Minerals at the nanoscale: university textbook
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
London
Eeropean Mineralogical Union [u.a.]
2013
|
| Schriftenreihe: | EMU notes in mineralogy
14 |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XV, 440 S. Ill., graph. Darst. |
| ISBN: | 9780903056342 |
Internformat
MARC
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| 020 | |a 9780903056342 |9 978-0903056-34-2 | ||
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| 245 | 1 | 0 | |a Minerals at the nanoscale |b university textbook |c ed. by F. Nieto |
| 264 | 1 | |a London |b Eeropean Mineralogical Union [u.a.] |c 2013 | |
| 300 | |a XV, 440 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a EMU notes in mineralogy |v 14 | |
| 700 | 1 | |a Nieto Garcia, Fernando |e Sonstige |0 (DE-588)1041258747 |4 oth | |
| 830 | 0 | |a EMU notes in mineralogy |v 14 |w (DE-604)BV014391074 |9 14 | |
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Datensatz im Suchindex
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| adam_text | IMAGE 1
CONTENTS
PREFACE ^ . . .^
CHAPTER 1. INCLUSIONS AND TRACES STUDIED BY TEM-AEM 1
BY CRISTIANO FERRARIS AND GRAEME AUCHTERLONIE 1. INTRODUCTION 1
2. DIFFERENT IMAGING METHODS 3
2.1. IMAGING IN TEM 7
2.1.1. AMPLITUDE CONTRAST IMAGES 8
2.1.2. PHASE-CONTRAST IMAGES 10
2.1.3. STEM AND Z-CONTRAST IMAGES 12
3. ANALYTICAL PROCEDURES AND APPLICATIONS 13
3.1. ENERGY-DISPERSIVE X-RAY (EDX) SPECTROSCOPY 14
3.2. ELECTRON ENERGY LOSS SPECTROSCOPY (EELS) 14
3.3. ENERGY-FIITERED TEM (EFTEM) 18
4. SOME EXAMPLES OF HRTEM-STEM-HAADF-AEM-EELS INVESTIGATIONS 19 4.1.
NANOCLUSTERS WITHIN NOMINALLY STOICHIOMETRIC MINERAL PHASES; THE
EXSOLUTION PHENOMENA 20
4.1.1. SULFIDES AND SULFOSALTS IN ORE DEPOSITS 20
4.1.2. IR-BEARING MTILE EXSOFVED FROM A MANTLE-DERIVED CR-SPINEL 23 4.2.
NANOSCALED INTERGROWTHS AND CO-PRECIPITATES 26
4.2.1. PB-BEARING PRECIPITATES WITHIN PYRITE 26
4.2.2. NANOSIZED GRAPHITE LAYERS INTERGROWN WITHIN PHLOGOPITE 28 4.2.3.
NI-CU RETENTION MECHANISMS IN SHEET SILICATES 28
4.3. NANOSCALED MINERAL AND FLUID INCLUSIONS 31
4.3.1. NANOCRYSTALLINE PEROVSKITE INCLUSIONS IN OLIVINE 31
4.3.2. NANOSIZED MINERAL AND FLUID INCLUSIONS IN DIAMONDS 33 4.4.
NANOSCALED MINERAL REACTIONS 34
4.4.1. SULFIDATION OF LEPIDOCROCITE AND FE-PHASE PRECIPITATION 34 4.4.2.
ELEMENT REDISTRIBUTION VIA DISSOLUTION-PRECIPITATION IN A MONAZITE
ALTERATION PROCESS 36
4.4.3. NANOMETRIC MODULATION IN APATITE 37
5. CONCLUSIONS 39
ACKNOWLEDGMENTS 40
REFERENCES 40
CHAPTER 2. ENERGY DISPERSIVE X-RAY MICROANALYSIS BY TEM APPLIED TO
EXTRATERRESTRIAL MATERIALS 49
BY HUGUES LEROUX 1. INTRODUCTION 49
2. EDX MICROANALYSIS 50
2.1. GENERATION OF X-RAYS FROM THE SPECIMEN 51
2.2. DETECTION CHAIN 52
2.3. SPECTRUM AND QUANTIFICATION PROCEDURE 54
IMAGE 2
2.3.1. IDENTIFICATION OF THE ELEMENTS 54
2.3.2. BACKGROUND SUBTRACTION AND QUANTIFICATION 54
2.3.3. DETERMINATION OF K FACTORS 55
2.3.4. ABSORPTION CORRECTION 56
2.3.5. ACCURACY AND DETECTION LIMITS 57
