Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany):
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2013
|
| Schlagworte: | |
| Online-Zugang: | Volltext Inhaltsverzeichnis |
| Beschreibung: | Nebentitel: Screening, quantitative Analyse und Toxikologie organischer Verbindungen in Sedimenten und Schwebstoffen der Saar und des Rheins (Deutschland) |
| Beschreibung: | XXVII, 210, XLIII S. Ill., graph. Darst. |
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Datensatz im Suchindex
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| adam_text | IMAGE 1
TABLE OF CONTENTS
1 INTRODUCTION 1
1.1 OBJECTIVES 1
1.2 SYNOPSIS OF THE REMAINING CHAPTERS AND SECTIONS 1
2 SCREENING AND IDENTIFICATION OF ORGANIC COMPOUNDS IN SEDIMENTS
AND SUSPENDED PARTICULATE MATTER OF THE SAAR AND THE RHINE 8
2.1 INTRODUCTION 8
2.2 MATERIALS UND METHODS 10
2.2.1 CHEMICALS AND SOLVENTS 10
2.2.2 SAMPLING DEVICES 10
2.2.3 SAMPLING SITES AND SAMPLES 13
2.2.4 SAMPLE EXTRACTION AND ANALYSIS 13
2.2.5 RADIOMETRIC DATING OF SEDIMENT CORES 16
2.2.6 TOTAL ORGANIC CARBON CONTENT 16
2.2.7 DATA ANALYSIS 17
2.3 RESULTS AND DISCUSSION 20
2.3.1 RADIOMETRIC DATING OF SEDIMENT CORES . 20
2.3.2 TOTAL ORGANIC CARBON IN SEDIMENTS AND SUSPENDED PARTICULATE MATTER
21
2.3.3 PAHS, PCBS AND HCB IN SEDIMENTS 22
2.3.4 PAHS IN SUSPENDED PARTICULATE MATTER 23
2.3.5 SOURCE APPOINTMENT OF PAHS 24
2.3.6 PCBS IN SUSPENDED PARTICULATE MATTER 27
2.3.7 HCB IN SUSPENDED PARTICULATE MATTER 28
2.3.8 SPATIOTEMPORAL ASSESSMENT OF SUSPENDED PARTICULATE MATTER 29
2.3.9 IDENTIFICATION OF SUSPECT AND NONTARGET COMPOUNDS 32
2.4 CONCLUSIONS 54
2.5 ACKNOWLEDGEMENTS 55
3 COMPARISON OF DIFFERENT EXHAUSTIVE AND ONE BIOMIMETIC
EXTRACTION TECHNIQUES FOR CHEMICAL AND BIOLOGICAL ANALYSIS OF
POLYCYCLIC AROMATIC COMPOUNDS IN RIVER SEDIMENTS 58
3.1 INTRODUCTION 58
3.2 MATERIALS AND METHODS 62
3.2.1 CHEMICALS 62
3.2.2 STUDY AREA AND SAMPLING 62
3.2.3 SAMPLE STORAGE AND PREPARATION 63
3.2.4 GRAIN SIZE DISTRIBUTION, TOTAL ORGANIC CARBON AND BLACK CARBON 63
HTTP://D-NB.INFO/1042512620
IMAGE 2
3.2.5 EXTRACTION METHODS 64
3.2.6 EXTRACTS PREPARATION 65
3.2.7 SILICA GEL FRACTIONATION 66
3.2.8 GAS CHROMATOGRAPHY - MASS SPECTROMETRY 66
3.2.9 TOXICITY TESTING 67
3.2.10 DATA ANALYSIS 68
3.3 RESULTS AND DISCUSSION 70
3.3.1 GRAIN SIZE DISTRIBUTION 70
3.3.2 EXTRACTABILITY OF PAHS 70
3.3.3 COMPOUND SPECIFIC EXTRACTABILITY OF PAH 73
3.3.4 ROLE OF ORGANIC AND BLACK CARBON ON THE EXTRACTABILITY 76
3.3.5 CYTOTOXIC POTENCY AND EROD INDUCTION OF THE PRIMARY EXTRACTS 76
3.3.6 EFFECT-CONFIRMATION USING TOXICITY EQUIVALENTS AND ARTIFICIAL
MIXTURES 78
3.4 IMPLICATIONS FOR THE RISK ASSESSMENT OF SEDIMENTS 81
3.5 CONCLUSIONS 82
3.6 ACKNOWLEDGMENTS 83
4 EXCURSUS: ON THE COMPARABILITY OF PROCEDURES FOR SEDIMENT
EXTRACTION IN ENVIRONMENTAL ASSESSMENT 84
4.1 INTRODUCTION 84
4.2 MATERIALS AND METHODS 86
