Mass spectrometry in polymer chemistry:
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2012
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| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XV, 483 S. Ill., graph. Darst. |
| ISBN: | 9783527641826 9783527641857 9783527329243 3527329242 |
Internformat
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IMAGE 1
CONTENTS
LIST OF CONTRIBUTORS XIII
INTRODUCTION 1 CHRISTOPHER BARNER-KOWOLLIK, JANA FALKENHAGEN, TILL
GRUENDLING, AND STEFFEN WEIDNER REFERENCES 4
1
1.1 1.2 1.2.1 1.2.2 1.2.3
1.2.4 1.2.5 1.3 1.3.1 1.3.2
1.3.3 1.3.4 1.3.5 1.3.6
1.3.7 1.4
1.5
MASS ANALYSIS 5 CENE HART-SMITH AND STEPHEN J. BLANKSBY INTRODUCTION 5
MEASURES OF PERFORMANCE 5 MASS RESOLVING POWER 6 MASS ACCURACY 8 MASS
RANGE 9 LINEAR DYNAMIC RANGE 9 ABUNDANCE SENSITIVITY 10
INSTRUMENTATION 12 SECTOR MASS ANALYZERS 12 QUADRUPOLE MASS FILTERS 15
3D ION TRAPS 17 LINEAR ION TRAPS 19 TIME-OF-FLIGHT MASS ANALYZERS 20
FOURIER TRANSFORM ION CYCLOTRON RESONANCE MASS ANALYZERS ORBITRAPS 24
INSTRUMENTATION IN TANDEM AND MULTIPLE-STAGE MASS SPECTROMETRY 25
CONCLUSIONS AND OUTLOOK 29
REFERENCES 30
22
2 LONIZATION TECHNIQUES FOR POLYMER MASS SPECTROMETRY 33 ANTHONY P. CIES
2.1 INTRODUCTION 33
2.2 SMALL MOLECULE LONIZATION ERA 34
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1012093875
DIGITALISIERT DURCH
IMAGE 2
VI CONTENTS
2.2.1 ELECTRON LONIZATION (EI) 34
2.2.2 CHEMICAL LONIZATION (CI) 36 2.2.3 PYROLYSIS MASS SPECTROMETRY
(PY-MS) 37 2.3 MACROMASS ERA OF LONIZATION 38
2.3.1 FIELD DESORPTION (FD) AND FIELD LONIZATION (FI) 38 2.3.2 SECONDARY
ION MASS SPECTROMETRY (SIMS) 40 2.3.3 FAST ATOM BOMBARDMENT (FAB) AND
LIQUID SECONDARY ION MASS SPECTROMETRY (LSIMS) 42
2.3.4 LASER DESORPTION (LD) 43 2.3.5 PLASMA DESORPTION (PD) 44 2.3.6
OTHER LONIZATION METHODS 45 2.4 MODERN ERA OF LONIZATION TECHNIQUES 45
2.4.1 ELECTROSPRAY LONIZATION (ESI) 46 2.4.2 NEW TRENDS 48
2.4.3 ATMOSPHERIC PRESSURE CHEMICAL LONIZATION (APCI) 49 2.4.4 NEW
TRENDS 49
2.4.5 MATRIX-ASSISTED LASER DESORPTION/IONIZATION (MALDI) 49 2.4.6 NEW
TRENDS 52
2.5 CONCLUSIONS 53
REFERENCES 53
3 TANDEM MASS SPECTROMETRY ANALYSIS OF POLYMER STRUCTURES AND
ARCHITECTURES 57 VINCENZO SCIONTI AND CHRYS WESDEMIOTIS 3.1 INTRODUCTION
57
3.2 ACTIVATION METHODS 59
3.2.1 COLLISIONALLY ACTIVATED DISSOCIATION (CAD) 59 3.2.2
SURFACE-INDUCED DISSOCIATION (SID) 60 3.2.3 PHOTODISSOCIATION METHODS 60
