A new approach to industrial melt crystallization of acrylic acid:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Aachen
Shaker
2010
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | VI, 208 S. Ill., graph. Darst. |
| ISBN: | 9783832295011 |
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Record in the Search Index
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| adam_text | TABLE OF CONTENTS CHAPTER 1 INTRODUCTION 1.1 INDUSTRIAL NEEDS AND
ADVANTAGES OF MELT CRYSTALLIZATION 1 1.2 MELT CRYSTALLIZATION 2 1.2.1
SOLID-LIQUID EQUILIBRIUM 3 1.2.2 INDUSTRIAL CRYSTALLIZATION TECHNIQUES 4
1.2.3 DRIVING FORCE FOR MELT CRYSTALLIZATION 7 1.3 CRYSTAL GROWTH 8
1.3.1 GROWTH MECHANISMS IN SUSPENSION 8 1.3.2 GROWTH RATES 10 1.4
SOLID-LIQUID SEPARATION AND CRYSTAL PURIFICATION IN SUSPENSION
CRYSTALLIZATION 11 1.4.1 WASH COLUMNS 13 1.5 THE SYSTEM ACRYLIC ACID 14
1.5.1 PHYSICAL PROPERTIES 15 1.5.2 SOLID-LIQUID PHASE DIAGRAM ACRYLIC
ACID AND WATER 16 1.6 OBJECTIVES 17 1.7 OUTLINE OF THE THESIS 19
NOMENCLATURE 21 REFERENCES 23 CHAPTER 2 INFLUENCE OF SUPERCOOLING AND
WATER CONTENT ON CRYSTAL MORPHOLOGY OF ACRYLIC ACID ABSTRACT 27 2.1
INTRODUCTION 28 2.2 STATE OF KNOWLEDGE 28 2.2.1 ACRYLIC ACID CRYSTAL
STRUCTURE 28 2.2.2 CHEMICAL COMPOSITION OF THE FACES 29 2.2.3 MORPHOLOGY
DEVELOPMENT IN PRESENCE OF WATER 31 2.2.4 EXTENSION OF THE THEORY FOR
SURFACE INTEGRATION PROCESSES 32 2.2.5 PREDICTION OF CRYSTAL FACE GROWTH
RATES 37 2.3 EXPERIMENTAL 38 2.3.1 EQUIPMENT AND SETUP 38 I
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1007745991 DIGITALISIERT
DURCH TABLE OF CONTENTS 2.3.2 EXPERIMENTAL PROCEDURE 39 2.3.3
EXPERIMENTAL RESULTS 40 2.3.4 DISCUSSION OF EVALUATED RESULTS 43 2.4
CRYSTAL MORPHOLOGY DEVELOPMENT - A QUALITATIVE APPROACH 44 2.4.1 GROWTH
RATE ANALYSIS AND MODELING 45 2.4.2 CAVITY ANGLE ANALYSIS 47 2.5
CONCLUSION 48 NOMENCLATURE 49 REFERENCES 51 CHAPTER 3 THE INFLUENCE OF
WATER AND SUPERCOOLING ON PERMEABILITY AND COMPRESSIBILITY OF ACRYLIC
ACID CRYSTAL BEDS ABSTRACT 55 3.1 INTRODUCTION 56 3.2 STATE OF KNOWLEDGE
56 3.2.1 PERMEABILITY MODEL FOR SPHERICAL PARTICLES 57 3.2.2 EXTENDED
INPUT TO THE PERMEABILITY CALCULATIONS FOR NONSPHERICAL PARTICLES 60 3.3
PERMEABILITY MODEL FOR NONSPHERICAL PARTICLES 61 3.4 EXPERIMENTAL 63
3.4.1 APPARATUS AND SETUP 63 3.4.2 CRYSTAL PROPERTY MEASUREMENTS 65
3.4.3 EXPERIMENTAL PROCEDURE 67 3.5 RESULTS 67 3.5.1 SUPERCOOLING 67