3. APPLICATION TO EXTRATERRESTRIAL MATERIALS 57
3.1. PYROXENE EXSOLUTION IN A MARTIAN METEORITE 57
3.2. COMPOSITION GRADIENT ACROSS INTERFACES IN A PRIMITIVE CHONDRITE 59
3.3. FINE-GRAINED MATERIAL OF THE WILD 2 COMET (STARDUST MISSION) 60
3.4. ELEMENT LOSS UNDER THE ELECTRON BEAM 63
4. CONCLUSIONS 65
ACKNOWLEDGMENTS 65
REFERENCES 65
CHAPTER 3. CHARACTERIZATION OF DISLOCATIONS AND DEFORMATION PROCESSES BY
TRANSMISSION ELECTRON MICROSCOPY 67
BY PATRICK CORDIER 1. INTRODUCTION 67
2. DISLOCATIONS 68
3. DECORATION AND CHEMICAL ETCHING 71
4. DISLOCATIONS AT THE ATOMIC SCALE 72
4.1. PHASE CONTRAST IN HIGH-RESOLUTION TEM AND Z CONTRAST IN SCANNING
TRANSMISSION ELECTRON MICROSCOPY (STEM) 72
4.1.1. COHERENT IMAGING 72
4.1.2. INCOHERENT IMAGING 73
4.2. APPLICATION TO DISLOCATIONS 73
4.3. FROM THE ATOMIC SCALE TO THE DISPLACEMENT HELD: GEOMETRIC PHASE
ANALYSIS 74
5. CHARACTERIZATION OF DISLOCATIONS BASED ON THEIR DISPLACEMENT FIELD 77
5.1. DIFFRACTION CONTRAST IN CONVENTIONAL TRANSMISSION ELECTRON
MICROSCOPY (CTEM) 78
5.1.1. DISLOCATION IMAGING IN BRIGHT HELD/DARK FIELD 78
5.1.2. WEAK-BEAM DARK-FIELD (WBDF) IMAGES OF DISLOCATIONS 81 5.1.3.
BURGERS VECTOR CHARACTERIZATION BASED ON THE INVISIBILITY CRITERION
...82 5.1.4. THE THICKNESS FRINGES METHOD 84
5.2. STEREOGRAPHIC TECHNIQUES AND TOMOGRAPHY 84
5.3. SCANNING TRANSMISSION ELECTRON MICROSCOPY (STEM) 86
5.4. LARGE ANGLE CONVERGENT BEAM ELECTRON DIFFRACTION (LACBED) AND
RELATED TECHNIQUES 89
5.4.1. LACBED 89
5.4.2. CONVERGENT BEAM IMAGING (CBIM) 92
5.4.3. BEND CONTOURS 93
6. ORIENTATION MAPPING IN THE TEM 94
IMAGE 3
7. CONCLUSION 95
ACKNOWLEDGEMENTS 98
REFERENCES 98
APPENDIX 102
CHAPTER 4, STRUCTURES AND MICROSTRUCTURES OF NON-CLASSICAL PYRIBOLES 109
BY KRASSIMIR N. BOZHITOV 1. INTRODUCTION 109
2. DEFINITIONS AND STRUCTURAL ASPECTS I LL
2.1. PYROXENE TOPOLOGY 111
2.2. MICA TOPOLOGY 113
2.3. PYRIBOLE TOPOLOGY 117
3. BASIC, LONG-RANGE, NON-CLASSICAL PYRIBOLE STRUCTURES 120
3.1. JIMTHOMPSONITE 120
3.2. CLINOJIMTHOMPSONITE 120
3.3. CHESTERITE 120
3.4. CLINOCHESTERITE 121
3.5. PROTO-POLYMORPH OF JIMTHOMPSONITE 121
3.6. PROTO-POLYMORPH OF CHESTERITE 121
3.7. CA ANALOGUE OF CLINOJIMTHOMPSONITE 121
3.8. (21)-CLINOPYRIBOLE 121
3.9. SYNTHETIC NA ANALOGUES OF CLINOJIMTHOMPSONITE 122
3.10. NA-CA ANALOGUE OF CLINOJIMTHOMPSONITE 123
4. TEM IMAGING AND ANALYSIS OF PYRIBOLES 123
4.1.TEM/STEM 124
4.1.1. AMPLITUDE CONTRAST 125
4.1.2. PHASE CONTRAST 126
4.2. ANALYTICAL ELECTRON MICROSCOPY 128
4.3. CHAIN MULTIPLICITY CHARACTERIZATION BY AEM 128
5. NCP OCCURRENCE AND MIERUSTRIICLURES 132
6. SOLID SOLUTION VS. POLYSOMATIC DISORDER IN PYRIBOLES 138
6.2. CHAIN MULTIPLICITY IN AMPHIBOLE SYSTEMS 139
6.2.1. TRETNOLITE-RNAGNESIOCUINMINGTONITE 139
6.2.2. FERRO-ACTINOLITE-GRUNERITE 140
6.2.3. PARGASITE-TREMOLITE-CUMMINGTONITE 141
6.2.4. RICHTERITE-TREMOLITE-CUMMINGTONITE 141
6.2.5. ANTHOPHYLLITE/CUMMINGTONITE- SUENOKE / CLINO-SUCNOITE 142 6.2.6.
ANTHOPHYLLITE/CUMMINGTONITE-GRUNERITE/FERRO-ANTHOPHYLLITE 142 6.2.7.
