Surface science: foundations of catalysis and nanoscience
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Chichester
Wiley
2012
|
| Edition: | 3. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Includes bibliographical references and index |
| Physical Description: | XIII, 556 S. Ill., graph. Darst. |
| ISBN: | 9780470665565 9781119990352 9781119990369 |
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MARC
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| 020 | |a 9781119990352 |c pbk. |9 978-1-119-99035-2 | ||
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| 100 | 1 | |a Kolasinski, Kurt W. |e Verfasser |0 (DE-588)138439060 |4 aut | |
| 245 | 1 | 0 | |a Surface science |b foundations of catalysis and nanoscience |c Kurt W. Kolasinski |
| 250 | |a 3. ed. | ||
| 264 | 1 | |a Chichester |b Wiley |c 2012 | |
| 300 | |a XIII, 556 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Includes bibliographical references and index | ||
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Record in the Search Index
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| adam_text | Contents
Acknowledgements
XV
Introduction
j
1.1 Heterogeneous catalysis
2
1.2
Why surfaces?
3
1.3
Where are heterogeneous reactions important?
3
1.3.1
Haber-Bosch process
3
1.3.2
Fischer-Tropsch chemistry
4
1.3.3
Three-way catalyst
4
1.4
Semiconductor processing and nanotechnology
4
1.5
Other areas of relevance
5
1.6
Structure of the book
5
References
7
1
Surface and
Adsórbate
Structure
9
1.1
Clean surface structure
10
1.1.1
Ideal flat surfaces
10
1.1.2
High index and vicinal planes
13
1.1.3
Faceted surfaces
14
1.1.4
Bimetallic surfaces
14
1.1.5
Oxide and compound semiconductor surfaces
15
1.1.6
The carbon family: Diamond, graphite, graphene,
fullerenes
and carbon nanotubes
18
1.1.7
Porous solids
21
1.2
Reconstruction and
adsórbate
structure
22
1.2.1
Implications of surface heterogeneity for adsorbates
22
1.2.2
Clean surface reconstructions
23
1.2.3
Adsórbate
induced reconstructions
24
1.2.4
Islands
27
1.2.5
Chiral surfaces
28
1.3
Band structure of solids
30
1.3.1
Bulk electronic states
30
1.3.2
Metals, semiconductors and insulators
30
1.3.3
Energy levels at metal interfaces
34
1.3.4
Energy levels at metal-semiconductor interfaces
36
1.3.5
Surface electronic states
38
1.3.6
Size effects in nanoscale systems
39
1.4
The vibrations of solids
41
1.4.1
Bulk systems
41
1.4.2
Nanoscale systems
43
viii Contents
1.5
Summary of important concepts
43
1.6
Frontiers and challenges
44
1.7
Further reading
44
1.8
Exercises
44
References
47
2
Experimental Probes and Techniques
51
2.1
Ultrahigh vacuum
51
2.1.1
The need for UHV
51
2.1.2
Attaining UHV
52
2.2
Light and electron sources
53
2.2.1
Types of lasers
54
2.2.2
Atomic lamps
54
2.2.3
Synchrotrons
56
2.2.4
Free electron laser
(FEL)
56
2.2.5
Electron guns
57
2.3
Molecular beams
57
2.3.1
Knudsen molecular beams
57
2.3.2
Free Jets
58
2.3.3
Comparison of Knudsen and supersonic beams
60
2.4
Scanning probe techniques
63
2.4.1
Scanning tunnelling microscopy (STM)
63
2.4.2
Scanning tunnelling spectroscopy
(STS)
67
2.4.3
Atomic force microscopy (AFM)
67
2.4.4
Near-field scanning optical microscopy (NSOM)
70
2.5
Low energy electron diffraction
(LEED)
73
Advanced Topic:
LEED
structure determination
77
2.6
Electron spectroscopy
80
2.6.1
X-ray photoelectron spectroscopy (XPS)
80
2.6.2
Ultraviolet photoelectron spectroscopy (UPS)
85
Advanced Topic: Multiphoton photoemission (MPPE)
89
2.6.3
Auger electron spectroscopy (AES)
90
2.6.4
Photoelectron microscopy
94
2.7
Vibrational spectroscopy
95
2.7.1
IR
spectroscopy
97
2.7.2
Electron energy loss spectroscopy (EELS)
101
2.8
Second harmonic and sum frequency generation
103
2.9
Other surface analytical techniques
105
2.10
Summary of important concepts
106
2.11
Frontiers and challenges
106
2.12
Further reading
107
2.13
Exercises
107
References
111
3
Chemisorption, Physisorption and Dynamics
115
3.1
Types of interactions
115
3.2
Binding sites and diffusion
116
Contents
¡χ
3.3 Physisorption J2O
Advanced
Topic: Theoretical Description of Physisorption
120
3.4
Non-dissociative chemisorption
121
3.4.1
Theoretical treatment of chemisorption
121
3.4.2
The Blyholder model of CO chemisorption on a metal
124
3.4.3
Molecular oxygen chemisorption
127
3.4.4
The binding of ethene
128
3.5
Dissociative chemisorption: H2 on a simple metal
129
3.6
What determines the reactivity of metals?
