Non-equilibrium dynamics of lipid bilayers: Time resolved x-ray scattering at in-house and synchrotron sources
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Göttingen
Univ.-verl.
2013
|
| Series: | Göttingen Series in X-ray Physics
12 |
| Subjects: | |
| Online Access: | Beschreibung für Marketing Inhaltstext Inhaltsverzeichnis |
| Physical Description: | II, 140 S. Ill., graph. Darst. |
| ISBN: | 9783863951276 |
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| 245 | 1 | 0 | |a Non-equilibrium dynamics of lipid bilayers |b Time resolved x-ray scattering at in-house and synchrotron sources |c Tobias Reusch |
| 264 | 1 | |a Göttingen |b Univ.-verl. |c 2013 | |
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Record in the Search Index
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CONTENTS
INTRODUCTION 1
1 TIME RESOLVED X-RAY SCATTERING 5
1.1 A TYPICAL PUMP-PROBE EXPERIMENT 5
1.2 IN HOUSE FEMTOSECOND X-RAY GENERATION 8
1.2.1 X-RAY GENERATION IN LASER INDUCED PLASMAS 9
1.2.2 IN HOUSE SETUP FOR TIME RESOLVED X-RAY SCATTERING AT THE PXS 11
1.2.3 OPTICAL EXCITATION MECHANISMS AVAILABLE AT THE PXS . 14
1.2.4 THE TIMING SYSTEM AT THE PXS 16
1.3 TIME RESOLVED EXPERIMENTS AT P08 / PETRA III 18
1.4 TIME RESOLVED DIFFRACTION AT BEAMLINE ID09B. ESRF 23
2 MATERIALS AND METHODS 25
2.1 SURFACE ACOUSTIC WAVE GENERATION 25
2.2 SAMPLE PREPARATION AND ENVIRONMENTS 29
2.3 SPECULAR AND DIFFUSE SCATTERING FROM LIPID MULTILAYERS 31
2.3.1 SPECULAR SCATTERING FROM LIPID MULTILAYERS 33
2.3.2 DIFFUSE SCATTERING FROM LIPID MULTILAYERS 34
3 ULTRAFAST MULTI PHOTON COUNTING * DETECTOR DEVELOPMENT 39
3.1 DESIRED SPECIFICATIONS / ULTRAFAST MULTI PHOTON COUNTING 39
3.2 THE ANALOG SIGNAL CHAIN 42
3.2.1 PREAMPLIFIER 43
3.2.2 GATED INTEGRATOR (BOXCAR AVERAGER) 43
3.2.3 COMMISSIONING OF THE ANALOG SIGNAL CHAIN - SINGLE PHOTON
COUNTING CAPABILITY 47
3.3 HIGH SPEED DATA ACQUISITION AND ONLINE ANALYSIS AT 31MHZ 49
3.3.1 COMMISSIONING OF THE DIGITAL SIGNAL CHAIN - SPEED AND EFFEC
TIVE DYNAMIC RANGE 50
3 4 POWER SUPPLY AND USER INTERFACE 57
3.5 CONCLUSION AND OUTLOOK 59
4 SAW INDUCED DYNAMICS IN LIPID MULTILAYERS 63
4.1 THE HIGH RESOLUTION DIFFRACTION BEAMLINE P08 AT
PETRA III, DESY, HAMBURG 63
4.2 RESULTS - PURE LINBO$ SUBSTRATES 64
4.2.1 GENERAL REMARKS ON X-RAY SCATTERING FROM A SAW DISTORTED
CRYSTAL LATTICE 64
4.2.2 TIME RESOLVED MEASUREMENTS OF THE ROCKING CURVE AT THE FIRST
AND FIFTH HARMONIC SAW FREQUENCY 66
4.2.3 MEASUREMENTS AT THE FIFTH HARMONIC SAW FREQUENCY . 68
4.2.4 THE FIRST HARMONIC SAW FREQUENCY 69
4.2.5 HIGHER ACOUSTIC HARMONIC GENERATION? 70
HTTP://D-NB.INFO/1038272882
II
CONTENTS
4.2.6 ANALYTIC CALCULATION OF THE STRUCTURE FACTOR OF A SAW DIS
TORTED CRYSTAL LATTICE IN KINEMATIC APPROXIMATION 72
4.3 RESULTS - LIPIDS EXCITED BY SAWS OF RAYLEIGH TYPE 74
4.4 CONCLUSIONS 79
5 LASER INDUCED STRUCTURAL DYNAMICS 81
5.1 PURE PHOSPHOLIPIDS ON SILICON SUBSTRATES 81
5.1.1 PREPARATORY EXPERIMENTS AT THE IN-HOUSE FEMTOSECOND X-RAY
SOURCE 81
5.1.2 X-RAY SCATTERING SETUP AT THE ID09B AT THE ESRF, GRENOBLE 88
5.1.3 ELIMINATION OF LASER AND X-RAY INDUCED DRIFT - SAMPLE ENVI
RONMENTS AND POSSIBLE PITFALLS 88
5.1.4 EXCITATION OF LIPID MULTILAYERS ON SILICON SUBSTRATES BY NANOSEC
OND LASER PULSES - A MOLECULAR MOVIE 92
5.1.5 CONCLUSION 99
5.2 COLLECTIVE UNDULATIONS IN TEXAS-RED LABELED LIPID MULTILAYERS .
100
5.2.1 CONCLUSIONS 107
6 SUMMARY AND OUTLOOK 109
A APPENDIX 111
A.L EXCITATION MECHANISMS FOR LIPID BILAYERS ILL
A. 1.1 EXCITATION OF LIPID MEMBRANES BY PULSED LASER RADIATION . . ILL
A.1.2 LIPID BILAYERS EXCITED BY STRONG ELECTRIC FIELD PULSES 112
A.1.3 THE HIGH VOLTAGE PULSER / THE THIN FILM DIFFRACTION CHAMBER 116
A.2 IONIZATION CHAMBERS IN THE CASE OF FEMTOSECOND X-RAY PULSES . 119
A.3 ELECTRONIC SCHEMATICS OF THE PREAMPLIFIER CIRCUIT 121
A.4 ELECTRONIC SCHEMATICS OF THE GATED INTEGRATOR 124
