Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif: = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
2012
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| Subjects: | |
| Online Access: | Volltext https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-34153 http://d-nb.info/1024608670/34 Inhaltsverzeichnis |
| Physical Description: | VI, 240 S. Ill., graph. Darst. |
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| 100 | 1 | |a Ulm, Nadine |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif |b = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv |c von Nadine Ulm |
| 246 | 1 | 1 | |a Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv |
| 264 | 1 | |c 2012 | |
| 300 | |a VI, 240 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |a Erlangen-Nürnberg, Univ., Diss., 2012 | ||
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Record in the Search Index
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| adam_text | IMAGE 1
TABLE OF CONTENTS
I INTRODUCTION 1
1.1 DENDRIMERS 2
1.1.1 TERMS IN DENDRIMER CHEMISTRY 2
1.1.2 SYNTHESIS OF DENDRITIC ARCHITECTURES 3
1.1.3 BASIC TYPES OF DENDRIMERS 5
1.2 THE USE OF DENDRIMERS IN MOLECULAR RECOGNITION 7
1.2.1 SELF-ASSEMBLY PHENOMENA IN DENDRIMERS INTERIOR SHELL 7
1.2.2 SELF-ASSEMBLY PROCESSES IN DENDRIMERS OUTER SHELL 8
1.2.3 SELF-ASSEMBLED DENDRITIC ARCHITECTURES MEDIATED BY INTERMOLECULAR
HYDROGEN BONDINGS 11
1.3 SUPRAMOLECULAR POLYMERS 14
1.3.1 GENERAL ASPECTS OF SUPRAMOLECULAR POLYMERS 14
1.3.2 SUPRAMOLECULAR POLYMERS GENERATED FROM MULTIPLE HYDROGEN BONDING
ARRAYS 16
1.3.3 SUPRAMOLECULAR POLYMERS CONSISTING OF VARIOUS NON-COVALENT
INTERACTIONS 21
1.4 GOLD NANOPARTICLES 24
1.4.1 GENERAL ASPECTS OF GOLD NANOPARTICLES 25
1.4.2 SUPRAMOLECULAR STABILIZATION AND DISTRIBUTION OF GOLD
NANOPARTICLES 27
II PROPOSAL 3 2
III RESULTS AND DISCUSSION 3 5
111.1 SYNTHESIS OF SELF-ASSOCIATING HETEROCOMPLEMENTARY MONOMERIC
BUILDING BLOCKS 35
III. 1.1 SYNTHESIS OF NOVEL ACHIRAL AND CHIRAL HAMILTON RECEPTOR SPACER
UNITS 3 7
111.1.1.1 HAMILTON RECEPTOR UNITS 3 7
111.1.1.2 AMINO-FUNCTIONALIZED HAMILTON SPACER UNITS 4 0
I
HTTP://D-NB.INFO/1026239494
IMAGE 2
III.1.1.3 HYDROXYL-FUNCTIONALIZED HAMILTON SPACER UNITS 48
111.1.2 SYNTHESIS OF NOVEL LINEAR AND BRANCHED CYANURIC ACID DERIVATIVES
49
111.1.2.1 ALIPHATIC CYANURIC DERIVATIVES 51
111.1.2.2 AROMATIC CYANURIC DERIVATIVES 53
111.1.3 SYNTHESIS OF LINEAR AND BRANCHED SUPRAMOLECULAR BUILDING BLOCKS
62
111.1.3.1 LINEAR HETEROCOMPLEMENTARYAB BUILDING BLOCKS 62
111.1.3.2 BRANCHED HETEROCOMPLEMENTARY AB 2 BUILDING BLOCKS 69
111.2 SYNTHESIS OF SELF-COMPLEMENTARY LINEAR AA AND BB MONOMERS 74
111.2.1 SYNTHESIS OF HIGHLY SOLUBLE LINEAR AA BISCYANURATES 75
111.2.1.1 ACHIRAL AA BISCYANURIC DERIVATIVES 75
111.2.1.2 CHIRAL AA BISCYANURIC DERIVATIVES 82
111.2.2 SYNTHESIS OF HIGHLY SOLUBLE LINEAR BB BISRECEPTOR UNITS 85
111.2.2.1 ACHIRAL BB BISRECEPTOR UNITS 85
111.2.2.2 CHIRAL BB BISRECEPTOR UNITS 87
111.3 SYNTHESIS OF DENDRONIZED END CAPS 90
111.3.1 SYNTHESIS O F FRCHET-TYPE CYANURIC END CAPS 9 0
111.3.2 SYNTHESIS O F FRECHET-TYPE H AMILTON END CAPS 9 2
111.4 STABILIZATION OF GOLD NANOPARTICLES VIA SUPRAMOLECULAR
ARCHITECTURES
TO FABRICATE SELF-ASSOCIATED NANOSTRUCTURES 94
111.4.1 STABILIZATION OF GOLD NANOPARTICLES IN SOLUTION 94
III.4.1.1 INVESTIGATIONS USING H-NMR SPECTROSCOPY 96
ML.4.1.2 INVESTIGATIONS USING IR AND UVWIS SPECTROSCOPY 103
111.4.2 STABILIZATION AND DISTRIBUTION OF GOLD NANOPARTICLES ON
AIR/SOLID INTERFACE... 108
111.4.2.1 INVESTIGATIONS ON THE INFLUENCE OF CYANURIC ACID MOIETIES IN
STABILIZATION AND SIZE
DISTRIBUTION PROCESSES OF NANOPARTICLELS 108
111.4.2.2 INVESTIGATIONS ON THE INFLUENCE OF THE SCAFFOLD OF SBBS IN
STABILIZATION AND SIZE
DISTRIBUTION PROCESSES OF NANOPARTICLELS 113
111.5 FORMATION OF SUPRAMOLECULAR POLYMERS GENERATED FROM
COMPLEMENTARY LINEAR AA AND BB MONOMERIC UNITS 119
II
IMAGE 3
111.5.1 SELF-ASSEMBLY PROPERTIES OF LINEAR BISCYANURATES IN COMBINATION
WITH THEIR
STRUCTURAL BISRECEPTOR ANALOGUES - FORMATION OF HOMOPOLYMERS 119
111.5.1.1 DETERMINATION OF THE ASSOCIATION CONSTANTS AND STUDIES ON THE
