Ordered mesoporous materials:
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| Main Authors: | , , |
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| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH
2013
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| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XVII, 522 S. Ill., graph. Darst. |
| ISBN: | 9783527326358 3527326359 |
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MARC
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| 245 | 1 | 0 | |a Ordered mesoporous materials |c Dongyuan Zhao, Ying Wan, and Wuzong Zhou |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2013 | |
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Record in the Search Index
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|---|---|
| adam_text |
IMAGE 1
CONTENTS
PREFACE X I
ABBREVIATIONS X I I I
1 INTRODUCTION 1
REFERENCES 4
2 SYNTHESIS APPROACH O F MESOPOROUS MOLECULAR SIEVES 5 2.1 SYNTHESIS 5
2.2 HYDROTHERMAL SYNTHESIS 12
2.2.1 SURFACTANT 12
2.2.2 INORGANIC PRECURSOR 15
2.2.3 SYNTHESIS TEMPERATURE 15 2.2.4 SYNTHETIC MEDIA 19
2.2.5 HYDROTHERMAL TREATMENT 21 2.2.6 FORMATION RATE 23
2.2.7 SEPARATION AND DRYING 23
2.3 REMOVAL O F TEMPLATE 2 4
2.3.1 CALCINATION 2 4
2.3.2 EXTRACTION 25
2.3.3 SUPERCRITICAL FLUID EXTRACTION 25 2.3.4 MICROWAVE IRRADIATION 26
2.3.5 ULTRAVIOLET IRRADIATION 2 7 2.3.6 MICROWAVE DIGESTION 2 8
2.3.7 OXIDATION O F AMMONIUM PERCHLORATE 29 2.4 BASIC SYNTHESIS 3 0
2.5 ACIDIC SYNTHESIS 3 0
2.6 NONAQUEOUS SYNTHESES 3 3
2.7 POSTSYNTHESIS TREATMENT 3 7
2.7.1 HYDROTHERMAL TREATMENT 3 7 2.7.2 SECONDARY SYNTHESIS 3 8
2.7.3 RECRYSTALLIZATION 3 8
2.8 STABILITY O F MESOPOROUS MATERIALS 39
HTTP://D-NB.INFO/1024048144
IMAGE 2
V I | CONTENTS
2.8.1 THERMAL STABILITY 39
2.8.2 HYDROTHERMAL STABILITY 41 2.8.3 MECHANICAL STABILITY 4 4
2.9 PORE-SIZE CONTROL 4 4
REFERENCES 4 8
3 MECHANISMS FOR FORMATION O F MESOPOROUS MATERIALS 55 3.1 INTRODUCTION
55
3.2 SYNTHESIS PATHWAYS 66
3.3 MESOPHASE TAILORING 73
3.3.1 MICELLAR MESOSTRUCTURE 73 3.3.2 CRITICAL MICELLE CONCENTRATION 76
3.3.3 THE PACKING PARAMETER 76
3.3.4 THE HYDROPHILIC/HYDROPHOBIC VOLUME RATIO 79 3.3.5 SURFACTANT PHASE
DIAGRAM 8 2
3.3.6 "ACID-BASE" ROUTE 8 4
3.4 HARD-TEMPLATING APPROACH 91
3.4.1 PRECURSOR 92
3.4.1.1 IMPROVING VOLUME CONVERSION 94 3.4.1.2 IMPROVING THE INTERACTION
BETWEEN TEMPLATE AND PRECURSOR 97 3.4.1.3 ENHANCING THE INTERACTION
BETWEEN PRECURSORS THEMSELVES 98 3.4.2 CONVERSION O F PRECURSORS 100
3.4.3 THE INFLUENCE O F THE TEMPLATE STRUCTURE 102
3.4.3.1 TEMPLATES WITH 2D CHANNELED PORES 103 3.4.3.2 TEMPLATES WITH
CAGE-LIKE PORES 104 3.4.3.3 TEMPLATES WITH 3D HELIX CHANNELS 104 3.4.4
REPLICATED MESOPOROUS CARBON AS A HARD TEMPLATE 107
REFERENCES 109
4 STRUCTURAL CHARACTERIZATION METHODS 4.1 XRD 117
4.1.1 BASIC PRINCIPLES O F XRD 118 4.1.2 XRD MEASUREMENT 119