3.2.4 ELECTRON CAPTURE DISSOCIATION AND ELECTRON TRANSFER DISSOCIATION
(ECD/ETD) 61
3.2.5 POST-SOURCE DECAY (PSD) 62 3.3 INSTRUMENTATION 62
3.3.1 QUADRUPOLE ION TRAP (QIT) MASS SPECTROMETERS 63 3.3.2
QUADRUPOLE/TIME-OF-FLIGHT (Q/TOF) MASS SPECTROMETERS 69 3.3.3 TOF/TOF
INSTRUMENTS 72 3.4 STRUCTURAL INFORMATION FROM MS 2 STUDIES 75
3.4.1 END-GROUP ANALYSIS AND ISOMER/ISOBAR DIFFERENTIATION 75 3.4.2
POLYMER ARCHITECTURES 75 3.4.3 COPOLYMER SEQUENCES 76 3.4.4 ASSESSMENT
OF INTRINSIC STABILITIES AND BINDING ENERGIES 77
3.5 SUMMARY AND OUTLOOK 78
REFERENCES 79
IMAGE 3
CONTENTS VII
4 MATRIX-ASSISTED INLET LONIZATION AND SOLVENT-FREE GAS-PHASE
SEPARATION USING ION MOBILITY SPECTROMETRY FOR IMAGING AND ELECTRON
TRANSFER DISSOCIATION MASS SPECTROMETRY OF POLYMERS 85 CHRISTOPHER B.
LIETZ, ALICIA L RICHARDS, DARREIL D. MARSHALL, YUE REN, AND SARAH
TRIMPIN 4.1 OVERVIEW 85
4.2 INTRODUCTION 87
4.3 NEW SAMPLE INTRODUCTION TECHNOLOGIES 92 4.3.1 LASERSPRAY LONIZATION
- ION MOBILITY SPECTROMETRY-MASS SPECTROMETRY 95 4.3.2 MATRIX ASSISTED
INLET LONIZATION (MAII) 99 4.3.3 LSIV IN REFLECTION GEOMETRY AT
INTERMEDIATE PRESSURE (IP) 100 4.4 FRAGMENTATION BY ETD AND CID 102 4.5
SURFACE ANALYSES BY IMAGING MS 103 4.5.1 ULTRAF FAST LSII-MS IMAGING IN
TRANSMISSION GEOMETRY (TG) 105 4.5.2 LSIV-IMS-MS IMAGING IN REFLECTION
GEOMETRY (RG) 106 4.6 FUTURE OUTLOOK 109
REFERENCES 110
5 POLYMER M ALDI SAMPLE PREPARATION 119 SCOTT D. HANTON AND KEVIN C.
OWENS 5.1 INTRODUCTION 119
5.2 ROLES OF THE MATRIX 120
5.2.1 INTIMATE CONTACT 121 5.2.2 ABSORPTION OF LASER LIGHT 121 5.2.3
EFFICIENT DESORPTION 122 5.2.4 EFFECTIVE LONIZATION 123
5.3 CHOICE OF MATRIX 125
5.4 CHOICE OF THE SOLVENT 125
5.5 BASIC SOLVENT-BASED SAMPLE PREPARATION RECIPE 127 5.6 DEPOSITION
METHODS 127
5.7 SOLVENT-FREE SAMPLE PREPARATION 130 5.8 THE VORTEX METHOD 132
5.9 MATRIX-TO-ANALYTE RATIO 134 5.10 SALT-TO-ANALYTE RATIO 136 5.11
CHROMATOGRAPHY AS SAMPLE PREPARATION 138 5.12 PROBLEMS IN MALDI SAMPLE
PREPARATION 140 5.13 PREDICTING MALDI SAMPLE PREPARATION 142 5.14
CONCLUSIONS 143
REFERENCES 144
6 SURFACE ANALYSIS AND IMAGING TECHNIQUES 149 CHRISTINE M. MAHONEY AND
STEFFEN M. WEIDNER 6.1 IMAGING MASS SPECTROMETRY 149 6.2 SECONDARY ION
MASS SPECTROMETRY 150
IMAGE 4
VIII CONTENTS
6.2.1 STATIC SIMS OF POLYMERS 150
6.2.1.1 THE FINGERPRINT REGION 151 6.2.1.2 HIGH-MASS REGION 162 6.2.2
IMAGING IN POLYMER BLENDS AND MULTICOMPONENT SYSTEMS 168 6.2.3 DATA
ANALYSIS METHODS 171
