Microreactors in preparative chemistry: practical aspects in bioprocessing, nanotechnology, catalysis and more
Saved in:
| Format: | Book |
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| Language: | English |
| Published: |
Weinheim
Wiley-VCH-Verl.
2013
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| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Item Description: | Literaturangaben |
| Physical Description: | XV, 335 S. Ill., graph. Darst. 24 cm |
| ISBN: | 9783527332823 9783527652921 9783527652914 9783527652907 9783527652891 3527332820 |
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Record in the Search Index
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| adam_text |
IMAGE 1
.1
.2
.3
.3.1 .3.2 .3.3 .4 [5
.1 .2
.3
.3.1 .3.2 .4 .4.1
.4.2 .4.2. .4.2. .4.3 .4.3. .4.3. .5 .5.1 .5.2
CONTENTS
PREFACE X I
LIST OF CONTRIBUTORS X I I I
PRINCIPLES OF MICROPROCESS TECHNOLOGY 1 WLADIMIR RESCHETILOWSKI
INTRODUCTION 1
HISTORY 2
BASIC CHARACTERISTICS 3 MICROFLUIDICS AND MICROMIXING 4 TEMPERATURE AND
PRESSURE CONTROL 5 SAFETY AND ECOLOGICAL IMPACT 7
INDUSTRIAL APPLICATIONS 8 CONCLUDING REMARKS 9 REFERENCES 10
EFFECTS OF MICROFLUIDICS ON PREPARATIVE CHEMISTRY PROCESSES 13
MADHVANAND KASHID, ALBERT RENKEN, AND LIOUBOV KIWI-MINSKER INTRODUCTION
13 MIXING 15
HEAT MANAGEMENT 18 HEAT TRANSFER IN CONTINUOUS-FLOW DEVICES 19 HEAT
CONTROL OF MICROCHANNEL REACTORS 22 MASS TRANSFER AND CHEMICAL REACTIONS
26 FLUID-SOLID CATALYTIC SYSTEMS 26 FLUID-FLUID SYSTEMS 31 FLOW REGIMES
32 MASS TRANSFER 34 THREE-PHASE SYSTEMS 36
GAS-LIQUID-SOLID SYSTEMS 36 GAS-LIQUID-LIQUID SYSTEMS 40 FLOW SEPARATION
40 GEOMETRICAL MODIFICATIONS 41
WETTABILITY-BASED FLOW SPLITTERS 42
HTTP://D-NB.INFO/103164735X
IMAGE 2
VII CONTENTS
2.5.3 CONVENTIONAL SEPARATOR ADAPTED FOR MICROSTRUCTURED REACTORS 44
2.6 NUMBERING-UP STRATEGY 45
2.7 PRACTICAL EXERCISE: EXPERIMENTAL CHARACTERIZATION OF MIXING IN
MICROSTRUCTURED REACTORS 46 REFERENCES 50
3 MODULAR MICRO- AND MILLIREACTOR SYSTEMS FOR PREPARATIVE CHEMICAL
SYNTHESIS AND BIOPROCESSES 55 FRANK SCHAE! M MARC-OLIVER PIEPENBROCK,
J'ORN EMMERICH, AND JOACHIM HECK 3.1 INTRODUCTION 55
3.2 MODULAR MICROREACTION SYSTEM 57
3.3 EXAMPLES FOR MICROREACTOR APPLICATIONS 60 3.3.1 SYNTHESIS OF VITAMIN
A ACETATE 60
3.3.2 SCREENING OF PROCESS PARAMETERS FOR A SUZUKI-MIYAURA REACTION 62
3.3.3 SCALE-UP OF THERMAL REARRANGEMENT OF FURFURYL ALCOHOL 64 3.3.4
ONLINE REACTION MONITORING AND AUTOMATION OF CHEMICAL SYNTHESIS AND
BIOPROCESSES 66
3.4 LABORATORY EXERCISE: SUZUKI REACTION IN A MODULAR MICROREACTOR SETUP
70
REFERENCES 73
4 POTENTIAL OF LAB-ON-A-CHIP: SYNTHESIS, SEPARATION, AND ANALYSIS OF
BIOMOLECULES 77 MARTIN BERTAU 4.1 INTRODUCTION 77
