETRIC ANALYSIS 12
1.3.4 OPTICAL PROPERTIES OF GRAPHENE 13
1.3.5 X-RAY DIFFRACTION PATTERN 17
REFERENCES 18
2 COVALENT ATTACHMENT OF ORGANIC FUNCTIONAL GROUPS ON PRISTINE
GRAPHENE 21
VASILIOS GEORGAKILAS
2.1 INTRODUCTION 21
2.2 CYCLOADDITION REACTIONS 22
2.2.1 1,3-DIPOLAR CYCLOADDITION OF AZOMETHINE YLIDE 22
2.2.1.1 THROUGH A SUBSTITUTED ALDEHYDE PATHWAY 24
2.2.1.2 THROUGH SUBSTITUTED A AMINO ACID PATHWAY 27
2.2.2 CYCLOADDITION BY ZWITTERIONIC INTERMEDIATE 28
2.2.3 DIELS-ALDER CYCLOADDITION 29
2.2.4 NITRENE ADDITION 30
2.2.5 CARBENE ADDITION 35
2.2.6 ARYNE ADDITION 36
2.2.7 BINGEL TYPE CYCLOADDITION 37
HTTP://D-NB.INFO/1044721022
VII CONTENTS
2.3 ADDITION OF FREE RADICALS 39
2.3.1 DIAZONIUM SALT REACTION 39
2.3.2 OTHER RADICAL ADDITIONS 42
2.4 NUCLEOPHILIC ADDITION 46
2.5 ELECTROPHILIC ADDITION ON GRAPHENE 46
2.6 ORGANOMETALLIC CHEMISTRY OF GRAPHENE 48
2.7 POST FUNCTIONALIZATION REACTIONS 50
2.8 CONCLUSION 55
REFERENCES 56
3 ADDITION OF ORGANIC CROUPS THROUGH REACTIONS WITH OXYGEN
SPECIES OF GRAPHENE OXIDE 59
VASILIOS GEORGAKILAS
3.1 INTRODUCTION 59
3.1.1 GRAPHENE/POLYMER NANOCOMPOSITES 60
3.2 THE ROLE OF CARBOXYLIC ACIDS OF GO 61
3.2.1 ORGANIC FUNCTIONALIZATION THROUGH AMIDE BOND FORMATION 61
3.2.1.1 LIPOPHILIC DERIVATIVES 61
3.2.1.2 HYDROPHILIC - BIOCOMPATIBLE DERIVATIVES 62
3.2.1.3 ADDITION OF CHROMOPHORES 64
3.2.1.4 POLYMER GRAPHENE COMPOSITE 69
3.2.2 ESTERIFICATION OF GO 71
3.2.3 FUNCTIONALIZATION OF GO THROUGH HETEROCYCLIC RING
FORMATION 75
3.3 THE ROLE OF HYDROXYL GROUPS OF GO 77
3.4 MISCELLANEOUS ADDITIONS 78
3.4.1 REACTION OF CARBOXYLIC ACID AND HYDROXYL GROUPS WITH ISOCYANATE
DERIVATIVES 78
3.4.2 REACTION OF EPOXIDES WITH CARBOXYLIC ACIDS OR HYDROXYL
GROUPS 78
3.4.3 INTERACTION OF AMMONIA WITH CARBOXYLIC ACIDS AND EPOXIDES OF
GO 80
3.4.4 ENRICHMENT OF GO IN CARBOXYLIC ACIDS 81
3.4.5 ADDITION OF GALLIUM-PHTHALOCYANINE (GA-PC) TO GO THROUGH GA-O
COVALENT BOND 82
3.5 THE ROLE OF EPOXIDE GROUPS OF GO 83
3.5.1 NUCLEOPHILIC ADDITION OF AMINE TO EPOXIDES 83
3.5.2 ADDITION OF CHROMOPHORES 85
3.5.3 ADDITION OF POLYMERS 86
3.6 POST FUNCTIONALIZATION OF GO 87
3.6.1 POST FUNCTIONALIZATION OF ORGANICALLY MODIFIED GO VIA CLICK
CHEMISTRY 87
3.6.2 COUNTER ANION EXCHANGE 89
3.7 CONCLUSIONS 90
REFERENCES 92
CONTENTS I VII
4 CHEMICAL FUNCTIONALIZATION OF GRAPHENE FOR BIOMEDICAL
APPLICATIONS 95
CINZIA SPINATO, CECILIA MINARD-MOYON, AND ALBERTO BIANCO
4.1 INTRODUCTION 95