6.2.4 POLYMER DEPTH PROFILING WITH CLUSTER ION BEAMS 174 6.2.4.1 A BRIEF
DISCUSSION ON THE PHYSICS AND CHEMISTRY OF SPUTTERING AND ITS ROLE IN
OPTIMIZED BEAM CONDITIONS 180 6.2.5 3-D ANALYSIS IN POLYMER SYSTEMS 182
6.3 MATRIX-ASSISTED LASER DESORPTION LONIZATION (MALDI) 184 6.3.1
HISTORY OF MALDI IMAGING MASS SPECTROMETRY 184 6.3.2 SAMPLE PREPARATION
IN MALDI IMAGING 185 6.3.3 MALDI IMAGING OF POLYMERS 188
6.3.4 OUTLOOK 192
6.4 OTHER SURFACE MASS SPECTROMETRY METHODS 192 6.4.1 DESORPTION
ELECTROSPRAY LONIZATION 192 6.4.2 PLASMA DESORPTION LONIZATION METHODS
194 6.4.3 ELECTROSPRAY DROPLET IMPACT FOR SIMS 194 6.5 OUTLOOK 196
REFERENCES 296
7 HYPHENATED TECHNIQUES 209
JANA FALKENHAGEN AND STEFFEN WEIDNER 7.1 INTRODUCTION 209
7.2 POLYMER SEPARATION TECHNIQUES 210 7.3 PRINCIPLES OF COUPLING:
TRANSFER DEVICES 214 7.3.1 ONLINE COUPLING DEVICES 214 7.3.2 OFF-LINE
COUPLING DEVICES 218
7.4 EXAMPLES 220
7A.I COUPLING OF SEC WITH MALDI-/ESI-MS 220 7.4.2 COUPLING OF LAC/LC-CC
WITH MALDI-/ESI-MS 224 7.5 CONCLUSIONS 228
REFERENCES 228
8 AUTOMATED DATA PROCESSING AND QUANTIFICATION IN POLYMER MASS
SPECTROMETRY 237 TILL GRUENDLING, WILLIAM E. WALLACE, CHRISTOPHER
BARNER-KOWOLLIK, CHARLES M. GUTTMAN, AND ANTHONY J. KEARSLY 8.1
INTRODUCTION 237
8.2 FILE AND DATA FORMATS 237
8.3 OPTIMIZATION OF LONIZATION CONDITIONS 239 8.4 AUTOMATED SPECTRAL
ANALYSIS AND DATA REDUCTION IN MS 241 8.4.1 LONG-STANDING APPROACHES 242
8.4.2 SOME NEW CONCEPTS 243 8.4.3 MASS AUTOCORRELATION 243
IMAGE 5
CONTENTS IX
8.4.4 TIME-SERIES SEGMENTATION 245
8.5 COPOLYMER ANALYSIS 248
8.6 DATA INTERPRETATION IN MS/MS 251 8.7 QUANTITATIVE MS AND THE
DETERMINATION OF MMDS BY MS 252 8.7.1 QUANTITATIVE MMD MEASUREMENT BY
MALDI-MS 253 8.7.1.1 EXAMPLE FOR MIXTURES OF MONODISPERSE COMPONENTS 256
8.7.1.2 EXAMPLE FOR MIXTURES OF POLYDISPERSE COMPONENTS 257 8.7.1.3
CALCULATING THE CORRECTION FACTOR FOR EACH OLIGOMER 260 8.7.1.4 STEP BY
STEP PROCEDURE FOR QUANTISATION 261 8.7.1.5 DETERMINATION OF THE
ABSOLUTE MMD 262 8.7.2 QUANTITATIVE MMD MEASUREMENT BY SEC/ESI-MS 266
8.7.2.1 EXACT MEASUREMENT OF THE MMD OF HOMOPOLYMERS 266 8.7.2.2 MMD OF
THE INDIVIDUAL COMPONENTS IN MIXTURES OF FUNCTIONAL
HOMOPOLYMERS 270
8.7.3 COMPARISON OF THE TWO METHODS FOR MMD CALCULATION 273 8.7.4 SIMPLE
METHODS FOR THE DETERMINATION OF THE MOLAR ABUNDANCE OF FUNCTIONAL
POLYMERS IN MIXTURES 274 8.8 CONCLUSIONS AND OUTLOOK 276
REFERENCES 276
9 COMPREHENSIVE COPOLYMER CHARACTERIZATION 281 ANNA C. CRECELIUS AND