4.2.1 STUDY AREA, SAMPLING AND SAMPLE PREPARATION 86
4.2.2 CHEMICALS AND SOLVENTS 87
4.2.3 EXTRACTION AND CLEAN-UP 87
4.2.4 PROCESS CONTROLS 91
4.2.5 BIOASSAYS 91
4.2.6 INSTRUMENTAL ANALYSIS 93
4.2.7 GRAPHICAL EVALUATION AND STATISTICAL ANALYSIS 94
4.2.8 ARTIFICIAL MIXTURES AND CALCULATION OF BIOLOGICAL TOXICITY
EQUIVALENTS FOR EROD DATA 95
4.3 RESULTS 96
4.3.1 CHEMICAL ANALYSIS 96
4.3.2 BIOLOGICAL ANALYSIS 100
4.4 DISCUSSION 103
4.4.1 RANKING ACCORDING EXTRACTION EFFICIENCY 103
4.4.2 RANKING ACCORDING REPEATABILITY 105
4.4.3 RELATIONSHIP BETWEEN EXTRACTION EFFICIENCY AS WELL AS SEDIMENT AND
COMPOUND SPECIFIC
PROPERTIES 106
4.4.4 RELATIONSHIP BETWEEN EXTRACTION EFFICIENCY AND EFFECT POTENTIAL
108
4.4.5 CONFIRMATION OF EROD-INDUCTION USING ARTIFICIAL MIXTURES 110
IMAGE 3
4.5 CONCLUSIONS 112
4.6 ACKNOWLEDGEMENTS 112
5 RISK ASSESSMENT OF RIVER SUSPENDED PARTICULATE MATTER AND
FLOODPLAIN SOILS IN THE RHINE CATCHMENT USING CHEMICAL ANALYSIS AND
IN VITRO BIOASSAYS 114
5.1 INTRODUCTION 114
5.2 MATERIAL AND METHODS 116
5.2.1 CHEMICALS 116
5.2.2 SAMPLING SITES, COLLECTION OF SOIL AND SPM SAMPLES AND SAMPLE
PREPARATION 116
5.2.3 GRAIN SIZE DISTRIBUTION AND TOTAL ORGANIC CARBON 119
5.2.4 ANALYSIS OF TRACE ELEMENTS 119
5.2.5 SOXHLET EXTRACTION AND SILICA GEL FRACTIONATION 119
5.2.6 INSTRUMENTAL ANALYSIS OF ORGANIC COMPOUNDS 120
5.2.7 DIOXINS AND FURANS 121
5.2.8 BIOASSAYS 121
5.2.9 DATA ANALYSIS 123
5.3 RESULTS AND DISCUSSION 124
5.3.1 GRAIN SIZE DISTRIBUTION AND CONTENTS OF TOTAL ORGANIC CARBON 124
5.3.2 TRACE ELEMENTS IN WHOLE SAMPLES 125
5.3.3 ORGANIC COMPOUNDS IN CRUDE EXTRACTS 128
5.3.4 BIOANALYSIS OF CRUDE EXTRACTS AND WHOLE SAMPLES 131
5.3.5 RISK ASSESSMENT OF HAZARD POTENTIALS 134
5.4 CONCLUSIONS 140
5.5 ACKNOWLEDGEMENTS 140
6 IMPACT OF CONTAMINANTS BOUND TO SUSPENDED PARTICULATE MATTER
IN THE CONTEXT OF FLOOD EVENTS 141
6.1 INTRODUCTION 141
6.2 MATERIALS AND METHODS 143
6.2.1 CHEMICALS USED 143
6.2.2 SPM SAMPLING 144
6.2.3 PREPARATION OF CRUDE EXTRACTS 145
6.2.4 CHEMICAL ANALYSIS OF HCB AND PCBS 146
6.2.5 GC-MS ANALYSIS FOR PAHS T 147
6.2.6 EROD INDUCTION ASSAY 147
6.2.7 AMES FLUCTUATION ASSAY 149
6.3 RESULTS 150
6.3.1 SPM SAMPLED IN 2006 150
IMAGE 4
6.3.2 SPM SAMPLED IN THE CONTEXT OF THE FLOOD EVENT IN AUGUST 2007 150
6.4. IDENTIFICATION OF EFFECTIVE FRACTIONS..; 152
6.5 DISCUSSION 155
6.5.1 CHEMICAL LOADS OF CRUDE EXTRACTS 155
6.5.2 BIOLOGICAL HAZARD POTENTIAL IN CRUDE EXTRACTS 156
6.5.3 AHR-AGONISTS AND MUTAGENIC POTENTIAL IN FRACTIONS 156
6.6 CONCLUSIONS 158
6.7 ACKNOWLEDGEMENTS 159
7 INVESTIGATION ON SOIL CONTAMINATION AT RECENTLY INUNDATED AND
NONINUNDATED SITES 160
7.1 INTRODUCTION 160
7.2 MATERIALS AND METHODS 162
7.2.1 CHEMICALS USED 162
7.2.2 DESCRIPTION OF METHODS 162
7.2.3 SOIL SAMPLING 162
7.2.4 SOIL EXTRACTION FOR ASSESSMENT OF TOTAL SAMPLES 163
7.2.5 SOIL EXTRACTION AND CLEANUP FOR FRACTIONATION 163