4.2 COVALENT FUNCTIONALIZATION OF GRAPHENE NANOMATERIALS 97
4.2.1 SYNTHESIS OF GO AND RGO 99
4.2.1.1 SYNTHESIS OF GRAPHENE OXIDE 99
4.2.1.2 REDUCTION OF GRAPHENE OXIDE 99
4.2.2 FUNCTIONALIZATION OF GRAPHENE OXIDE WITH POLYMERS 100
4.2.2.1 PEGYLATED-GO CONJUGATES 100
4.2.2.2 COVALENT LINKAGE OF BIOPOLYMERS 103
4.2.3 TETHERING OF ANTIBODIES 105
4.2.4 ATTACHMENT OF NUCLEIC ACIDS 106
4.2.5 GRAFTING OF PEPTIDES AND ENZYMES 108
4.2.6 ATTACHMENT OF OTHER ORGANIC MOLECULES AND BIOMOLECULES 108
4.3 NON-COVALENT FUNCTIONALIZATION OF GRAPHENE 110
4.3.1 ADSORPTION VIA 3T-STACKING 110
4.3.1.1 ADSORPTION OF DRUGS 111
4.3.1.2 ADSORPTION OF PYRENE DERIVATIVES 111
4.3.1.3 NON-COVALENT INTERACTIONS WITH NUCLEIC ACIDS AND APTAMERS 113
4.3.1.4 IMMOBILIZATION OF ENZYMES, PROTEINS, AND OTHER
M ACROMOLECULES 116
4.3.2 ELECTROSTATIC AND HYDROPHOBIC INTERACTIONS 116
4.3.2.1 COATING WITH POLYMERS AND BIOPOLYMERS 116
4.3.2.2 DEPOSITION OF NANOPARTICLES 119
4.3.2.3 ADSORPTION OF QUANTUM DOTS 121
4.4 GRAPHENE-BASED CONJUGATES PREPARED BY A COMBINATION OF COVALENT
AND NON-COVALENT FUNCTIONALIZATION 121
4.4.1 POLYMER- AND BIOPOLYMER-GRAFTED GRAPHENE NANOMATERIALS USED AS
NANOCARRIERS 121
4.4.1.1 POLYMER-FUNCTIONALIZED GO FOR DRUG DELIVERY 122
4.4.1.2 POLYMER-FUNCTIONALIZED GO FOR GENE DELIVERY 123
4.4.1.3 CHITOSAN-FUNCTIONALIZED GO 125
4.4.2 GO FUNCTIONALIZED WITH TARGETING LIGANDS AND ANTIBODIES 125
4.4.2.1 FOLIC ACID-CONJUGATED GO 125
4.4.2.2 ANTIBODY-FUNCTIONALIZED GO FOR RADIOIMAGING
AND BIOSENSING 127
4.5 CONCLUSIONS 129
ACKNOWLEDGMENTS 130
REFERENCES 130
5 IMMOBILIZATION OF ENZYMES AND OTHER BIOMOLECULES ON GRAPHENE 139
LOANNIS V. PAVLIDIS, MICHAELA PATILA, ANGELIKI C. POLYDERA,
DIMITRIOS GOURNIS, AND HARALAMPOS STAMATIS
5.1 INTRODUCTION 139
VIII CONTENTS
5.2 IMMOBILIZATION APPROACHES 141
5.3 APPLICATIONS OF IMMOBILIZED BIOMOLECULES 145
5.3.1 BIOSENSORS 145
5.3.1.1 GLUCOSE OXIDASE-BASED BIOSENSORS 146
5.3.1.2 HORSERADISH PEROXIDASE-BASED BIOSENSORS 150
5.3.1.3 TYROSINASE-BASED BIOSENSORS 151
5.3.1.4 CYTOCHROME C-BASED BIOSENSORS 152
5.3.1.5 OTHER PROTEIN/ENZYME BIOSENSORS 152
5.3.1.6 DNA SENSORS 152
5.3.1.7 IMMUNOSENSORS AND APTASENSORS 154
5.3.2 BIOCATALYSIS 155
5.3.3 BIOFIIEL CELLS 159
5.3.4 DRUG AND GENE DELIVERY 161
5.4 INTERACTIONS BETWEEN ENZYMES AND NANOMATERIALS 162
5.5 CONCLUSIONS 165
ABBREVIATIONS 165
REFERENCES 166
6 HALOGENATED GRAPHENES: EMERGING FAMILY OF TWO-DIMENSIONAL
MATERIALS 173