TREMOLITE-MAGNESIO-HORNBLENDE 143
7. SYNCHESIS OF TRIPLE-CHAIN PYRIBOLES (TCP) 143
8. CONCLUSIONS 146
ACKNOWLEDGEMENTS 147
REFERENCES 147
IMAGE 4
CHAPTER 5. STRUCTURE AND MICRESTRUCTURE OF SERPENTINE MINERALS 153
BY MAKCKLJ.O MELLIIII 1. INTRODUCTION 153
2. THE DAWN OF ELECTRON OPTICS OF SERPENTINE: FROM RUSKA TO YADA 154 3.
GEOLOGICAL CONSTRAINTS 156
4. STRUCTURAL HIERARCHY 158
5. POLYTYPISM 160
6. ANTIGORITE POLYSOMATISM 161
7. POLYGONAL SERPENTINE 163
8. POLYHEDRAL SERPENTINE 164
9. FIVEFOLD SYMMETRY IN SERPENTINE 166
10. ASSOCIATED AND INTERLEAVED SERPENTINES 166
11. SERPENTINE REACTIONS 168
12. ALTERNATIVE METHODS FOR STRUCTURAL ANALYSIS 169
14. NANOTUBES AND NANOWIRES 170
15. CONCLUSIONS 171
ACKNOWLEDGEMENTS 171
REFERENCES 171
CHAPTER 6. CLAYS IN LOW-TEMPERATURE ENVIRONMENTS 181
BY BLANCA BAULUZ 1. INTRODUCTION 181
2. PHYLLOSILICATE STRUCTURE 182
3. PREPARATION OF CLAY SAMPLES FORTEM STUDY 184
4. INFORMATION PROVIDED BY TEM 188
5. CLAYS UNDER TEM 189
5.1. KAOLIN MINERALS UNDER TEM 189
5.2. SMECTITE, ILLITE-SMECTITE AND ILLITE PHASES UNDER TEM 193
5.3. SMECTITE, CHLORITE-SMECTITE AND CHLORITE PHASES UNDER TEM 200 5.4.
GLAUCONITIC MINERALS UNDER TEM 202
5.5. SEPIOLITE AND PALYGORSKITE UNDER TEM 205
6. CONCLUSIONS 207
ACKNOWLEDGMENTS 208
REFERENCES 209
CHAPTER 7. THE ROLE OF TRANSMISSION ELECTRON MICROSCOPY IN THE STUDY OF
MICAS AND RELATED MINERALS IN SELECTED METAMORPHIC ENVIRONMENTS 217
BY KENNETH J.T. LIVI AND ISABEL ABAD 1. INTRODUCTION 217
1.1. MICA STRUCTURE AND COMPOSITIONAL RANGES 218
1.2. SAMPLE PREPARATION 218
1.3. EDX OF PHYLLOSILKATES 219
IMAGE 5
1.3.1. VALIDITY OF TEM ANALYSES OF LOW-GRADE METAMORPHIC;
PHYLLOSILICATES 220
2. SHEET SILICATES IN LOW-GRADE METAMORPHIC CLASTIC SEDIMENTS 220
2.1. HRTEM AND THE KIIBLER INDEX 222
2.2. THE B PARAMETER OF WHITE MICA 224
2.3. CHLORITE AND MICA POLYTYPES 225
2.4. TEXTURAL EVOLUTION OF PHYLLOSILICATES WITH METAMORPHIC GRADE 227
2.5. CRYSTAL CHEMICAL EVOLUTION 229
2.5.1. DIOCTAHEDRAL MICAS - INTERLAYER CHANGES 229
2.5.2. DIOCTAHEDRAL MICAS - OCTAHEDRAL CHANGES 231
2.5.3. CHLORITES 234
2.5.4. KAOLIN MINERALS 236
2.6. INDEX MINERALS 236
2.7. RETROGRADE PHYLLOSILICATES 237
