Simultaneous AFM and STM measurements: carbon allotropes, polymers and supramolecular compounds
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
2011
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | 110 S. Ill., graph. Darst. |
Staff View
MARC
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| 100 | 1 | |a Jum'h, Inshad Yousef |d 1974- |e Verfasser |0 (DE-588)1018629726 |4 aut | |
| 245 | 1 | 0 | |a Simultaneous AFM and STM measurements |b carbon allotropes, polymers and supramolecular compounds |c vorgelegt von Inshad Yousef Jum'h |
| 264 | 1 | |c 2011 | |
| 300 | |a 110 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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| 502 | |a Erlangen-Nürnberg, Univ., Diss., 2011 | ||
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Record in the Search Index
| _version_ | 1804148736810549248 |
|---|---|
| adam_text | CONTENTS
ABSTRACT
.................................................................................................................................
4
ZUSAMMENFASSUNG
...........................................................................................................
5
CHAPTER
1
INTRODUCTION
...........................................................................................
6
CHAPTER
2
BASICS
OF
SCANNING
TUNNELING
AND
ATOMIC
FORCE
10
MICROSCOPY
2.1
THEORY
OF
SCANNING
TUNNELING
MICROSCOPY
..........................................................................
10
2.1.1
TUNNEL
CURRENT
...............................................................................................................
10
2.1.2
OPERATION
MODE
OF
AN
STM
.........................................................................................
12
2.1.2.1
TOPOGRAPHY
IMAGE
..........................................................................................
12
2.1.2.2
CURRENT
IMAGING
TUNNELING
SPECTROSCOPY
(CITS)
........................................
13
2.1.3
TUNNELING
THROUGH
MOLECULAR
ORBITALS
........................................................................
13
2.1.4
OBSERVATION
OF
MOLECULES
AT
LOW
BIAS
VOLTAGES
.........................................................
15
2.2
ATOMIC
FORCE
MICROSCOPY
.....................................................................................................
16
2.2.1
INTERACTION
FORCES
IN
AFM
...........................................................................................
16
2.2.2
OPERATING
MODES
OF
AFM
...........................................................................................
18
2.2.3
RESOLUTION
OF
THE
FM-AFM
.........................................................................................
19
2.2.4
FORCE
SENSOR
...................................................................................................................
20
2.2.5
TUNING
FORK
SENSORS
......................................................................................................
21
2.2.6
DYNAMICS
OF
A
VIBRATING
TUNING
FORK
WITH
TIP
............................................................
24
2.2.7
FM-AFM
CONTROL
SYSTEM
FOR
TUNING
FORK
...................................................................
27
2.2.8
DISSIPATION
ENERGY
IN
FM-AFM
.................................................................................
27
2.2.9
ADVANCED
AFM
MODES
OF
OPERATION
..........................................................................
29
CHAPTER
3
EXPERIMENTAL
SET-UP
.....................................................................
33
3.1
CONTROL
ELECTRONICS
OF
THE
STM/AFM
MICROSCOPE
.............................................................
33
3.2
CONSTRUCTION
OF
THE
MICROSCOPE
...........................................................................................
36
3.3
VIBRATION
ISOLATION
..................................................................................................................
39
3.4
CALIBRATION
OF
THE
X
Y
AND
Z
PIEZO
...................................................................................
39
3.5
QUARTZ
TUNING
FORK
................................................................................................................
40
3.5.1
INSTALLATION
OF
THE
TUNING
FORK
SENSORS
........................................................................
41
3.5.2
EXCITATION
OF
THE
TUNING
FORK
.....................................................................................
42
3.5.3
DETERMINATION
OF
THE
QUALITY
FACTOR
..........................................................................
44
3.5.4
CALIBRATION
OF
THE
AMPLITUDE
.......................................................................................
45
3.6
TIP
PREPARATION
......................................................................................................................
46
3.7
SAMPLE
PREPARATION
.................................................................................................................
49
CHAPTER
4
RESULTS
AND
DISCUSSION
..............................................................
51
4.1
SIMULTANEOUS
AFM/STM
ON
CARBON
ALLOTROPES
................................................................
51
4.1.1
ATOMIC
RESOLUTION
ON
HOPG
.......................................................................................
51
4.1.2
CARBON
NANOTUBES
........................................................................................................