4.2 LEARNING FROM NATURE: ANALOGIES TO LIVING CELLS 77 4.3 MICROENZYME
REACTORS 79
4.3.1 ENZYME IMMOBILIZATION ON THE MICROCHANNEL SURFACE 80 4.3.2 ENZYME
IMMOBILIZATION ON SUPPORTS 81 4.3.3 MODES OF OPERATION 81
4.3.4 ENZYMATIC CONVERSIONS 81
4.3.5 ENZYMATIC CLEAVAGE OF PEPTIDES 84 4.3.6 DETERMINATION OF INHIBITOR
PROPERTIES 84 4.3.7 CYTOTOXICITY ASSESSMENT 87
4.4 MICROCHIP ELECTROPHORESIS 87
4.4.1 PEPTIDE ANALYSIS 88
4.4.2 CHIRAL SEPARATION 88
4.4.3 COUPLING BIOCATALYSIS AND ANALYSIS 88 4.4.4 DETERMINATION OF AMINO
ACIDS IN GOODS AND FOODS 89 4.5 MICROENZYME MEMBRANE
REACTOR/MICROMEMBRANE CHROMATOGRAPHY 89
4.6 NUCLEIC ACID ANALYSIS IN MICROCHANNELS 91
4.7 SACCHARIDE ANALYSES IN MICRODEVICES 94
4.8 PRACTICAL EXERCISE: LIPASE-CATALYZED ESTERIFICATION REACTION 96
REFERENCES 97
IMAGE 3
CONTENTS IVII
5 BIOPROCESSING IN MICROREACTORS 101
FRIDOLIN OKKELS AND DOROTA KWASNY 5.1 INTRODUCTION 101
5.2 BACKGROUND 101
5.2.1 BASIC ELEMENTS OF A BIOSENSOR 101
5.2.2 DIFFERENT SENSING METHODS 103
5.2.3 THE EFFECT OF REDUCING DIMENSIONALITY AND LENGTH SCALES OF
BIOSENSORS 103 5.2.4 .BIOSENSORS BASED ON FIELD-EFFECT TRANSISTORS 104
5.2.4.1 THE MAIN WORKING PRINCIPLE OF FET SENSORS 105
5.2.4.2 FABRICATION OF SINW FET SENSORS 306 5.2.4.3 FUNCTIONALIZATION OF
SINW FET SENSORS USING APTES 107 5.2.5 SHIELDING BY THE BUFFER COMBINED
INFLUENCE FROM IONS AND CHARGE CARRIERS 107 5.3 PRACTICAL EXERCISE:
FUNCTIONALIZATION OF SILICON SURFACE 108
REFERENCES 113
6 SYNTHESIS OF FINE CHEMICALS 115
SANDRA HUBNER, NORBERT STEINFELDT, AND KLAUSJAHNISCH 6.1 INTRODUCTION
115
6.2 ORGANIC SYNTHESIS IN LIQUID AND LIQUID-LIQUID PHASES 116 6.2.1
FLUORINATION REACTIONS 116
6.2.2 REACTIONS WITH DIAZOMETHANE 127 6.2.3 ULTRASOUND-ASSISTED
LIQUID-LIQUID BIPHASIC AND LIQUID REACTIONS 134 6.3 GAS-LIQUID BIPHASIC
ORGANIC SYNTHESIS 141
6.3.1 OZONOLYSIS REACTIONS 141
6.3.2 PHOTOOXYGENATION REACTIONS 151 6.4 PRACTICAL EXERCISE:
PHOTOCHEMICAL GENERATION OF SINGLET OXYGEN AND ITS [4 + 2] CYCLOADDITION
TO CYCLOPENTADIENE 159 REFERENCES 161
7 SYNTHESIS OF NANOMATERIALS USING CONTINUOUS-FLOW MICROREACTORS 165
CHIH-HUNG CHANG 7.1 INTRODUCTION 165
7.2 MICROFLUIDIC DEVICES 165
7.3 SYNTHESIS OF NANOMATERIALS USING MICROREACTORS 166 7.4 KINETIC
STUDIES 180
7.5 PROCESS OPTIMIZATION 183
7.6 POINT-OF-USE SYNTHESIS AND DEPOSITION 185
7.6.1 DEPOSITION OF NANOMATERIALS 185
7.7 PRACTICAL EXERCISES: SYNTHESIS OF NANOCRYSTALS 187 7.7.1 SYNTHESIS
OF ZNO NANOCRYSTALS 187
71.2 SYNTHESIS OF CDS NANOPARTICLES 190
REFERENCES 192
IMAGE 4
VILLI CONTENTS
8 POLYMERIZATION IN MICROFLUIDIC REACTORS 197
JESSE GREENER AND EUGENIA KUMACHEVA 8.1 INTRODUCTION 197
8.2 PRACTICAL CONSIDERATIONS 198