3. METAMORPHISM OF MICAS AT HIGHER METAMORPHIC GRADES 237
3.1. EXSOLUTION IN MICAS 238
3.1.1. EXSOLUTION IN MICAS INVOLVING THE OCTAHEDRAL CATIONS 238 3.1.2.
UNMIXING OF INTERLAYER CATIONS 241
3.2. MINERAL INTERGROWTHS IN MICAS 241
3.2.1. CHLORITE AFTER BIOTITE (N ON -WEATHERING ENVIRONMENTS) 244 3.2.2.
ALTERATION OF PHLOGOPITE TO SERPENTINE 245
3.3. INTERGROWTHS OF MICAS WITH OTHER MINERALS 246
3.3.1. NATIVE COPPER IN BIOTITE 246
3.3.2. SAGENITIC BIOTITE 246
4. POLYTYPES AND STACKING FAULTS 247
5. DEFORMATION OF MICAS 247
6. THE FUTURE 251
ACKNOWLEDGEMENTS 251
REFERENCES 252
CHAPTER 8. NON-STOICHIOMETRY, DETECTS AND SUPERSTRUCTURES IN SULFIDE AND
OXIDE MINERALS 261
BY FALKO LANGENHORST, DENNIS HARRIES AND KILIAN POLL OK 1. INTRODUCTION
261
2. PYRRHOTITE (FEI _^S) - A FAMILY OF NON-STOICHIOMETRIC IRON
MONOSULFIDES 262 2.1 TYPES OF IRON MONOSULFIDES 262
2.2 MODULAR ARCHITECTURE VS. MODULATION OF PYRRHOTITES 263
2.3. CATION VACANCIES AND SUPERSTRUCTURES IN PYRRHOTITES 265
2.4 THERMOCHEMICAL BACKGROUND OF CATION VACANCY ORDERING IN PYRRHOTITES
271
2.5 MAGNETIC PROPERTIES OF PYRRHOTITES 273
3. NON-STOICHIOMETRY IN THE WIISTITE ( F E ^ O) - PERICLASE (MGO) SYSTEM
274 3.1. NON-STOICHIOMETRY AND POINT DEFECTS IN WIISTITE ( F E ^ O) 274
IMAGE 6
3.2. DEFECT CLUSTERS AND INCOMMENSURATE STRUCTURE OF WIISTITE ( F E ^ O)
275
3.3. POINT DEFECTS IN LOWER-MANTLE FERROPERIELASE 276
4. CRYSTALLOGRAPHIC SHEAR PLANES AND SUPERSTRUCTURES IN THE RUTILE (TIO
2 )-TISTARITE (TI 2 O 3 ) SERIES 277
4.1. OXYGEN DEFICIENCY AND CRYSTAL LOGRAPHIC SHEAR PLANES IN RUTILE 277
4.2. SUPERSTRUCTURES OF THE MAGNEII PHASES 277
5. NON-STOICHIOMETRY IN PEROVSKITE SYSTEMS 279
5.1. STRUCTURE, CATION SUBSTITUTIONS AND VACANCIES IN PEROVSKITE 279
5.2. OXYGEN VACANCY ORDERING AND SUPERSTRUCTURES IN THE CATIO3-CAFEO2.S
MODEL SYSTEM 281
5.3. CRYSTAL CHEMISTRY AND CATION SUBSTITUTIONS IN SILICATE PEROVSKITE
285 6. CONCLUDING REMARKS 289
ACKNOWLEDGEMENTS 290
REFERENCES 290
CHAPTER 9. IRON, MANGANESE AND ALUMINIUM OXIDES AND OXY HYDROXIDES 297
BY VIDAL BAR RON AND JOSE TORRENT 1. INTRODUCTION 297
2. IRON OXIDES 300
2.1. CRYSTAL STRUCTURE, MORPHOLOGY AND SIZE 300
2.2. FORMATION OF IRON OXIDES: PATHWAYS AND EFFECT OF TEMPERATURE, PH,