A.5 ELECTRONIC SCHEMATICS OF THE POWER SUPPLY CIRCUIT 127
REFERENCES 131
DANKSAGUNG 141 |
| any_adam_object | 1 |
| author | Reusch, Tobias 1983- |
| author_GND | (DE-588)1043601465 |
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| author_variant | t r tr |
| building | Verbundindex |
| bvnumber | BV041457256 |
| classification_rvk | UM 3280 |
| ctrlnum | (OCoLC)915303862 (DE-599)DNB1038272882 |
| dewey-full | 537.535 |
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| dewey-ones | 537 - Electricity and electronics |
| dewey-raw | 537.535 |
| dewey-search | 537.535 |
| dewey-sort | 3537.535 |
| dewey-tens | 530 - Physics |
| discipline | Physik |
| format | Book |
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| id | DE-604.BV041457256 |
| illustrated | Illustrated |
| indexdate | 2024-08-03T01:06:52Z |
| institution | BVB |
| isbn | 9783863951276 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-026903683 |
| oclc_num | 915303862 |
| open_access_boolean | |
| owner | DE-83 |
| owner_facet | DE-83 |
| physical | II, 140 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Univ.-verl. |
| record_format | marc |
| series | Göttingen Series in X-ray Physics |
| series2 | Göttingen Series in X-ray Physics |
| spelling | Reusch, Tobias 1983- Verfasser (DE-588)1043601465 aut Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources Tobias Reusch Göttingen Univ.-verl. 2013 II, 140 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Göttingen Series in X-ray Physics 12 Lipide (DE-588)4035873-2 gnd rswk-swf Doppelschicht (DE-588)4150451-3 gnd rswk-swf Nichtgleichgewicht (DE-588)4171730-2 gnd rswk-swf Nichtgleichgewicht (DE-588)4171730-2 s Lipide (DE-588)4035873-2 s Doppelschicht (DE-588)4150451-3 s DE-604 Göttingen Series in X-ray Physics 12 (DE-604)BV037380493 12 X:MVB text/html http://www.univerlag.uni-goettingen.de/content/list.php?notback=1&details=isbn-978-3-86395-127-6 Beschreibung für Marketing X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4417773&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026903683&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Reusch, Tobias 1983- Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources Göttingen Series in X-ray Physics Lipide (DE-588)4035873-2 gnd Doppelschicht (DE-588)4150451-3 gnd Nichtgleichgewicht (DE-588)4171730-2 gnd |
| subject_GND | (DE-588)4035873-2 (DE-588)4150451-3 (DE-588)4171730-2 |
| title | Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources |
| title_auth | Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources |
| title_exact_search | Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources |
| title_full | Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources Tobias Reusch |
| title_fullStr | Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources Tobias Reusch |
| title_full_unstemmed | Non-equilibrium dynamics of lipid bilayers Time resolved x-ray scattering at in-house and synchrotron sources Tobias Reusch |
| title_short | Non-equilibrium dynamics of lipid bilayers |
| title_sort | non equilibrium dynamics of lipid bilayers time resolved x ray scattering at in house and synchrotron sources |
| title_sub | Time resolved x-ray scattering at in-house and synchrotron sources |
| topic | Lipide (DE-588)4035873-2 gnd Doppelschicht (DE-588)4150451-3 gnd Nichtgleichgewicht (DE-588)4171730-2 gnd |
| topic_facet | Lipide Doppelschicht Nichtgleichgewicht |
| url | http://www.univerlag.uni-goettingen.de/content/list.php?notback=1&details=isbn-978-3-86395-127-6 http://deposit.dnb.de/cgi-bin/dokserv?id=4417773&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026903683&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV037380493 |
| work_keys_str_mv | AT reuschtobias nonequilibriumdynamicsoflipidbilayerstimeresolvedxrayscatteringatinhouseandsynchrotronsources |