4.1.3 XRD PATTERN ANALYSIS 120 4.1.4 SAXS 122
4.2 ELECTRON MICROSCOPY 123
4.2.1 TEM 125
4.2.2 SAED 129
4.2.3 SEM 130
4.2.4 EDX 133
4.2.5 STEM 135
4.3 NMR 136
4.4 PHYSICAL SORPTION 138
4.4.1 BASIC PRINCIPLES 138
4.4.2 PORE-SIZE CALCULATION 141
IMAGE 3
CONTENTS | V I I
4.4.3 WINDOW-SIZE CALCULATION FOR CAVITY-LIKE PORES 144
4.4.4 DETECTION O F MICROPORES AND MESOPORES 147 4.4.5 OTHER PROBES 148
REFERENCES 149
5 REPRESENTATIVE MESOPOROUS SILICA MOLECULAR SIEVES 153
5.1 D MESOSTRUCTURES 153
5.1.1 MCM-41 153
5.1.2 SBA-15 161
5.1.3 OTHER 2D PHASES 166
5.1.3.1 FSM-16 AND FSM-10 166 5.1.3.2 KSW-2 168
5.1.3.3 SBA-3 168
5.1.3.4 SBA-8 170
5.1.3.5 CMI-1 170
5.1.3.6 AMS-3 171
5.2 3D HEXAGONAL PHASES 171
5.2.1 SBA-2 171
5.2.2 SBA-12 176
5.2.3 IBN-9 178
5.3 CUBIC PHASES 181
5.3.1 MCM-48, FDU-5 AND KIT-6 181 5.3.2 SBA-1 AND SBA-6 190
5.3.3 SBA-16 192
5.3.4 FDU-1 195
5.3.5 FDU-2 196
5.3.6 FDU-12 AND KIT-5 198
5.3.6.1 FDU-12 198
5.3.7 SBA-11 203
5.3.8 AMS-8 AND AMS-10 205 5.4 DISORDERED MESOSTRUCTURES 207
5.4.1 HMS AND MSU 210
5.4.2 KIT-1 213
5.4.3 TUD-1 213
REFERENCES 2 1 5
6 DOPING IN MESOPOROUS MOLECULAR SIEVES 219
6.1 ALUMINUM DOPING 219
6.2 BORON DOPING 224
6.3 GALLIUM AND INDIUM DOPING 226
6.4 GERMANIUM AND TIN DOPING 227
6.5 TRANSITION-METAL DOPING 228
6.5.1 TITANIUM AND ZIRCONIUM DOPING 229 6.5.2 VANADIUM AND NIOBIUM
DOPING 231 6.5.3 CHROMIUM AND MOLYBDENUM DOPING 2 3 2
IMAGE 4
V I I I | CONTENTS
6.5.4 MANGANESE DOPING 233
6.5.5 IRON AND RUTHENIUM DOPING 234
6.5.6 COBALT DOPING 236
6.5.7 COPPER AND ZINC DOPING 237
6.5.8 HYBRID METAL DOPING 238
REFERENCES 239
7 MORPHOLOGY CONTROL 243
7.1 THE METHODS AND TECHNIQUES 243
7.2 TYPICAL MORPHOLOGIES 244
7.2.1 FIBERS AND RODS 244
7.2.2 THIN FILMS 254
7.2.3 MONOLITHS 2 6 0
7.2.4 SPHERES 266
7.2.5 SINGLE CRYSTALS 2 7 0
7.3 MAGNETICALLY RESPONSIVE ORDERED MESOPOROUS MATERIALS 273
7.3.1 MAGNETIC NANOMATERIALS AND MESOPOROUS MATERIALS 273 7.3.2
SYNTHESIS O F MAGNETIC MESOPOROUS MATERIALS 274 7.3.3 SOL-GEL COATING
APPROACH 274
7.3.4 POSTLOADING APPROACH 283 7.3.5 NANOCASTING SYNTHESIS 286
REFERENCES 287
8 MESOPOROUS NONSILICA MATERIALS 293
8.1 MESOPOROUS CARBON 293
8.1.1 NANOCASTING 294
8.1.1.1 MORPHOLOGY CONTROL 297 8.1.1.2 PORE-WALL STRUCTURE CONTROL 316
8.1.1.3 SPECIAL MESOSTRUCTURED TEMPLATES 324 8.1.2 SURFACTANT
SELF-ASSEMBLY 325
8.1.2.1 ELECTROSTATIC INTERACTION 3 2 5 8.1.2.2 COMPATIBILITY BETWEEN
BLOCK COPOLYMERS AND PRECURSORS 3 2 7 8.1.2.3 MORPHOLOGY CONTROL 336
8.1.2.4 HYBRID MESOPOROUS CARBON MATERIALS 337
8.1.2.5 PHENOLIC RESOL AND TITANIUM COMPLEX 3 4 0 8.2 MESOPOROUS
POLYMERS 341
8.2.1 NANOCASTING 341
8.2.2 DIRECT SYNTHESIS 348
8.2.2.1 IN-SITU CROSSLINKAGE OF MICELLES 348 8.2.2.2 SELECTIVE ETCHING O
F ONE BLOCK IN ORDERED AGGREGATES O F BLOCK COPOLYMER 3 5 0 8.2.3
SURFACTANT SELF-ASSEMBLY 351 8.3 MESOPOROUS NONSILICEOUS OXIDES 351