130
3.7
Atoms and molecules incident on a surface 133
3.7.1
Scattering channels I33
3.7.2
Non-activated adsorption I35
3.7.3
Hard cube model I37
3.7.4
Activated adsorption I39
3.7.5
Direct versus precursor mediated adsorption
140
3.8
Microscopic reversibility in Ad/Desorption phenomena I44
3.9
The influence of individual degrees of freedom on adsorption and desorption
148
3.9.1
Energy exchange
148
3.9.2
PES
topography and the relative efficacy of energetic components
149
3.10
Translations, corrugation, surface atom motions
150
3.10.1
Effects on adsorption
150
3.10.2
Connecting adsorption and desorption with microscopic reversibility
153
3.10.3
Normal energy scaling I54
3.11
Rotations and adsorption
156
3.11.1
Non-activated adsorption
156
3.11.2
Activated adsorption
157
3.12
Vibrations and adsorption
158
3.13
Competitive adsorption and collision induced processes
158
Advanced Topic: High Energy Collisions
161
3.14
Classification of reaction mechanisms
161
3.14.1
Langmuir-Hinshelwood mechanism
162
3.14.2
Eley-Rideal mechanism
164
3.14.3
Hot atom mechanism
164
3.15
Measurement of sticking coefficients
165
3.16
Summary of important concepts
168
3.17
Frontiers and challenges
169
3.18
Further reading
170
3.19
Exercises
170
References
177
4
Thermodynamics and Kinetics of Adsorption and Desorption
185
4.1
Thermodynamics of Ad/Desorption
185
4.1.1
Binding energies and activation barriers
185
4.1.2
Thermodynamic quantities
187
4.1.3
Some definitions
187
4.1.4
The heat of adsorption
188
4.2
Adsorption isotherms from thermodynamics
190
χ
Contents
4.3 Lateral
interactions
193
4.4 Rate
of
desorption 194
4.4.1
First-order
desorption 195
4.4.2
Transition state theory treatment of first-order desorption
196
4.4.3
Thermodynamic treatment of first-order desorption
199
4.4.4
Non-first-order desorption
201
4.5
Kinetics of adsorption
202
4.5.1
CTST approach to adsorption kinetics
202
4.5.2
Langmuirian adsorption: Non-dissociative adsorption
203
4.5.3
Langmuirian adsorption: Dissociative adsorption
205
4.5.4
Dissociative Langmuirian adsorption with lateral interactions
207
4.5.5
Precursor mediated adsorption
207
4.6
Adsorption isotherms from kinetics
210
4.6.1
Langmuir isotherm
210
4.6.2
Classification of adsorption isotherms
211
4.6.3
Thermodynamic measurements via isotherms
213
4.7
Temperature programmed desorption
(TPD)
213
4.7.1
The basis of
TPD
213
4.7.2
Qualitative analysis of
TPD
spectra
215
4.7.3
Quantitative analysis of
TPD
spectra
217
4.8
Summary of important concepts
221
4.9
Frontiers and challenges
222
4.10
Further reading
222
4.11
Exercises
222
References
227
5
Liquid Interfaces
229
5.1
Structure of the liquid/solid interface
229
5.1.1
The structure of the water/solid interface
230
5.2
Surface energy and surface tension
234
5.2.1
Liquid surfaces
234
5.2.2
Curved interfaces
236
5.2.3
Capillary waves
238
5.3
Liquid films
239
5.3.1
Liquid-on-solid films
239
5.4
Langmuir films
241
5.5
Langmuir-Blodgett films
243
5.5.1
Capillary condensation and meniscus formation
243
5.5.2
Vertical deposition
246
5.5.3
Horizontal lifting (Shaefer s method)
247
5.6
Self assembled monolayers (SAMs)
248
5.6.1
Thermodynamics of self-assembly
249
5.6.2
Amphiphiles and bonding interactions
250
5.6.3
Mechanism of SAM formation
250
Advanced Topic: Chemistry with Self Assembled Monolayers
253
Contents xi
5.7
Thermodynamics of liquid interfaces
254
5.7.1
The Gibbs model
254
5.7.2
Surface excess
254
5.7.3
Interfacial
enthalpy and internal, Helmholtz and Gibbs surface energies
256
5.7.4
Gibbs adsorption isotherm
257
5.8
Electrified and charged interfaces
257
5.8.1
Surface charge and potential
257
5.8.2
Relating work functions to the electrochemical series
259
5.9
Summary of important concepts
261
5.10
Frontiers and challenges
262
5.11
Further reading
262
5.12
Exercises
263