EH AND FOREIGN COMPOUNDS 302
2.3. OCCURRENCE IN NATURAL ENVIRONMENTS 305
2.3.1. LITHOSPHERE AND PEDOSPHERE 305
2.3.2. HYDROSPHERE 307
2.3.3. ATMOSPHERE 308
2.3.4. BIOSPHERE 309
2.4. DOES SIZE MATTER IN FE OXIDES? 311
2.4.1. COLOUR 311
2.4.2. MAGNETISM 312
2.4.3. REACTIVITY (STABILITY, SOLUBILITY, ION ADSORPTION) 313
2.5. SELECTED OLD AND NEW APPLICATIONS OF IRON OXIDES 315
3. MANGANESE OXIDES 316
3.1. NANOSCALE NATURE 316
3.1.1. TECTOMANGANATES (TUNNEL MN OXIDES) 316
3.1.2. PHYLLOMANGANATES 318
3.2. FORMATION AND OCCURRENCE 319
3.3. ENVIRONMENTAL SIGNIFICANCE 321
4. ALUMINIUM OXIDES 323
4.1. NANOSCALE NATURE AND OCCURRENCE 323
4.2. ENVIRONMENTAL SIGNIFICANCE 326
ACKNOWLEDGMENTS 326
REFERENCES 327
IMAGE 7
CHAPTER 10. CARBONATES: AN OVERVIEW OF RECENT TEM RESEARCH 337
BY CARLOS RODRIGUEZ-NAVARRO AND ENCAKNACION RUIZ-AGUDO 1. INTRODUCTION
337
2. CARBONATE MINERALS: OCCURRENCE AND IMPORTANCE 338
}. TLI.VL STUDIES OF CARBONATE MICRO STRUCTURES 341
3.1. GROWTH MICROSTRUCTURES 342
3.2. TRANSFORMATION AND REPLACEMENT MICROSTRUCTURES 346
3.3. DEFORMATION MICROSTRUCTURES 347
4. CALCIUM CARBONATE NUCLEATION AND GROWTH: NON-CLASSICAL VS. CLASSICAL
CRYSTALLIZATION 349
4.1. PHASES AND PHASE TRANSFORMATIONS IN THE CACO 3 -H 2 O SYSTEM 349
4.2. THE PRE-NUCLEATION STAGE 350
4.3. ORIENTED ATTACHMENT AND MESOCRYSTAL FORMATION 351
4.4. BIOMIMETIC SYNTHESIS OF CALCIUM CARBONATE 353
5. MICROSTRUCTURES IN BIOGENIC CARBONATES 354
5.1. BIOGENIC CALCITE 354
5.2. BIOGENIC ARAGONITE 358
5.3. BIOGENIC VATERITE 360
5.4. BIOGENIC CARBONATES AND NANOBACTERIA 361
6. TRANSFORMATION REACTIONS IN THE TEM 361
6.1. THE THERMAL DECOMPOSITION OF CARBONATES 363
6.2. ORIGIN OF EUHEDRAL MAGNETITE CRYSTALS IN ALH84001 MARTIAN METEORITE
366
7. CONCLUDING REMARKS 368
ACKNOWLEDGEMENTS 369
REFERENCES 369
CHAPTER 11. BIOMINERALS AT THE NANOSCAIE: TRANSMISSION ELECTRON
MICROSCOPY METHODS FOR STUDYING THE SPECIAL PROPERTIES OF BIOMINERALS
377 BY MIHALY POSFAI, TAKESHI KASAMA AND RAFAL E. DUNIN-BORKOWSKI 1.
INTRODUCTION 377
2. PRIMARY BIOMINERAL-FORMING PROCESSES AND BIOMINERAL GROUPS 379 3.
SPECIAL PROPERTIES OF BIOMINERALS AND TEM TECHNIQUES FOR THEIR STUDY 383
3.1. PARTICLE SIZE 385
3.2 CRYSTAL MORPHOLOGY 389