8.3.1 SURFACTANT SELF-ASSEMBLY 3 5 2 8.3.2 NANOCASTING 354
IMAGE 5
CONTENTS | I X
8.3.2.1 MESOPOROUS SILICA HARD TEMPLATE 3 5 4
8.3.2.2 PRECURSORS AND FILLING METHODS 363 8.3.2.3 MESOPOROUS CARBON
HARD TEMPLATE 3 7 0 8.4 MESOPOROUS METALS 371
8.4.1 LCT MECHANISM 371
8.4.2 NANOCASTING 374
8.5 MESOPOROUS METAL CHALCOGENIDES 3 7 8
8.5.1 CADMIUM, ZINC, INDIUM, COPPER CHALCOGENIDES 378 8.5.1.1
SOFT-TEMPLATING SYNTHESIS 378 8.5.1.2 NANCOCASTING SYNTHESIS 381 8.5.2
SN, GE, SB, MO, W CHALCOGENIDES 3 8 2 8.5.2.1 SOFT-TEMPLATING SYNTHESIS
3 8 2 8.5.2.2 NANOCASTING SYNTHESIS 3 8 4
8.6 ORDERED MESOPOROUS NONOXIDE CERAMIC MATERIALS 386 8.6.1 MESOPOROUS
SIC MATERIALS 386
8.6.2 MESOPOROUS SILICON NITRIDE AND OXYNITRIDE MATERIALS 391 8.6.3
MESOPOROUS SIOC MATERIALS 3 9 5
8.6.4 MESOPOROUS SICN AND SIBCN MATERIALS 396 8.6.4.1 NANOCASTING
SYNTHESIS 396 8.6.4.2 DIRECT SYNTHESIS BASED ON BLOCK COPOLYMER
SELF-ASSEMBLY 398 8.6.5 MESOPOROUS BN, B 4 C AND BCN MATERIALS 4 0 2
8.6.6 MESOPOROUS CARBON NITRIDE MATERIALS 4 0 4 8.6.7 MESOPOROUS
PHOSPHORUS NITRIDES 407
8.7 MESOPOROUS METAL NITRIDES, CARBIDES AND FLUORIDES 4 0 8 8.7.1
MESOPOROUS METAL NITRIDES 408 8.7.2 MESOPOROUS METAL FLUORIDE MATERIALS
411 8.7.3 MESOPOROUS METAL CARBIDES 4 1 2
REFERENCES 414
9 ORGANIC CROUP FUNCTIONALIZED MESOPOROUS SILICAS 4 2 9 9.1 SYNTHETIC
APPROACHES 4 3 0
9.1.1 GRAFTING ("TWO-STEP") METHOD 4 3 0 9.1.2 COCONDENSATION
("ONE-POT") APPROACH 434 9.1.3 INTERACTION O F THE PORE WALL WITH
ORGANIC FUNCTIONAL GROUP 436
9.1.3.1 LOADING O F ORGANIC GROUPS 436 9.1.3.2 MESOSTRUCTURE AND
MORPHOLOGY 4 4 0 9.1.3.3 CONDENSATION O F SILANES 4 4 2 9.1.3.4
DISTRIBUTION O F ORGANIC FUNCTIONAL GROUPS 444
9.2 COMBINATORIAL SYNTHESIS 446
9.3 ACCESSIBILITY TO THE ACTIVE SITE AND APPLICATIONS 451 9.3.1 SPATIAL
EFFECT 451
9.3.2 FURTHER REACTIVE ABILITY 4 5 3 9.3.3 ADSORPTION PROPERTIES 4 5 5
IMAGE 6
X | CONTENTS
9.4 CONCLUSIONS 459
REFERENCES 459
10 APPLICATIONS O F MESOPOROUS MOLECULAR SIEVES 465 10.1 CATALYSTS AND
CARRIERS 465
10.1.1 INCLUSION O F DISPERSED ATOMIC-LEVEL HETEROATOMS OR OXIDE SPECIES
465 10.1.1.1 ACIDIC CATALYSIS 466 10.1.1.2 BASIC CATALYSIS 469
10.1.1.3 OXIDATION CATALYSIS 470 10.1.2 LOADING HIGHLY DISPERSED METALS
AND THEIR NANOPARTICLES 472 10.1.3 LOADING O F MOLECULAR CATALYSTS 474
10.1.4 NONSILICA MESOPOROUS MATERIALS AS CARRIERS 478 10.2 BIOLOGY,
SEPARATION AND ADSORPTION 479 10.2.1 BIOLOGICAL FIELD 479 10.2.2
SEPARATION AND ADSORPTION 4 8 7 10.3 PHOTOELECTRIC APPLICATIONS 488 10.4
HIGH-TECH FIELDS SUCH AS ELECTROMAGNETISM 492 10.4.1 ELECTROCHEMICAL
CAPACITORS 492 10.4.1.1 DOUBLE-LAYER CAPACITOR 493 10.4.1.2
PSEUDOCAPACITANCE CAPACITOR 497 10.4.1.-3 LITHIUM ION BATTERY 499
10.4.1.4 LITHIUM-SULFUR BATTERY 5 0 2 10.4.1.5 FUEL CELLS 504
REFERENCES 506
11 OUTLOOK 513
INDEX 519 |
| any_adam_object | 1 |
