Magnetic particles in supported polymer nanostructures:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Aachen
Shaker
2013
|
| Series: | Berichte aus der Physik
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | 184 S. Ill., graph. Darst. |
| ISBN: | 9783844016277 |
Staff View
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| 245 | 1 | 0 | |a Magnetic particles in supported polymer nanostructures |c Mottakin Mohammad Abul Kashem |
| 264 | 1 | |a Aachen |b Shaker |c 2013 | |
| 300 | |a 184 S. |b Ill., graph. Darst. | ||
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Record in the Search Index
| _version_ | 1804150094064254976 |
|---|---|
| adam_text | IMAGE 1
C O N T E N T S
1 I N T R O D U C T I O N 5
2 T H E O R E T I C A L B A C K G R O U N D 9
2.1 POLYMER 9
2.1.1 CONSTITUTION, CONFIGURATION A N D CONFORMATION OF POLYMER CHAINS .
10
2.1.2 T H E GLASS TRANSITION TEMPERATURE. T G 12
2.1.3 P H A S E SEPARATION 13
2.1.4 MICROPHASE SEPARATION 17
2.1.5 SURFACE INDUCED ORDERING IN BULK 20
2.1.6 DIBLOCK COPOLYMER T H I N FILM 21
2.1.7 MICRODOMAIN ORIENTATION IN T H I N FILM 23
2.2 DEWET.TING OF POLYMER FILMS 25
2.3 INTRODUCTION T O BASIC MAGNETIC PROPERTIES 27
2.3.1 MAGNETIC FIELD A N D MAGNETIZATION 27
2.3.2 TYPES OF MAGNETIC MATERIALS 28
2.3.3 FERROINAGNETISM 28
2.3.4 P A R A M A G N E T I S M 29
2.3.5 SUPERPARAMAGNETISRN 31
2.3.6 DIAMAGNETISM 31
2.3.7 MAGNETIC DOMAINS 31
2.4 NANOPARTICLES 33
2.4.1 MAGNETIC NANOPARTICLES 33
2.5 X-RAY SCATTERING 35
2.5.1 INTERACTION OF X-RAYS WITH M A T T E R 35
2.5.2 BASIC PRINCIPLE OF X-RAY SCATTERING 36
2.5.3 SPECULAR REFLECTIVITY 38
1
HTTP://D-NB.INFO/1029371040
IMAGE 2
2
C O N T E N T S
2.5.4 OFF-SPECULAR SCATTERING 42
2.5.5 DISTORTED-WAVE BORN APPROXIMATION ( D W B A ) 4 3
3 E X P E R I M E N T A L T E C H N I Q U E S 4 7
3.1 SCATTERING TECHNIQUES 47
3.1.1 GRAZING INCIDENCE SMALL-ANGLE X-RAY SCATTERING (GISAXS) 48
3.1.2 X-RAY-REFLECTIVITY 5 3
3.2 REAL-SPACE IMAGING TECHNIQUES -54
3.2.1 ATOMIC FORCE MICROSCOPY (AFM) 54
3.2.2 OPTICAL MICROSCOPY 62
3.2.3 SCANNING ELECTRON MICROSCOPY 62
3.3 SQUID MAGNETOMETRY 62
4 M A G N E T I C N P O N D E W E T T E D D B C S T R . 6 5
4.1 INTRODUCTION 65
4.2 SAMPLE PREPARATION 66
4.3 EXPERIMENTAL SETUP OF GISAXS 66
4.4 RESULTS A N D DISCUSSION 6 /
4.4.1 FROZEN-IN NANOSTRUCTURES 67
4.4.2 NANOSTRUCTURES IN ANNEALED FILMS 82
4.4.3 COMPARISON OF NANOSTRUCTURES IN T H E AS-PREPARED A N D T H E AN
NEALED FILMS 93
4.4.4 MAGNETIC PROPERTIES OF AS-PREPARED FILMS 96
4.5 SUMMARY 102
5 R O U G H N E S S C O R R E L A T I O N 1 0 3
*5.1 INTRODUCTION 103
*5.2 SAMPLE PREPARATION 105
*5.3 RESULTS A N D DISCUSSION 106
5.3.1 SURFACE TOPOGRAPHY 106
5.3.2 FILM D E P T H PROFILE I L L
5.3.3 LONG-RANGE CORRELATION 115
5.3.4 LATERAL CUT-OFF LENGTH, R C 120
*5.4 SUMMARY 122
IMAGE 3
CONTENTS 3
6 P A R T I C L E C O - O P E R A T E D S E L F - A S S E M B L Y 1 2 5
6.1 INTRODUCTION 125
6.2 SAMPLE P R E P A R A T I O N 126
6.3 EXPERIMENTAL S E T U P 127
6.3.1 GISAXS 127
6.4 RESULTS A N D DISCUSSION 128
6.4.1 LOCAL SURFACE STRUCTURES 128
6.4.2 NANOSTRUCTURES INSIDE T H E FILMS 135
