Inorganic micro- and nanomaterials: synthesis and characterization
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
De Gruyter
2013
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XIV, 215 S. 240 mm x 170 mm |
| ISBN: | 9783110306668 |
Internformat
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Datensatz im Suchindex
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IMAGE 1
TABLE OF CONTENTS
INTRODUCTION: NANO- (AND MICRO-)MATERIALS AND HUMAN WELLBEING 1
1 COATING ANTIBACTERIAL NANOPARTICLES ON TEXTILES: TOWARDS THE FUTURE
HOSPITAL IN WHICH ALL TEXTILES WILL BE ANTIBACTERIAL 3
1.1 INTRODUCTION: APPLICATION OF NANOTECHNOLOGY FOR "SMART" TEXTILES 3
1.2 SONOCHEMICAL METHOD FOR THE SYNTHESIS OF NANOSTRUCTURED MATERIALS
AND
THEIR ADHERENCE TO SOLID SUBSTRATES 6
1.3 ULTRASOUND ASSISTED DEPOSITION OF METAL NANO-OXIDES ON TEXTILES AND
THEIR
ANTIBACTERIAL PROPERTIES 8
1.3.1 SYNTHESIS AND DEPOSITION OF CUO NANOPARTICLES 8
1.3.2 FINISHING OF TEXTILES WITH CRYSTALLINE TI0 2 NANOPARTICLES VIA A
ONE-STEP
PROCESS 10
1.3.3 SYNTHESIS AND DEPOSITION OF ZNO 16
1.3.4 ENZYMATIC PRETREATMENT AS A MEANS OF ENHANCING ANTIBACTERIAL
ACTIVITY
AND STABILITY OF ZNO NANOPARTICLES SONOCHEMICALLY COATED ON COTTON
FABRICS 22
1.3.5 SIZE DEPENDENCE OF THE ANTIBACTERIAL ACTIVITY OF ZNO NPS 28
1.4 CONCLUSION 28
BIBLIOGRAPHY 29
2 AUTOMATED SOLUTIONS FOR HIGH-THROUGHPUT EXPERIMENTATION IN
HETEROGENEOUS CATALYST RESEARCH 35
2.1 INTRODUCTION 35
2.2 THE PREPARATION OF SOLID CATALYSTS 37
2.3 AUTOMATION CHALLENGES EXAMPLES 37
2.3.1 INTEGRATION OF COMMERCIALLY AVAILABLE DEVICES 38
2.4 A FULLY-AUTOMATED SOLUTION 39
2.4.1 SOPHAS-CAT HT 39
2.4.2 THE LOADING 39
2.4.3 THE SYNTHESIZER 40
2.4.4 EXTRUDATE PREPARATION 41
2.4.5 IMPREGNATION AND DRYING 41
2.4.6 CALCINATION 42
2.4.7 SCRAPING AND PELLETIZING 42
2.4.8 GRINDING 43
2.4.9 SIEVING 43
2.5 CONCLUSION 44
BIBLIOGRAPHY 45
HTTP://D-NB.INFO/1028834330
IMAGE 2
XII ~ ~ TABLE OF CONTENTS
3 INSIGHTS FROM XPS ON NANOSIZED INORGANIC MATERIALS 47
3.1 INTRODUCTION 47
3.2 XPS IN THE NANODOMAIN 47
3.3 CONCLUSIONS 53
BIBLIOGRAPHY 55
4 SINGLE CRYSTAL AND POWDER XRD TECHNIQUES: AN OVERVIEW 57
4.1 THE SINGLE CRYSTAL XRD TECHNIQUE 57
4.1.1 BASICS OF THE RADIATION-MATTER INTERACTION 58
4.1.2 BASICS OF CRYSTALLOGRAPHY AND X-RAY DIFFRACTION BY CRYSTAL 61
4.1.3 SOLVING THE PHASE PROBLEM BY DIRECT METHODS 69
4.2 THE POWDER XRD TECHNIQUE 74
4.2.1 INDEXATION 74
4.2.2 SPACE GROUP DETERMINATION 76
4.2.3 PROFILE DECOMPOSITION AND INTENSITY EXTRACTION 77
4.2.4 STRUCTURE SOLUTION 79
4.2.5 RIETVELD REFINEMENT 84
4.2.6 EXAMPLES 85
4.3 CONCLUSIONS 88
BIBLIOGRAPHY 89
5 STRUCTURAL AND ELECTRONIC CHARACTERIZATION OF NANOSIZED INORGANIC
MATERIALS BY X-RAY ABSORPTION SPECTROSCOPIES 93
5.1 INTRODUCTION 93
5.2 XAS SPECTROSCOPY: BASIC BACKGROUND 93
5.2.1 THEORETICAL BACKGROUND OF XAS SPECTROSCOPY 94
5.2.2 THE XANES REGION 96
5.2.3 THE EXAFS REGION 96
5.2.4 ADVANTAGES AND DRAWBACKS OF THE TECHNIQUE 99
5.3 CUCI 2/AI203-BASED CATALYSTS FOR ETHYLENE OXYCHLORINATION 100
5.3.1 INDUSTRIAL RELEVANCE OF THE CUCL 2/AL203 SYSTEM 100
5.3.2 PRELIMINARY IN SITU XAFS EXPERIMENTS 101
5.3.2.1 THE DETERMINATION OF THE CU-ALUMINATE PHASE: HOW TO AVOID
POSSIBLE
PITFALLS IN THE EXAFS DATA ANALYSIS 101