KASIBHATTA KUMARA RAMANATHA DATTA AND RADEK ZBOFIL
6.1 INTRODUCTION 173
6.2 SYNTHESIS OF HALOGENATED GRAPHENES 174
6.2.1 FLUOROGRAPHENE 175
6.2.1.1 MECHANICAL OR CHEMICAL EXFOLIATION - FROM GRAPHITE FLUORIDE TO
FLUOROGRAPHENE 175
6.2.1.2 FLUORINATION OF GRAPHENE - FROM GRAPHENE
TO FLUOROGRAPHENE 175
6.2.2 NONSTOICHIOMETRIC FLUORINATED GRAPHENE AND FLUORINATED
GRAPHENE OXIDE 175
6.2.3 OTHER HALOGENATED GRAPHENES 178
6.3 CHARACTERIZATION OF HALOGENATED GRAPHENES 179
6.3.1 FLUOROGRAPHENE 179
6.3.2 PARTIALLY FLUORINATED AND HALOGENATED GRAPHENES 183
6.4 CHEMISTRY, PROPERTIES, AND APPLICATIONS OF FLUOROGRAPHENE AND
FLUORINATED GRAPHENES 184
6.5 CHEMISTRY AND PROPERTIES OF CHLORINATED AND BROMINATED
GRAPHENES 190
6.6 OTHER INTERESTING PROPERTIES OF HALOGENATED GRAPHENES AND THEIR
APPLICATIONS 190
6.7 HALOGENATED GRAPHENE-GRAPHENE HETEROSTRUCTURES - PATTERNED
HALOGENATION 193
6.8 CONCLUSION AND FUTURE PROSPECTS 195
REFERENCES 19 5
CONTENTS
IIX
7 NONCOVALENT FUNCTIONALIZATION OF GRAPHENE 199
KINGSLEY CHRISTIAN KEMP, YEONCHOO CHO, VIMLESH CHANDRA, AND
KWANG SOO KIM
7.1 NONCOVALENT FUNCTIONALIZATION OF GRAPHENE - THEORETICAL
BACKGROUND 199
7.1.1 INSIGHT INTO THE IT-INTERACTION OF BENZENE 200
7.1.2 ADSORPTION ON GRAPHENE 201
7.2 GRAPHENE-LIGAND NONCOVALENT INTERACTIONS-EXPERIMENT 202
7.2.1 POLYCYCLIC MOLECULES 202
7.2.2 BIOMOLECULES 205
7.2.3 POLYMERS 207
7.2.4 OTHER MOLECULES 210
7.3 CONCLUSIONS 213
REFERENCES 213
8 IMMOBILIZATION OF METAL AND METAL OXIDE NANOPARTIDES ON
GRAPHENE 219
GERMAN Y. V&EZ, ARMANDO ENCINAS, AND MILDRED QUINTANA
8.1 INTRODUCTION 219
8.2 GRAPHENE PRODUCTION 219
8.2.1 GRAPHENE OXIDE (GO) 220
8.2.2 FUNCTIONALIZED GRAPHENE (/"-GRAPHENE) 220
8.2.3 GRAPHENE GROWTH ON METAL SURFACES 220
8.2.4 MICROMECHANICAL CLEAVAGE OF GRAPHITE 221
8.3 GRAPHENE FUNCTIONALIZED WITH METAL NANOPARTIDES (M-NPS) 221
8.3.1 GO-REDUCING APPROACH 221
8.3.1.1 REDUCTION ASSISTED BY SONICATION 222
8.3.2 ANCHORING NPS ON/-GRAPHENE 223
8.3.2.1 CONTROLLING SIZE OF NPS 226
8.3.3 APPLICATIONS OF M-NPS/GRAPHENE NANOHYBRIDS 227
8.3.3.1 OPTOELECTRONIC DEVICES 227
8.3.3.2 APPLICATIONS IN CATALYSIS 229
8.3.3.3 APPLICATIONS IN BIOLOGY 232
8.4 GRAPHENE FUNCTIONALIZED WITH METAL OXIDE NANOPARTIDES 233
8.4.1 LITHIUM BATTERIES 233
8.4.2 OPTICAL PROPERTIES 236
8.4.2.1 WATER SPLITTING 237
8.4.2.2 /-GRAPHENE-POM 238
8.4.3 PHOTOCATALYTIC REDUCTION OF GO 238
8.5 GRAPHENE FUNCTIONALIZED WITH MAGNETIC NPS 242