COOPERATIVITY OF THE
BINDING 120
111.5.1.2 STUDIES ON THE DYNAMIC CHARACTER OF THE SUPRAMOLECULAR
POLYMERIC ASSEMBLIES IN
SOLUTION 126
111.5.2 SELF-ASSEMBLY PROPERTIES OF LINEAR BISCYANURATES IN COMBINATION
WITH
RIGID AND FLEXIBLE METAL-CENTERED BISRECEPTOR UNITS - FORMATION OF
COPOLYMERS 131
111.5.2.1 GENERAL ASPECTS OF METAL-CENTERED BISRECEPTOR UNITS 131
111.5.2.2 SUPRAMOLECULAR POLYMERS GENERATED FROM AXIALLY-COORDINATED
RUTHENIUMPHTHALOCYANINE BISRECEPTORS AND FLEXIBLE BISCYANURATES 135
111.5.2.3 SUPRAMOLECULAR POLYMERS GENERATED FROM FE -TERPYRIDINE-BASED
BISRECEPTORS
AND FLEXIBLE BISCYANURIC UNITS 138
IV S U M M A R Y 1 4 3
V Z U S A M M E N F A S S U N G 1 4 5
VI EXPERIMENTAL SECTION 1 4 8
VI.1 GENERAL REMARKS 148
VI.2 EXPERIMENTAL DETAILS 151
VI.3 EXPERIMENTAL PROCEDURES 152
VI.4 TABLE OF COMPOUNDS 223
VII REFERENCES 2 2 6
VIII APPENDIX 2 3 7
III
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| spelling | Ulm, Nadine Verfasser aut Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv von Nadine Ulm Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv 2012 VI, 240 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Erlangen-Nürnberg, Univ., Diss., 2012 Wasserstoffbrückenbindung (DE-588)4064787-0 gnd rswk-swf Supramolekulare Struktur (DE-588)4208977-3 gnd rswk-swf Supramolekulare Chemie (DE-588)4306141-2 gnd rswk-swf Selbstorganisation (DE-588)4126830-1 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Supramolekulare Struktur (DE-588)4208977-3 s Supramolekulare Chemie (DE-588)4306141-2 s Selbstorganisation (DE-588)4126830-1 s Wasserstoffbrückenbindung (DE-588)4064787-0 s DE-604 Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:29-opus-34153 https://open.fau.de/handle/openfau/2297 Verlag kostenfrei Volltext https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-34153 Resolving-System http://d-nb.info/1024608670/34 Langzeitarchivierung Nationalbibliothek DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025264856&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ulm, Nadine Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv Wasserstoffbrückenbindung (DE-588)4064787-0 gnd Supramolekulare Struktur (DE-588)4208977-3 gnd Supramolekulare Chemie (DE-588)4306141-2 gnd Selbstorganisation (DE-588)4126830-1 gnd |
| subject_GND | (DE-588)4064787-0 (DE-588)4208977-3 (DE-588)4306141-2 (DE-588)4126830-1 (DE-588)4113937-9 |
| title | Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv |
| title_alt | Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv |
| title_auth | Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv |
| title_exact_search | Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv |
| title_full | Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv von Nadine Ulm |
| title_fullStr | Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv von Nadine Ulm |
| title_full_unstemmed | Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv von Nadine Ulm |
| title_short | Flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the Hamilton receptor, cyanuric acid recognition motif |
| title_sort | flexible supramolecular polymers consisting of multiple hydrogen bonding arrays based on the hamilton receptor cyanuric acid recognition motif flexible supramolekulare polymere basierend auf dem hamiltonrezeptor cyanursaure wasserstoffbruckenbindungsmotiv |
| title_sub | = Flexible supramolekulare Polymere basierend auf dem Hamiltonrezeptor-Cyanursäure-Wasserstoffbrückenbindungsmotiv |
| topic | Wasserstoffbrückenbindung (DE-588)4064787-0 gnd Supramolekulare Struktur (DE-588)4208977-3 gnd Supramolekulare Chemie (DE-588)4306141-2 gnd Selbstorganisation (DE-588)4126830-1 gnd |
| topic_facet | Wasserstoffbrückenbindung Supramolekulare Struktur Supramolekulare Chemie Selbstorganisation Hochschulschrift |
| url | https://open.fau.de/handle/openfau/2297 https://nbn-resolving.org/urn:nbn:de:bvb:29-opus-34153 http://d-nb.info/1024608670/34 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025264856&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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