7.2.6 AUTOMATED FRACTIONATION PROCEDURE 164
7.2.7 GC-MS ANALYSIS OF FRACTIONS 164
7.2.8 EROD INDUCTION ASSAY 164
7.2.9 BIO-TEQ VALUES 165
7.2.10 AMES FLUCTUATION ASSAY 165
7.3 RESULTS 167
7.3.1 AHR-MEDIATED ACTIVITIES AND IDENTIFIED COMPOUNDS 167
7.3.2 EROD-INDUCING POTENTIAL BY SOIL FRACTIONS 167
7.3.3 MUTAGENIC POTENTIAL OF INDIVIDUAL FRACTIONS 169
7.4 DISCUSSION 170
7.4.1 CHEMICAL CONTAMINATION OF CRUDE EXTRACTS 170
7.4.2 BIOLOGICAL HAZARD POTENTIALS BY CRUDE EXTRACTS 172
7.4.3 IDENTIFICATION OF ACTIVE FRACTIONS 173
7.4.4 REGULATORY ASPECTS 175
7.5 CONCLUSIONS 176
7.6 ACKNOWLEDGMENTS 177
8 REFERENCES 178
9 ACKNOWLEDGEMENTS I
10 SCIENTIFIC DISSEMINATION II
11 APPENDIX VIII
|
| any_adam_object | 1 |
| author | Schulze, Tobias 1970- |
| author_GND | (DE-588)1034402900 |
| author_facet | Schulze, Tobias 1970- |
| author_role | aut |
| author_sort | Schulze, Tobias 1970- |
| author_variant | t s ts |
| building | Verbundindex |
| bvnumber | BV040987838 |
| collection | ebook |
| ctrlnum | (OCoLC)863655749 (DE-599)BVBBV040987838 |
| dewey-full | 551.35409434 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 551 - Geology, hydrology, meteorology |
| dewey-raw | 551.35409434 |
| dewey-search | 551.35409434 |
| dewey-sort | 3551.35409434 |
| dewey-tens | 550 - Earth sciences |
| discipline | Geologie / Paläontologie |
| format | Thesis Book |
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| id | DE-604.BV040987838 |
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| indexdate | 2024-07-10T00:36:53Z |
| institution | BVB |
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| publishDateSort | 2013 |
| record_format | marc |
| spelling | Schulze, Tobias 1970- Verfasser (DE-588)1034402900 aut Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) vorgelegt von Tobias Schulze Screening, quantitative Analyse und Toxikologie organischer Verbindungen in Sedimenten und Schwebstoffen der Saar und des Rheins (Deutschland) 2013 XXVII, 210, XLIII S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Nebentitel: Screening, quantitative Analyse und Toxikologie organischer Verbindungen in Sedimenten und Schwebstoffen der Saar und des Rheins (Deutschland) Berlin, Freie Univ., Diss., 2013 Aquatisches Sediment (DE-588)4129652-7 gnd rswk-swf Screening (DE-588)4054045-5 gnd rswk-swf Umwelttoxikologie (DE-588)4121813-9 gnd rswk-swf Schwebstoff (DE-588)4053818-7 gnd rswk-swf Organische Verbindungen (DE-588)4043816-8 gnd rswk-swf Flusssediment (DE-588)4130033-6 gnd rswk-swf Analyse (DE-588)4122795-5 gnd rswk-swf Rhein (DE-588)4049739-2 gnd rswk-swf Saar (DE-588)4051095-5 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Rhein (DE-588)4049739-2 g Flusssediment (DE-588)4130033-6 s Organische Verbindungen (DE-588)4043816-8 s Umwelttoxikologie (DE-588)4121813-9 s Screening (DE-588)4054045-5 s DE-604 Saar (DE-588)4051095-5 g Aquatisches Sediment (DE-588)4129652-7 s Schwebstoff (DE-588)4053818-7 s Analyse (DE-588)4122795-5 s Erscheint auch als Online-Ausgabe urn:nbn:de:kobv:188-fudissthesis000000094124-8 http://www.diss.fu-berlin.de/diss/receive/FUDISS_thesis_000000094124 kostenfrei Volltext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025965691&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Schulze, Tobias 1970- Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) Aquatisches Sediment (DE-588)4129652-7 gnd Screening (DE-588)4054045-5 gnd Umwelttoxikologie (DE-588)4121813-9 gnd Schwebstoff (DE-588)4053818-7 gnd Organische Verbindungen (DE-588)4043816-8 gnd Flusssediment (DE-588)4130033-6 gnd Analyse (DE-588)4122795-5 gnd |
| subject_GND | (DE-588)4129652-7 (DE-588)4054045-5 (DE-588)4121813-9 (DE-588)4053818-7 (DE-588)4043816-8 (DE-588)4130033-6 (DE-588)4122795-5 (DE-588)4049739-2 (DE-588)4051095-5 (DE-588)4113937-9 |
| title | Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) |
| title_alt | Screening, quantitative Analyse und Toxikologie organischer Verbindungen in Sedimenten und Schwebstoffen der Saar und des Rheins (Deutschland) |
| title_auth | Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) |
| title_exact_search | Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) |
| title_full | Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) vorgelegt von Tobias Schulze |
| title_fullStr | Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) vorgelegt von Tobias Schulze |
| title_full_unstemmed | Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) vorgelegt von Tobias Schulze |
| title_short | Screening, quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the Saar and the Rhine (Germany) |
| title_sort | screening quantitative analysis and toxicology of organic compounds in sediments and suspended particulate matter of the saar and the rhine germany |
| topic | Aquatisches Sediment (DE-588)4129652-7 gnd Screening (DE-588)4054045-5 gnd Umwelttoxikologie (DE-588)4121813-9 gnd Schwebstoff (DE-588)4053818-7 gnd Organische Verbindungen (DE-588)4043816-8 gnd Flusssediment (DE-588)4130033-6 gnd Analyse (DE-588)4122795-5 gnd |
| topic_facet | Aquatisches Sediment Screening Umwelttoxikologie Schwebstoff Organische Verbindungen Flusssediment Analyse Rhein Saar Hochschulschrift |
| url | http://www.diss.fu-berlin.de/diss/receive/FUDISS_thesis_000000094124 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025965691&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT schulzetobias screeningquantitativeanalysisandtoxicologyoforganiccompoundsinsedimentsandsuspendedparticulatematterofthesaarandtherhinegermany AT schulzetobias screeningquantitativeanalyseundtoxikologieorganischerverbindungeninsedimentenundschwebstoffendersaarunddesrheinsdeutschland |