References
265
6
Heterogeneous Catalysis
267
6.1
The prominence of heterogeneous reactions
267
6.2
Measurement of surface kinetics and reaction mechanisms
269
6.3
Haber-Bosch process
273
6.4
From microscopic kinetics to catalysis
277
6.4.1
Reaction kinetics
277
6.4.2
Kinetic analysis using
De Donder
relations
278
6.4.3
Definition of the rate determining step (RDS)
279
6.4.4
Microkinetic analysis of ammonia synthesis
280
6.5
Fischer-Tropsch synthesis and related chemistry
283
6.6
The three-way automotive catalyst
286
6.7
Promoters
288
6.8
Poisons
290
6.9
Bimetallic and bifunctional catalysts
291
6.10
Rate oscillations and
spatiotemporal
pattern formation
292
Advanced Topic: Cluster assembled catalysts
294
6.11
Sabatier analysis and optimal catalyst selection
295
6.12
Summary of important concepts
296
6.13
Frontiers and challenges
297
6.14
Further reading
298
6.15
Exercises
298
References
300
7
Growth and Epitaxy
305
7.1
Stress and strain
305
7.2
Types of interfaces
308
7.2.1
Strain relief
309
7.3
Surface energy, surface tension and strain energy
310
7.4
Growth modes
311
7.4.1
Solid-on-solid growth
311
7.4.2
Strain in solid-on-solid growth
313
xii Contents
7.4.3 Ostwald
ripening
314
7.4.4
Equilibrium overlay
er
structure and growth mode
315
7.5
Nucleation theory
317
7.6
Growth away from equilibrium
319
7.6.1
Thermodynamics versus dynamics
319
7.6.2
Non-equilibrium growth modes
320
7.7
Techniques for growing layers
322
7.7.1
Molecular beam epitaxy (MBE)
323
7.7.2
Chemical vapour deposition (CVD)
326
7.7.3
Ablation techniques
327
7.8
Catalytic growth of nanotubes and nanowires
327
7.9
Etching
332
7.9.1
Classification of etching
332
7.9.2
Etch morphologies
335
7.9.3
Porous solid formation
336
7.9.4
Silicon etching in aqueous fluoride solutions
337
7.9.5
Coal gasification and graphite etching
340
7.9.6
Selective area growth and etching
341
Advanced Topic: Si Pillar Formation
343
7.10
Summary of important concepts
344
7.11
Frontiers and challenges
344
7.12
Further reading
345
7.13
Exercises
345
References
347
8
Laser and Non-Thermal Chemistry: Photon and Electron Stimulated Chemistry and
Atom Manipulation
353
8.1
Photon excitation of surfaces
354
8.1.1
Light absorption by condensed matter
354
8.1.2
Lattice heating
355
Advanced Topic: Temporal evolution of electronic excitations
359
8.1.3
Summary of laser excitations
365
8.2
Mechanisms of electron and photon stimulated processes
366
8.2.1
Direct versus substrate mediated processes
366
8.2.2
Gas phase photochemistry
367
8.2.3
Gas phase electron stimulated chemistry
369
8.2.4
MGR
and Antoniewicz models of DIET
369
8.2.5
Desorption induced by ultrafast excitation
373
8.3
Photon and electron induced chemistry at surfaces
374
8.3.1
Thermal desorption, reaction and diffusion
374
8.3.2
Stimulated desorption/reaction
375
8.3.3
Ablation
381
8.4
Charge transfer and electrochemistry
384
8.4.1
Homogeneous electron transfer
385
8.4.2
Corrections to and improvements on Marcus theory
387
Contents xiii
8.4.3
Heterogeneous electron transfer
339
8.4.4
Current flow at a metal electrode
391
Advanced Topic: Semiconductor photoelectrodes and the
Grätzel
photovoltaic cell
393
8.5
Tip Induced process: mechanisms of atom manipulation
397
8.5.1
Electric field effects
39g
8.5.2
Tip induced
ESD
39g
8.5.3
Vibrational ladder climbing
399
8.5.4
Pushing
400
8.5.5
Pulling
402
8.5.6
Atom manipulation by covalent forces
402
8.6
Summary of important concepts
404
8.7
Frontiers and challenges
404
8.8
Further reading
405
8.9
Exercises
405
References
408
9
Answers to Exercises from Chapter
1.
Surface and
Adsórbate
Structure
415
10
Answers to Exercises from Chapter
2.
Experimental Probes and Techniques
427
11
Answers to Exercises from Chapter
3.
Chemisorption, Physisorption and Dynamics
445
12
Answers to Exercises from Chapter
4.