8.5.1 MAGNETIC PROPERTIES 243
8.5.2 APPLICATIONS OF GO-MAG NPS 246
8.5.2.1 MAGNETIC SEPARATION OF METALS AND POLLUTANTS WITH
GO-MAG NPS 247
8.5.2.2 BIOMEDICAL APPLICATIONS OF GO-MAG NPS 248
X | CONTENTS
8.6
9
9.1
9.2
9.2.1
9.2.2
9.3
9.3.1
9.3.2
9.4
9.5
9.6
10
10.1
10.2
10.2.1
10.2.2
10.2.3
10.2.4
10.2.5
10.2.6
10.2.7
10.3
10.3.1
10.3.2
10.3.3
10.3.4
10.4
10.5
10.6
11
11.1
11.2
CONCLUSIONS 252
REFERENCES 252
FUNCTIONALIZATION OF GRAPHENE BY OTHER CARBON NANOSTRUCTURES 255
VASILIOS GEORGAKILAS
INTRODUCTION 255
GRAPHENE-C
60
NANOCOMPOSITES 255
COVALENT BONDING OF C
M
ON GO 256
DEPOSITION OF C
60
ON GRAPHENE 256
GRAPHENE-CNT HYBRID NANOSTRUCTURES 262
GRAPHENE-CNT COMPOSITES BY SIMPLE MUTING 264
GRAPHENE-CNTS HYBRID NANOSTRUCTURES BY DIRECT DEVELOPMENT
OF CNTS ON GRAPHENE SURFACE 272
GRAPHENE-CARBON NANOSPHERES 274
GRAPHENE-CARBON NITRIDE DOTS HYBRID NANOCOMPOSITE 277
CONCLUSIONS 279
REFERENCES 280
DOPING OF GRAPHENE BY NITROGEN, BORON, AND OTHER ELEMENTS 283
ACHUTHARAO GOVINDARAJ AND C.N.R. RAO
INTRODUCTION 283
NITROGEN-DOPED GRAPHENE 284
DC ARCING 284
HEATING WITH AMMONIA, HYDRAZINE, AND OTHER
REAGENTS 287
CHEMICAL FUNCTIONALIZATION ROUTE 288
SOLVOTHERMAL SYNTHESIS 289
CHEMICAL VAPOR DEPOSITION AND PYROLYSIS 293
PYROLYSIS METHODS 300
OTHER METHODS 306
BORON DOPING 320
MECHANICAL EXFOLIATION 321
THERMAL ANNEALING 321
CHEMICAL VAPOR DEPOSITION 323
OTHER METHODS 326
BN DOPING IN GRAPHENE 329
DOPING WITH OTHER ELEMENTS 334
PROPERTIES AND APPLICATIONS 33 9
REFERENCES 352
LAYER-BY-LAYER ASSEMBLY OF GRAPHENE-BASED HYBRID MATERIALS 359
ANTONIOS KOULOUMPIS, PANAGIOTA ZYGOURI, KONSTANTINOS DIMOS, AND
DIMITRIOS GOURNIS
INTRODUCTION
359
LBL GRAPHENE-BASED HYBRID FILMS 360
CONTENTS | XI
11.2.1 HYBRID THIN FILMS FOR ELECTRONICS 360
11.2.2 HYBRID THIN FILMS AS SENSORS 375
11.2.3 HYBRID FILMS FOR OTHER APPLICATIONS 383
11.3 GRAPHENE-BASED HYBRIDS THROUGH THE LANGMUIR-BLODGETT
APPROACH 385
11.3.1 MONOLAYERS OF GRAPHENE OXIDE 385
11.3.2 NANOCOMPOSITE FILMS 389
11.3.3 APPLICATIONS AND PROPERTIES OF LB THIN FILMS 390
11.4 CONCLUSIONS 397
REFERENCES 397
INDEX 401 |
| any_adam_object | 1 |
| author2 | Geōrgakilas, Basilēs |
| author2_role | edt |
| author2_variant | b g bg |
| author_GND | (DE-588)1050751019 |
| author_facet | Geōrgakilas, Basilēs |
| building | Verbundindex |
| bvnumber | BV041846567 |
| classification_rvk | UQ 8225 |
| ctrlnum | (OCoLC)865141998 (DE-599)DNB1044721022 |