8.2.1 CONTROL OVER REACTION CONDITIONS 198 8.2.1.1 BATCH REACTORS 198
8.2.1.2 MICROREACTORS 199
8.2.2 CONTROL OF MIXING 199
8.2.3 CONTROL OF REAGENT CONCENTRATIONS 200 8.2.4 DISTANCE-TO-TIME
TRANSFORMATION 200 8.2.5 POTENTIAL NEGATIVE IMPACTS OF POLYMERIZATION
REACTIONS ON REACTOR OPERATION 201
8.2.5.1 BUILDUP IN SOLUTION VISCOSITY 201 8.2.5.2 PRECIPITATION 202
8.2.5.3 ADSORPTION 202
8.2.6 SELECTION OF MATERIALS FOR FABRICATION OF MF REACTORS 203 8.2.6.1
POLYMER MATERIALS 203 8.2.6.2 METALS 205
8.2.6.3 GLASS 205
8.3 SINGLE-PHASE POLYMERIZATION 205
8.4 MULTIPHASE POLYMERIZATION 208
8.4.1 FORMATION OF POLYMER PARTICLES 209
8.4.1.1 FORMATION OF PRECURSOR DROPLETS 209 8.4.1.2 TRANSFORMATION OF
PRECURSOR DROPLETS INTO POLYMER PARTICLES 213 8.4.2 REVIEW OF
DEMONSTRATED APPLICATIONS 214 8.4.2.1 CONTROLLED ENCAPSULATION 214
8.4.2.2 ENCAPSULATION AND DELIVERY 215
8.4.2.3 CELL ENCAPSULATION 217 8.4.2.4 MICROGELS AS MODEL CELLS 219 8.5
BEYOND SYNTHESIS: NEW DEVELOPMENTS FOR NEXT-GENERATION MF POLYMERIZATION
220
8.5.1 SCALED-UP MF SYNTHESIS OF POLYMER PARTICLES 220 8.5.2 IN SITU
CHARACTERIZATION OF POLYMERIZATION IN MF REACTORS 223 8.5.3 AUTOMATED
SYSTEMS FOR POLYMERIZATION MICROREACTORS 223 8.6 PRACTICAL EXERCISE: MF
POLYMERIZATION REACTOR KINETICS STUDIES USING
IN SITU CHARACTERIZATION 224 REFERENCES 227
9 ELECTROCHEMICAL REACTIONS IN MICROREACTORS 231
JUN-ICHI YOSHIDA AND AIICHIRO NAGAKI 9.1 INTRODUCTION 231
9.2 ELECTRODE CONFIGURATION 232
9.2.1 SERIAL ELECTRODE CONFIGURATION 232 9.2.2 INTERDIGITATED ELECTRODE
CONFIGURATION 233
IMAGE 5
CONTENTS IIX
9.2.3 PARALLEL ELECTRODE CONFIGURATION 233
9.3 ELECTROLYSIS WITHOUT SUPPORTING ELECTROLYTES 234 9.4 GENERATION AND
REACTIONS WITH UNSTABLE INTERMEDIATES 235 9.5 PRACTICAL EXERCISE:
ELECTROCHEMICAL REACTIONS IN FLOW MICROREACTORS 239
REFERENCES 241
10 HETEROGENEOUS CATALYSIS IN MICROREACTORS 243 EVGENY V. REBROV 10.1
INTRODUCTION 243
10.2 BULK CATALYSTS 244
10.3 SUPPORTED CATALYSTS 246
10.3.1 MACROPOROUS SUPPORTS 247 10.3.1.1 ZNO SUPPORT 247 10.3.1.2 -Y-AL
2C 3 SUPPORT 247 10.3.1.3 CATALYSTS IMMOBILIZED ONTO POLYMERIC PARTICLES
249 10.3.1.4 SILICA-SUPPORTED CATALYSTS 251 10.3.1.5 CARBON-SUPPORTED
CATALYSTS 253 10.4 MESOPOROUS SUPPORTS 256
10.4.1 MESOPOROUS TITANIA 258
10.4.2 MESOPOROUS SILICA 260
10.4.3_ MESOPOROUS ALUMINA 263 10.5 MICROPOROUS SUPPORTS 261
10.6 PRACTICAL EXERCISE: PDZN/TI0 2-CATALYZED SELECTIVE * HYDROGENATION
OF ACETYLENE ALCOHOLS IN A CAPILLARY MICROREACTOR 263 REFERENCES 265
11 CHEMICAL INTENSIFICATION IN FLOW CHEMISTRY THROUGH HARSH REACTION
CONDITIONS AND NEW REACTION DESIGN 273 TIMOTHY NOEL AND VOLKER HESSE!
11.1 INTRODUCTION 273