56
4.1.3
GRAPHENE
AND
FEW
LAYERED
GRAPHITE
(FLG)
ON
CONDUCTIVE
SUBSTRATES
.................
63
4.1.4
GRAPHITIZED
POLYIMIDE
..................................................................................................
71
4.2
ONE-DIMENSIONAL
NANOSTRUCTURES
..........................................................................................
76
4.2.1.
CU(II)
COORDINATION
POLYMER
.....................................................................................
77
4.2.2.
ZN
COORDINATION
POLYMER
........................................................................................
79
4.3
FE(II)
SPIN-CROSSOVER
COMPLEX
ON
HOPG
..........................................................................
82
CHAPTERS
CONCLUSIONS
........................................................................................
95
REFERENCES
.............................................................................................................................
98
PUBLICATIONS
AND
CONFERENCE
CONTRIBUTIONS
..............................................
105
ACKNOWLEDGEMENTS
........................................................................................................
106
CURRICULUM
VITAE
.............................................................................................................
108
|
| any_adam_object | 1 |
| author | Jum'h, Inshad Yousef 1974- |
| author_GND | (DE-588)1018629726 |
| author_facet | Jum'h, Inshad Yousef 1974- |
| author_role | aut |
| author_sort | Jum'h, Inshad Yousef 1974- |
| author_variant | i y j iy iyj |
| building | Verbundindex |
| bvnumber | BV039806728 |
| ctrlnum | (OCoLC)775091297 (DE-599)DNB1018775048 |
| dewey-full | 541.33 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541.33 |
| dewey-search | 541.33 |
| dewey-sort | 3541.33 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV039806728 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:11:53Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-024667081 |
| oclc_num | 775091297 |
| open_access_boolean | |
| owner | DE-29 DE-188 DE-355 DE-BY-UBR DE-29T DE-12 DE-703 |
| owner_facet | DE-29 DE-188 DE-355 DE-BY-UBR DE-29T DE-12 DE-703 |
| physical | 110 S. Ill., graph. Darst. |
| publishDate | 2011 |
| publishDateSearch | 2011 |
| publishDateSort | 2011 |
| record_format | marc |
| spelling | Jum'h, Inshad Yousef 1974- Verfasser (DE-588)1018629726 aut Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds vorgelegt von Inshad Yousef Jum'h 2011 110 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Erlangen-Nürnberg, Univ., Diss., 2011 Rastertunnelmikroskopie (DE-588)4252995-5 gnd rswk-swf Kohlenstoffverbindungen (DE-588)4164566-2 gnd rswk-swf Rasterkraftmikroskopie (DE-588)4274473-8 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Rasterkraftmikroskopie (DE-588)4274473-8 s Rastertunnelmikroskopie (DE-588)4252995-5 s Kohlenstoffverbindungen (DE-588)4164566-2 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024667081&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Jum'h, Inshad Yousef 1974- Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds Rastertunnelmikroskopie (DE-588)4252995-5 gnd Kohlenstoffverbindungen (DE-588)4164566-2 gnd Rasterkraftmikroskopie (DE-588)4274473-8 gnd |
| subject_GND | (DE-588)4252995-5 (DE-588)4164566-2 (DE-588)4274473-8 (DE-588)4113937-9 |
| title | Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds |
| title_auth | Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds |
| title_exact_search | Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds |
| title_full | Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds vorgelegt von Inshad Yousef Jum'h |
| title_fullStr | Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds vorgelegt von Inshad Yousef Jum'h |
| title_full_unstemmed | Simultaneous AFM and STM measurements carbon allotropes, polymers and supramolecular compounds vorgelegt von Inshad Yousef Jum'h |
| title_short | Simultaneous AFM and STM measurements |
| title_sort | simultaneous afm and stm measurements carbon allotropes polymers and supramolecular compounds |
| title_sub | carbon allotropes, polymers and supramolecular compounds |
| topic | Rastertunnelmikroskopie (DE-588)4252995-5 gnd Kohlenstoffverbindungen (DE-588)4164566-2 gnd Rasterkraftmikroskopie (DE-588)4274473-8 gnd |
| topic_facet | Rastertunnelmikroskopie Kohlenstoffverbindungen Rasterkraftmikroskopie Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024667081&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT jumhinshadyousef simultaneousafmandstmmeasurementscarbonallotropespolymersandsupramolecularcompounds |