| author | Zhao, Dongyuan 1963- Wan, Ying Zhou, Wuzong |
| author_GND | (DE-588)14075038X (DE-588)14075055X (DE-588)1030190119 |
| author_facet | Zhao, Dongyuan 1963- Wan, Ying Zhou, Wuzong |
| author_role | aut aut aut |
| author_sort | Zhao, Dongyuan 1963- |
| author_variant | d z dz y w yw w z wz |
| building | Verbundindex |
| bvnumber | BV040778642 |
| classification_rvk | VE 9670 VE 9850 VN 6060 ZM 7030 |
| ctrlnum | (OCoLC)827784939 (DE-599)DNB1024048144 |
| dewey-full | 620.116 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 620 - Engineering and allied operations |
| dewey-raw | 620.116 |
| dewey-search | 620.116 |
| dewey-sort | 3620.116 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Chemie / Pharmazie Maschinenbau / Maschinenwesen Werkstoffwissenschaften / Fertigungstechnik |
| format | Book |
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| id | DE-604.BV040778642 |
| illustrated | Illustrated |
| indexdate | 2024-08-21T00:34:27Z |
| institution | BVB |
| isbn | 9783527326358 3527326359 |
| language | English |
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| owner_facet | DE-11 DE-634 DE-29T DE-92 DE-19 DE-BY-UBM |
| physical | XVII, 522 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Zhao, Dongyuan 1963- Verfasser (DE-588)14075038X aut Ordered mesoporous materials Dongyuan Zhao, Ying Wan, and Wuzong Zhou Weinheim Wiley-VCH 2013 XVII, 522 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Nanoporöser Stoff (DE-588)4800345-1 gnd rswk-swf Nanoporöser Stoff (DE-588)4800345-1 s DE-604 Wan, Ying Verfasser (DE-588)14075055X aut Zhou, Wuzong Verfasser (DE-588)1030190119 aut X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4071678&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025756924&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zhao, Dongyuan 1963- Wan, Ying Zhou, Wuzong Ordered mesoporous materials Nanoporöser Stoff (DE-588)4800345-1 gnd |
| subject_GND | (DE-588)4800345-1 |
| title | Ordered mesoporous materials |
| title_auth | Ordered mesoporous materials |
| title_exact_search | Ordered mesoporous materials |
| title_full | Ordered mesoporous materials Dongyuan Zhao, Ying Wan, and Wuzong Zhou |
| title_fullStr | Ordered mesoporous materials Dongyuan Zhao, Ying Wan, and Wuzong Zhou |
| title_full_unstemmed | Ordered mesoporous materials Dongyuan Zhao, Ying Wan, and Wuzong Zhou |
| title_short | Ordered mesoporous materials |
| title_sort | ordered mesoporous materials |
| topic | Nanoporöser Stoff (DE-588)4800345-1 gnd |
| topic_facet | Nanoporöser Stoff |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4071678&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025756924&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT zhaodongyuan orderedmesoporousmaterials AT wanying orderedmesoporousmaterials AT zhouwuzong orderedmesoporousmaterials |