11.2 HIGH-TEMPERATURE PROCESSING IN MICROFLOW 273 11.3 HIGH-PRESSURE
PROCESSING IN MICROFLOW 278 11.4 SOLVENT EFFECTS IN MICROFLOW 280
11.5 EX-REGIME PROCESSING AND HANDLING OF HAZARDOUS COMPOUNDS IN
MICROFLOW 283 11.6 NEW CHEMICAL TRANSFORMATIONS IN MICROFLOW 284 11.7
PROCESS INTEGRATION IN MICROFLOW 286
11.8 PRACTICAL EXERCISES 288
11.8.1 CLAISEN REARRANGEMENT AT ELEVATED TEMPERATURES 288 11.8.2
COPPER(I)-CATALYZED AZIDE-ALKYNE CYDOADDITION WITH INTEGRATED COPPER
SCAVENGING UNIT 290 REFERENCES 292
IMAGE 6
X | CONTENTS
12 MODELING IN MICROREACTORS 297
EKATERINA S. BOROVINSKAYA 12.1 INTRODUCTION 297
12.2 PROCESSES IN MICROREACTORS AND THE ROLE OF MIXING 298 12.3 MODELING
OF PROCESSES IN MICROREACTORS BASED ON GENERAL BALANCE EQUATION 300
12.3.1 PLUG FLOW TUBE REACTOR MODEL 300 12.3.2 LAMINAR FLOW MODEL 302
12.4 COMPUTATIONPF REACTION FLOWS IN MICROREACTORS 308 12.4.1
COMPUTATIONAL FLUID DYNAMICS 308 12.4.2 SINGLE-PHASE MODELING 309 12.4.3
TWO-PHASE MODELING 310
12.4.3.1 LIQUID-LIQUID FLOW WITH CHEMICAL REACTION 310 12.4.3.2
LIQUID-GAS FLOW WITH CHEMICAL REACTION 312 12.4.4 THREE-PHASE MODELING
315 12.5 PRACTICAL EXERCISE: ALKYLATION OF PHENYLACETONITRILE 320
REFERENCES 323
INDEX 327 |
| any_adam_object | 1 |
| author_GND | (DE-588)1038701295 |
| building | Verbundindex |
| bvnumber | BV041282158 |
| classification_rvk | VN 7320 |
| classification_tum | CIT 920f CIT 325f |
| ctrlnum | (OCoLC)857912501 (DE-599)DNB103164735X |
| dewey-full | 660.2832 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660.2832 |
| dewey-search | 660.2832 |
| dewey-sort | 3660.2832 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie Chemie-Ingenieurwesen Biotechnologie |
| format | Book |
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV041282158 |
| illustrated | Illustrated |
| indexdate | 2024-08-03T00:56:35Z |
| institution | BVB |
| isbn | 9783527332823 9783527652921 9783527652914 9783527652907 9783527652891 3527332820 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-026255576 |
| oclc_num | 857912501 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-703 DE-634 DE-188 DE-29T |
| owner_facet | DE-91G DE-BY-TUM DE-703 DE-634 DE-188 DE-29T |
| physical | XV, 335 S. Ill., graph. Darst. 24 cm |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley-VCH-Verl. |
| record_format | marc |