5.3.2.2 CATALYST REACTIVITY WITH THE SEPARATE REACTANTS: IN SITU XAFS
EXPERIMENTS 103
5.3.3 OPERANDO EXPERIMENTS AND CRITERIA USED TO FACE THE PRESENCE OF
MORE
THAN ONE PHASE IN THE SAMPLE 105
5.4 STRUCTURAL AND ELECTRONIC CONFIGURATION OF CP 2CR MOLECULES
ENCAPSULATED
IN PS AND NA-Y ZEOLITE AND THEIR REACTIVITY TOWARDS CO 109
5.4.1 STRUCTURE OF CP 2CR ENCAPSULATED IN PS AND NA-Y ZEOLITE MATRICES
109
IMAGE 3
TABLE OF CONTENTS - XIII
5.4.2 DETERMINATION OF THE ELECTRONIC STRUCTURE OF CP 2CR BY COMBINED
UV-VIS
AND XANES SPECTROSCOPIES 111
5.4.3 REACTIVITY OF CP 2CR HOSTED IN PS AND IN NA-Y ZEOLITE TOWARDS CO:
IR AND
XAFS RESULTS 114
5.5 TRANSITION METAL COMPLEXES IN SOLUTION: THE [CIS-RU(BPY) 2(PY ) 2 ]
2 + CASE
STUDY 117
5.5.1 STRUCTURE REFINEMENT OF CIS-[RU(BPY) 2(PY)2] 2 + IN AQUEOUS
SOLUTION BY
EXAFS SPECTROSCOPY 118
5.5.2 ADVANCED DETAILS OF THE EXAFS STRUCTURE REFINEMENT OF CIS[RU(BPY)
2(PY)2] 2+ COMPLEX 120
5.6 EXAFS STUDY ON MOFS OF THE UIO-66/UIO-67 FAMILY: COMPARISON WITH
XRPD AND AB INITIO INVESTIGATIONS 122
5.7 APPLICATIONS OF X-RAY MICRO BEAMS: ELECTROABSORPTION MODULATED LASER
FOR
OPTOELECTRONIC DEVICES 127
BIBLIOGRAPHY 129
6 LENS-LESS SCANNING X-RAY MICROSCOPY WITH SAXS AND WAXS
CONTRAST 137
6.1 INTRODUCTION 137
6.2 X-RAY MICROSCOPES 138
6.3 SMALL-ANGLE AND WIDE-ANGLE SCATTERING CONTRAST (SAXS AND WAXS) 143
6.4 APPLICATIONS 149
BIBLIOGRAPHY 154
7 CHARACTERIZATION OF INORGANIC NANOSTRUCTURED MATERIALS BY ELECTRON
MICROSCOPY -157
7.1 INTRODUCTION 157
7.2 ELECTRON MICROSCOPY 158
7.2.1 WORKING PRINCIPLES 159
7.3 SCANNING ELECTRON MICROSCOPY 161
7.3.1 MAGNIFICATION AND RESOLUTION OF SEM 163
7.3.2 INTERACTION OF THE ELECTRON BEAM WITH THE SAMPLE: ELASTIC AND
INELASTIC
SCATTERING 163
7.3.2.1 SECONDARY ELECTRONS AND THEIR DETECTION 164
7.3.2.2 BACKSCATTERED ELECTRONS AND THEIR DETECTION 166
7.3.2.3 ENERGY LOSS 167
7.4 TRANSMISSION ELECTRON MICROSCOPY 167
7.4.1 THE INSTRUMENT 168
7.4.2 IMAGE FORMATION PROCESS 169
7.5 SAMPLE PREPARATION FOR ELECTRON MICROSCOPY 174
7.5.1 SEM SAMPLE PREPARATION 174
7.5.1.1 CASTING 174
IMAGE 4
XIV TABLE OF CONTENTS
7.5.1.2 ION SPUTTERING 175
7.5.2 SAMPLE PREPARATION FOR TEM 175
7.6 INORGANIC NANOCRYSTAL INVESTIGATION BY SEM 177
7.7 INORGANIC NANOCRYSTAL INVESTIGATION BY TEM 186
7.7.1 BRIGHT FIELD MODE 186
7.7.2 DARK FIELD CONTRAST MODE 189
7.7.3 DIFFRACTION MODE - ELECTRON DIFFRACTION 190
7.7.3.1 SELECTED AREA DIFFRACTION 191
7.7.3.2 CONVERGENT BEAM ELECTRON DIFFRACTION 191
7.7.3.3 INVESTIGATING CRYSTALLINE STRUCTURE: HIGH-RESOLUTION TEM 192
7.8 CHEMICAL ANALYSIS BY ELECTRON MICROSCOPY 193
7.8.1 ENERGY DISPERSION SPECTROSCOPY (EDS) 193
7.8.2 ELECTRON ENERGY LOSS SPECTROSCOPY (EELS) 194
7.8.3 ENERGY-FILTERED TRANSMISSION ELECTRON MICROSCOPY (EFTEM) 195
7.8.4 SOME EXAMPLES OF CHEMICAL ANALYSIS IN ELECTRON MICROSCOPY 195
7.9 CONCLUSIONS 197
BIBLIOGRAPHY 197
8 NANOSIZED PARTICLES: QUESTIONED FOR THEIR POTENTIAL TOXICITY, BUT SOME
ARE
APPLIED IN BIOMEDICINE 199
8.1 INTRODUCTION 199
8.2 NANOPARTICLES CLASSIFICATION 199
8.3 NANOPARTICLES AND BIOSYSTEMS 201
8.4 STABILITY AND TOXICITY 202
8.5 FIELDS OF APPLICATION OF ENGINEERED NANOPARTICLES 203
8.6 ACCESS TO BIO-ORGANISMS AND TOXICITY TO ORGANISMS 204