ULRICH S. SCHUBERT 9.1 INTRODUCTION 281
9.2 SCOPE 282
9.3 REVIEWS 282
9.4 SOFT LONIZATION TECHNIQUES 283 9.4.1 MALDI 283
9.4.2 ESI 292
9.4.3 APCI 294
9.5 SEPARATION PRIOR MS 297
9.5.1 LC-MS 297
9.5.2 ION MOBILITY SPECTROMETRY-MASS SPECTROMETRY (IMS-MS) 299 9.6
TANDEM MS (MS/MS) 301
9.7 QUANTITATIVE MS 303
9.8 COPOLYMERS FOR BIOLOGICAL OR (BIO)MEDICAL APPLICATION 304 9.9
SOFTWARE DEVELOPMENT 307 9.10 SUMMARY AND OUTLOOK 309 REFERENCES 309
10 ELUCIDATION OF REACTION MECHANISMS: CONVENTIONAL RADICAL
POLYMERIZATION 319 MICHAEL BUBACK, GREGORY T. RUSSELL, AND PHILIPP VANA
10.1 INTRODUCTION 319
10.2 BASIC PRINCIPLES AND GENERAL CONSIDERATIONS 320 10.3 INITIATION 321
IMAGE 6
X CONTENTS
10.3.1 RADICAL GENERATION 321
10.3.1.1 THERMALLY INDUCED INITIATOR DECOMPOSITION 321 10.3.1.2
PHOTOINDUCED INITIATOR DECOMPOSITION 331 10.3.1.3 OTHER MEANS 334 10.3.2
INITIATOR EFFICIENCY 335
10.4 PROPAGATION 335
10.4.1 PROPAGATION RATE COEFFICIENTS 336 10.4.2 CHAIN-LENGTH DEPENDENCE
OF PROPAGATION 340 10.4.3 COPOLYMERIZATION 342 10.5 TERMINATION 347
10.6 CHAIN TRANSFER 351
10.6.1 TRANSFER TO SMALL MOLECULES 351 10.6.2 ACRYLATE SYSTEMS 356 10.7
EMULSION POLYMERIZATION 364 10.8 CONCLUSION 365
REFERENCES 365
11 ELUCIDATION OF REACTION MECHANISMS AND POLYMER STRUCTURE:
LIVING/CONTROLLED RADICAL POLYMERIZATION 373 CHRISTOPHER
BARNER-KOWOLLIK, GUILLAUME DELAITTRE, TILL GRUENDLING, AND THOMAS
PAULOEHRL 11.1 PROTOCOLS BASED ON A PERSISTENT RADICAL EFFECT (NMP, ATRP,
AND RELATED) 374
11.2 PROTOCOLS BASED ON DEGENERATIVE CHAIN TRANSFER (RAFT, MADIX) 386
11.3 PROTOCOLS BASED ON CCT 393
11.4 NOVEL PROTOCOLS AND MINOR PROTOCOLS 397 11.5 CONCLUSIONS 398
REFERENCES 399
12 ELUCIDATION OF REACTION MECHANISMS: OTHER POLYMERIZATION MECHANISMS
405 GRAZYNA ADAMUS AND MAREK KOWALCZUK 12.1 INTRODUCTION 405
12.2 RING-OPENING POLYMERIZATION MECHANISMS OF CYCLIC ETHERS 406 12.3
RING-OPENING POLYMERIZATION MECHANISMS OF CYCLIC ESTERS AND CARBONATES
408 12.4 RING-OPENING METATHESIS POLYMERIZATION 423
12.5 MECHANISMS OF STEP-GROWTH POLYMERIZATION 425 12.6 CONCLUDING
REMARKS 430 REFERENCES 431
13 POLYMER DEGRADATION 437
PAOLA RIZZARELLI, SABRINA CARROCCIO, AND CONCETTO PUGLISI 13.1
INTRODUCTION 437
13.2 THERMAL AND THERMO-OXIDATIVE DEGRADATION 438
IMAGE 7
CONTENTS XI
13.3 PHOTOLYSIS AND PHOTOOXIDATION 449
13.4 BIODEGRADATION 454
13.5 OTHER DEGRADATION PROCESSES 455 13.6 CONCLUSIONS 457
REFERENCES 461
14 OUTLOOK 467