| dewey-full | 546.68159 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 546 - Inorganic chemistry |
| dewey-raw | 546.68159 |
| dewey-search | 546.68159 |
| dewey-sort | 3546.68159 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik |
| format | Book |
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV041846567 |
| illustrated | Illustrated |
| indexdate | 2024-09-10T01:13:38Z |
| institution | BVB |
| isbn | 352733551X 9783527335510 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-027291118 |
| oclc_num | 865141998 |
| open_access_boolean | |
| owner | DE-29T DE-11 DE-188 DE-355 DE-BY-UBR DE-19 DE-BY-UBM |
| owner_facet | DE-29T DE-11 DE-188 DE-355 DE-BY-UBR DE-19 DE-BY-UBM |
| physical | XVIII, 406 S. Ill., graph. Darst. |
| publishDate | 2014 |
| publishDateSearch | 2014 |
| publishDateSort | 2014 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Functionalization of Graphene ed. by Vasilios Georgakilas 201405 Weinheim Wiley-VCH 2014 XVIII, 406 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Funktionalisierung Chemie (DE-588)4279323-3 gnd rswk-swf Graphen (DE-588)7591667-8 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Graphen (DE-588)7591667-8 s Funktionalisierung Chemie (DE-588)4279323-3 s DE-604 Geōrgakilas, Basilēs (DE-588)1050751019 edt Erscheint auch als Online-Ausgabe 978-3-527-67279-0 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4526138&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027291118&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Functionalization of Graphene Funktionalisierung Chemie (DE-588)4279323-3 gnd Graphen (DE-588)7591667-8 gnd |
| subject_GND | (DE-588)4279323-3 (DE-588)7591667-8 (DE-588)4143413-4 |
| title | Functionalization of Graphene |
| title_auth | Functionalization of Graphene |
| title_exact_search | Functionalization of Graphene |
| title_full | Functionalization of Graphene ed. by Vasilios Georgakilas |
| title_fullStr | Functionalization of Graphene ed. by Vasilios Georgakilas |
| title_full_unstemmed | Functionalization of Graphene ed. by Vasilios Georgakilas |
| title_short | Functionalization of Graphene |
| title_sort | functionalization of graphene |
| topic | Funktionalisierung Chemie (DE-588)4279323-3 gnd Graphen (DE-588)7591667-8 gnd |
| topic_facet | Funktionalisierung Chemie Graphen Aufsatzsammlung |
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