8.7 APPLICATIONS OF NANOPARTICLES IN BIOMEDICINE 205
8.8 MEASUREMENT OF THE CONCENTRATION 206
8.9 CONCLUSIONS 206
BIBLIOGRAPHY 207
INDEX 211 |
| any_adam_object | 1 |
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| illustrated | Not Illustrated |
| indexdate | 2024-08-03T00:57:46Z |
| institution | BVB |
| isbn | 9783110306668 |
| language | English |
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| spelling | Inorganic micro- and nanomaterials synthesis and characterization ed. by Angela Dibenedetto ... Berlin [u.a.] De Gruyter 2013 XIV, 215 S. 240 mm x 170 mm txt rdacontent n rdamedia nc rdacarrier Nanostrukturiertes Material (DE-588)4342626-8 gnd rswk-swf Chemische Synthese (DE-588)4133806-6 gnd rswk-swf Anorganischer Werkstoff (DE-588)4142570-4 gnd rswk-swf Herstellung (DE-588)4159653-5 gnd rswk-swf Strukturanalyse (DE-588)4183787-3 gnd rswk-swf 1\p (DE-588)4143413-4 Aufsatzsammlung gnd-content Anorganischer Werkstoff (DE-588)4142570-4 s Nanostrukturiertes Material (DE-588)4342626-8 s Herstellung (DE-588)4159653-5 s Chemische Synthese (DE-588)4133806-6 s Strukturanalyse (DE-588)4183787-3 s DE-604 Dibenedetto, Angela 1968- (DE-588)1043471332 edt Erscheint auch als Online-Ausgabe 978-3-11-030687-3 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4208619&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026745204&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Inorganic micro- and nanomaterials synthesis and characterization Nanostrukturiertes Material (DE-588)4342626-8 gnd Chemische Synthese (DE-588)4133806-6 gnd Anorganischer Werkstoff (DE-588)4142570-4 gnd Herstellung (DE-588)4159653-5 gnd Strukturanalyse (DE-588)4183787-3 gnd |
| subject_GND | (DE-588)4342626-8 (DE-588)4133806-6 (DE-588)4142570-4 (DE-588)4159653-5 (DE-588)4183787-3 (DE-588)4143413-4 |
| title | Inorganic micro- and nanomaterials synthesis and characterization |
| title_auth | Inorganic micro- and nanomaterials synthesis and characterization |
| title_exact_search | Inorganic micro- and nanomaterials synthesis and characterization |
| title_full | Inorganic micro- and nanomaterials synthesis and characterization ed. by Angela Dibenedetto ... |
| title_fullStr | Inorganic micro- and nanomaterials synthesis and characterization ed. by Angela Dibenedetto ... |
| title_full_unstemmed | Inorganic micro- and nanomaterials synthesis and characterization ed. by Angela Dibenedetto ... |
| title_short | Inorganic micro- and nanomaterials |
| title_sort | inorganic micro and nanomaterials synthesis and characterization |
| title_sub | synthesis and characterization |
| topic | Nanostrukturiertes Material (DE-588)4342626-8 gnd Chemische Synthese (DE-588)4133806-6 gnd Anorganischer Werkstoff (DE-588)4142570-4 gnd Herstellung (DE-588)4159653-5 gnd Strukturanalyse (DE-588)4183787-3 gnd |
| topic_facet | Nanostrukturiertes Material Chemische Synthese Anorganischer Werkstoff Herstellung Strukturanalyse Aufsatzsammlung |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4208619&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026745204&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT dibenedettoangela inorganicmicroandnanomaterialssynthesisandcharacterization |