3.3. CHEMICAL COMPOSITION 393
3.4. CRYSTAL STRUCTURE 399
3.5. CRYSTALLOGRAPHIC ORIENTATION 405
3.6. MAGNETIC PROPERTIES 408
4. THE MINERAL-ORGANIC INTERFACE - ISSUES WITH SAMPLE PREPARATION AND
IMAGING 413
4.1. SPECIMEN PREPARATION FOR TTIM 414
4.2. ENHANCEMENT OF IMAGE CONTRAST AND REDUCTION OF RADIATION DAMAGE 418
IMAGE 8
5. COMBINATION OF TEM WITH OTHER NANOSCALE TECHNIQUES FOR THE STUDY
OF BIOMINERALS 420
5.1. CORRELATIVE TEM-OPTICAL MICROSCOPY AND ELECTRON BACKSCATTER
DIFFRACTION 421
5.2 TEM COMBINED WITH X-RAY-BASED TECHNIQUES FOR COMPOSITIONAL ANALYSIS
422
5.3. ADDITIONAL TECHNIQUES FOR THE NANO-SCALE CHARACTERIZATION OF
COMPOSITIONS, STRUCTURES AND PHYSICAL PROPERTIES OF BIOMINERALS 423 6.
CONCLUDING THOUGHTS 425
ACKNOWLEDGEMENTS 425
REFERENCES 426
INDEX 437
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| series2 | EMU notes in mineralogy |
| spelling | Minerals at the nanoscale university textbook ed. by F. Nieto London Eeropean Mineralogical Union [u.a.] 2013 XV, 440 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier EMU notes in mineralogy 14 Nieto Garcia, Fernando Sonstige (DE-588)1041258747 oth EMU notes in mineralogy 14 (DE-604)BV014391074 14 SWB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026128555&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Minerals at the nanoscale university textbook EMU notes in mineralogy |
| title | Minerals at the nanoscale university textbook |
| title_auth | Minerals at the nanoscale university textbook |
| title_exact_search | Minerals at the nanoscale university textbook |
| title_full | Minerals at the nanoscale university textbook ed. by F. Nieto |
| title_fullStr | Minerals at the nanoscale university textbook ed. by F. Nieto |
| title_full_unstemmed | Minerals at the nanoscale university textbook ed. by F. Nieto |
| title_short | Minerals at the nanoscale |
| title_sort | minerals at the nanoscale university textbook |
| title_sub | university textbook |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026128555&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV014391074 |
| work_keys_str_mv | AT nietogarciafernando mineralsatthenanoscaleuniversitytextbook |