CHRISTOPHER BARNER-KOWOLLIK, JANA FALKENHAGEN, TILL GRUENDLING, AND
STEFFEN WEIDNER
INDEX 469 |
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| id | DE-604.BV039764091 |
| illustrated | Illustrated |
| indexdate | 2024-07-21T00:18:57Z |
| institution | BVB |
| isbn | 9783527641826 9783527641857 9783527329243 3527329242 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-024625212 |
| oclc_num | 769467702 |
| open_access_boolean | |
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| owner_facet | DE-11 DE-703 DE-92 DE-526 DE-91G DE-BY-TUM DE-19 DE-BY-UBM |
| physical | XV, 483 S. Ill., graph. Darst. |
| publishDate | 2012 |
| publishDateSearch | 2012 |
| publishDateSort | 2012 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Mass spectrometry in polymer chemistry ed. by Christopher Barner-Kowollik ... Weinheim Wiley-VCH 2012 XV, 483 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Massenspektrometrie (DE-588)4037882-2 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Polymere (DE-588)4046699-1 s Massenspektrometrie (DE-588)4037882-2 s DE-604 Barner-Kowollik, Christopher 1973- (DE-588)121637514 edt X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3830296&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024625212&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Mass spectrometry in polymer chemistry Massenspektrometrie (DE-588)4037882-2 gnd Polymere (DE-588)4046699-1 gnd |
| subject_GND | (DE-588)4037882-2 (DE-588)4046699-1 |
| title | Mass spectrometry in polymer chemistry |
| title_auth | Mass spectrometry in polymer chemistry |
| title_exact_search | Mass spectrometry in polymer chemistry |
| title_full | Mass spectrometry in polymer chemistry ed. by Christopher Barner-Kowollik ... |
| title_fullStr | Mass spectrometry in polymer chemistry ed. by Christopher Barner-Kowollik ... |
| title_full_unstemmed | Mass spectrometry in polymer chemistry ed. by Christopher Barner-Kowollik ... |
| title_short | Mass spectrometry in polymer chemistry |
| title_sort | mass spectrometry in polymer chemistry |
| topic | Massenspektrometrie (DE-588)4037882-2 gnd Polymere (DE-588)4046699-1 gnd |
| topic_facet | Massenspektrometrie Polymere |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=3830296&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=024625212&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT barnerkowollikchristopher massspectrometryinpolymerchemistry |