| spelling | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more ed. by Wladimir Reschetilowski Weinheim Wiley-VCH-Verl. 2013 XV, 335 S. Ill., graph. Darst. 24 cm txt rdacontent n rdamedia nc rdacarrier Literaturangaben Mikrosystemtechnik (DE-588)4221617-5 gnd rswk-swf Chemischer Reaktor (DE-588)4121085-2 gnd rswk-swf Mikroverfahrenstechnik (DE-588)7660041-5 gnd rswk-swf Miniaturisierung (DE-588)4406753-7 gnd rswk-swf Mikroreaktor (DE-588)4786310-9 gnd rswk-swf Chemische Verfahrenstechnik (DE-588)4069941-9 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Mikroreaktor (DE-588)4786310-9 s DE-604 Chemischer Reaktor (DE-588)4121085-2 s Mikrosystemtechnik (DE-588)4221617-5 s Miniaturisierung (DE-588)4406753-7 s Chemische Verfahrenstechnik (DE-588)4069941-9 s Mikroverfahrenstechnik (DE-588)7660041-5 s Reschetilowski, Wladimir 1950- Sonstige (DE-588)1038701295 oth X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4260005&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026255576&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more Mikrosystemtechnik (DE-588)4221617-5 gnd Chemischer Reaktor (DE-588)4121085-2 gnd Mikroverfahrenstechnik (DE-588)7660041-5 gnd Miniaturisierung (DE-588)4406753-7 gnd Mikroreaktor (DE-588)4786310-9 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| subject_GND | (DE-588)4221617-5 (DE-588)4121085-2 (DE-588)7660041-5 (DE-588)4406753-7 (DE-588)4786310-9 (DE-588)4069941-9 (DE-588)4143413-4 |
| title | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more |
| title_auth | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more |
| title_exact_search | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more |
| title_full | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more ed. by Wladimir Reschetilowski |
| title_fullStr | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more ed. by Wladimir Reschetilowski |
| title_full_unstemmed | Microreactors in preparative chemistry practical aspects in bioprocessing, nanotechnology, catalysis and more ed. by Wladimir Reschetilowski |
| title_short | Microreactors in preparative chemistry |
| title_sort | microreactors in preparative chemistry practical aspects in bioprocessing nanotechnology catalysis and more |
| title_sub | practical aspects in bioprocessing, nanotechnology, catalysis and more |
| topic | Mikrosystemtechnik (DE-588)4221617-5 gnd Chemischer Reaktor (DE-588)4121085-2 gnd Mikroverfahrenstechnik (DE-588)7660041-5 gnd Miniaturisierung (DE-588)4406753-7 gnd Mikroreaktor (DE-588)4786310-9 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| topic_facet | Mikrosystemtechnik Chemischer Reaktor Mikroverfahrenstechnik Miniaturisierung Mikroreaktor Chemische Verfahrenstechnik Aufsatzsammlung |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4260005&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026255576&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT reschetilowskiwladimir microreactorsinpreparativechemistrypracticalaspectsinbioprocessingnanotechnologycatalysisandmore |