Thermodynamics and Kinetics of Adsorption and
Desorption
465
13
Answers to Exercises from Chapter
5.
Liquid Interfaces
487
14
Answers to Exercises from Chapter
6.
Heterogeneous Catalysis
499
15
Answers to Exercises From Chapter
7.
Growth and Epitaxy
509
16
Answers to exercises from Chapter
8.
Laser and Nonthermal Chemistry
515
Appendix I Abbreviations and Prefixes
531
Appendix II Symbols
535
Appendix III Useful Mathematical Expressions
541
Index
545
|
| any_adam_object | 1 |
| author | Kolasinski, Kurt W. |
| author_GND | (DE-588)138439060 |
| author_facet | Kolasinski, Kurt W. |
| author_role | aut |
| author_sort | Kolasinski, Kurt W. |
| author_variant | k w k kw kwk |
| building | Verbundindex |
| bvnumber | BV040108791 |
| classification_rvk | VE 7000 |
| classification_tum | CHE 180f CHE 167f PHY 629f |
| ctrlnum | (OCoLC)794246081 (DE-599)GBV683287052 |
| dewey-full | 541.33 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541.33 |
| dewey-search | 541.33 |
| dewey-sort | 3541.33 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Chemie |
| edition | 3. ed. |
| format | Book |
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| id | DE-604.BV040108791 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:17:03Z |
| institution | BVB |
| isbn | 9780470665565 9781119990352 9781119990369 |
| language | English |
| lccn | 2011051138 |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-024965186 |
| oclc_num | 794246081 |
| open_access_boolean | |
| owner | DE-703 DE-91G DE-BY-TUM DE-29T DE-20 |
| owner_facet | DE-703 DE-91G DE-BY-TUM DE-29T DE-20 |
| physical | XIII, 556 S. Ill., graph. Darst. |
| publishDate | 2012 |
| publishDateSearch | 2012 |
| publishDateSort | 2012 |
| publisher | Wiley |
| record_format | marc |
| spelling | Kolasinski, Kurt W. Verfasser (DE-588)138439060 aut Surface science foundations of catalysis and nanoscience Kurt W. Kolasinski 3. ed. Chichester Wiley 2012 XIII, 556 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references and index Festkörperoberfläche (DE-588)4127823-9 gnd rswk-swf Oberflächenphysik (DE-588)4134881-3 gnd rswk-swf Oberflächenchemie (DE-588)4126166-5 gnd rswk-swf Oberflächenreaktion (DE-588)4140095-1 gnd rswk-swf Heterogene Katalyse (DE-588)4123377-3 gnd rswk-swf Festkörperoberfläche (DE-588)4127823-9 s Oberflächenchemie (DE-588)4126166-5 s DE-604 Oberflächenphysik (DE-588)4134881-3 s Oberflächenreaktion (DE-588)4140095-1 s Heterogene Katalyse (DE-588)4123377-3 s Erscheint auch als Online-Ausgabe 978-1-118-30861-5 Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024965186&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kolasinski, Kurt W. Surface science foundations of catalysis and nanoscience Festkörperoberfläche (DE-588)4127823-9 gnd Oberflächenphysik (DE-588)4134881-3 gnd Oberflächenchemie (DE-588)4126166-5 gnd Oberflächenreaktion (DE-588)4140095-1 gnd Heterogene Katalyse (DE-588)4123377-3 gnd |
| subject_GND | (DE-588)4127823-9 (DE-588)4134881-3 (DE-588)4126166-5 (DE-588)4140095-1 (DE-588)4123377-3 |
| title | Surface science foundations of catalysis and nanoscience |
| title_auth | Surface science foundations of catalysis and nanoscience |
| title_exact_search | Surface science foundations of catalysis and nanoscience |
| title_full | Surface science foundations of catalysis and nanoscience Kurt W. Kolasinski |
| title_fullStr | Surface science foundations of catalysis and nanoscience Kurt W. Kolasinski |
| title_full_unstemmed | Surface science foundations of catalysis and nanoscience Kurt W. Kolasinski |
| title_short | Surface science |
| title_sort | surface science foundations of catalysis and nanoscience |
| title_sub | foundations of catalysis and nanoscience |
| topic | Festkörperoberfläche (DE-588)4127823-9 gnd Oberflächenphysik (DE-588)4134881-3 gnd Oberflächenchemie (DE-588)4126166-5 gnd Oberflächenreaktion (DE-588)4140095-1 gnd Heterogene Katalyse (DE-588)4123377-3 gnd |
| topic_facet | Festkörperoberfläche Oberflächenphysik Oberflächenchemie Oberflächenreaktion Heterogene Katalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024965186&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT kolasinskikurtw surfacesciencefoundationsofcatalysisandnanoscience |