6.4.3 EFFECT OF ANNEALING ON T H E SPATIAL ARRANGEMENT OF NANOPARTICLES
. . 142
6.4.4 EFFECT OF ANNEALING A N D NANOPARTICLES O N DOMAIN ORIENTATION . .
. 143
6.5 SUMMARY 145
7 D B C T E M P L A T E D O P I N G 1 4 7
7.1 INTRODUCTION 147
7.2 EXPERIMENTAL DETAILS 147
7.2.1 TEMPLATE PREPARATION 147
7.2.2 SPUTTERING 148
7.2.3 I N SITU GISAXS 149
7.3 RESULTS A N D DISCUSSION 149
7.3.1 TEMPLATE STRUCTURES 149
7.3.2 TEMPLATE DOPING WITH IRON BY SPUTTERING - A N I N SITU GISAXS S T
U D Y 151
7.3.3 IRON NANOPARTICLES FORMATION - A F M INVESTIGATION 156
7.4 S U M M A R Y 160
8 S U M M A R Y A N D O U T L O O K 1 6 3
|
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| format | Thesis Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV040765806 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:33:27Z |
| institution | BVB |
| isbn | 9783844016277 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-025744296 |
| oclc_num | 828809404 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM DE-12 |
| owner_facet | DE-91 DE-BY-TUM DE-12 |
| physical | 184 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Physik |
| spelling | Kashem, Mottakin Mohammad Abul Verfasser aut Magnetic particles in supported polymer nanostructures Mottakin Mohammad Abul Kashem Aachen Shaker 2013 184 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Physik Zugl.: München, Techn. Univ., Diss., 2009 Nanostruktur (DE-588)4204530-7 gnd rswk-swf Magnetteilchen (DE-588)4406122-5 gnd rswk-swf Diblockcopolymere (DE-588)4687200-0 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Magnetteilchen (DE-588)4406122-5 s Diblockcopolymere (DE-588)4687200-0 s Nanostruktur (DE-588)4204530-7 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025744296&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kashem, Mottakin Mohammad Abul Magnetic particles in supported polymer nanostructures Nanostruktur (DE-588)4204530-7 gnd Magnetteilchen (DE-588)4406122-5 gnd Diblockcopolymere (DE-588)4687200-0 gnd |
| subject_GND | (DE-588)4204530-7 (DE-588)4406122-5 (DE-588)4687200-0 (DE-588)4113937-9 |
| title | Magnetic particles in supported polymer nanostructures |
| title_auth | Magnetic particles in supported polymer nanostructures |
| title_exact_search | Magnetic particles in supported polymer nanostructures |
| title_full | Magnetic particles in supported polymer nanostructures Mottakin Mohammad Abul Kashem |
| title_fullStr | Magnetic particles in supported polymer nanostructures Mottakin Mohammad Abul Kashem |
| title_full_unstemmed | Magnetic particles in supported polymer nanostructures Mottakin Mohammad Abul Kashem |
| title_short | Magnetic particles in supported polymer nanostructures |
| title_sort | magnetic particles in supported polymer nanostructures |
| topic | Nanostruktur (DE-588)4204530-7 gnd Magnetteilchen (DE-588)4406122-5 gnd Diblockcopolymere (DE-588)4687200-0 gnd |
| topic_facet | Nanostruktur Magnetteilchen Diblockcopolymere Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025744296&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT kashemmottakinmohammadabul magneticparticlesinsupportedpolymernanostructures |