3.5.2 CLD MEASUREMENT 68 3.5.3 FILTRATION RESULTS 70 3.5.4
COMPRESSIBILITY 71 3.6 MODELING RESULTS 72 3.6.1 GROWTH RATES 73 3.6.2
POROSITY 74 3.6.3 SPECIFIC SURFACE 74 3.6.4 PERMEABILITY 75 3.7
DISCUSSION 76 3.8 CONCLUSIONS AND OUTLOOK 77 NOMENCLATURE 78 REFERENCES
81 II TABLE OF CONTENTS CHAPTER 4 COMPRESSIBILITY IMPROVEMENT OF AN
ACRYLIC ACID CRYSTAL BED BY THE IN- SITU FORMATION OF ICE CRYSTALS
ABSTRACT 85 4.1 INTRODUCTION 86 4.2 STATE OF KNOWLEDGE ABOUT EUTECTIC
FREEZING 86 4.3 APPROACH TO FILTRATION IMPROVEMENT 89 4.3.1 QUALITATIVE
APPROACH TO POROSITY IMPROVEMENT WITH AN N-SITU FORMED FILTER AID
....89 4.3.2 DATA ESTIMATION OF AN ACRYLIC ACID CRYSTAL BED NEAR
EUTECTIC COMPOSITION 90 4.3.3 THEORETICAL ESTIMATION OF THE POROSITY OF
NONSPHERICAL PARTICLES MIXTURES 94 4.4 EXPERIMENTAL 99 4.4.1 OBJECTIVES
99 4.4.2 EXPERIMENTAL SETUP AND PROCEDURE 99 4.4.3 EXPERIMENTS 101 4.4.4
RESULTS 102 4.5 DISCUSSION AND OUTLOOK 107 4.6 CONCLUSION 108
NOMENCLATURE 110 REFERENCES 112 CHAPTER 5 SOLVENT SCREENING AND
MEASUREMENT OF PHASE DIAGRAMS FOR THE YIELD MAXIMIZATION OF AN ACRYLIC
ACID CRYSTALLIZATION ABSTRACT 115 5.1 INTRODUCTION 116 5.2 SOLID-LIQUID
EQUILIBRIUM 116 5.2.1 THEORETICAL PREDICTION OF A SOLID-LIQUID PHASE
EQUILIBRIUM 116 5.2.2 THERMAL ANALYSIS METHODS FOR DETERMINATION OF
THERMODYNAMICAL PROPERTIES ....120 5.2.3 DETERMINATION OF THE BINARY
EUTECTIC POINT AND EQUILIBRIUM DIAGRAM 121 5.2.4 APPROACH TO DETERMINE
THE TERNARY EUTECTIC POINT AND SOLID-LIQUID EQUILIBRIUM ...123 5.3
APPROACH TO A FAST SOLVENT SCREENING METHOD 125 5.3.1 APPROACH TO A DATA
BASE REQUEST FOR FAST SOLVENT SCREENING 125 5.3. TABLE OF CONTENTS 5.4.2
EXPERIMENTAL SETUP AND PROCEDURE 130 5.4.3 RESULTS 130 5.5 DISCUSSION
136 5.6 CONCLUSION AND OUTLOOK 137 NOMENCLATURE 139 REFERENCES 141
APPENDIX 143 CHAPTER 6 BENCH MARK STUDY FOR A NOVEL ACRYLIC ACID
RECOVERY ABSTRACT 147 6.1 INTRODUCTION 148 6.2 STATE OF KNOWLEDGE 148
6.2.1 REACTION - ACRYLIC ACID FROM PROPENE 148 6.2.2 RECOVERY OF ACRYLIC
ACID 150 6.3 SIMULATION 152 6.3.1 SIMULATION TOOL 152 6.3.2 SIMULATION
OF CRYSTALLIZATION UNITS 152 6.3.3 SPECIFICATION OF UTILITIES 153 6.3.4
SIMULATION MARGIN AND FEED COMPOSITION 153 6.3.5 CONVENTIONAL ACRYLIC
ACID RECOVERY PROCESS 154 6.3.6 NOVEL ACRYLIC AID RECOVERY PROCESS USING
EUTECTIC CRYSTALLIZATION 157 6.4 RESULTS 159 6.4.1 HEAT BALANCE 162
6.4.2 DIMENSION OF MAIN PROCESS UNITS 166 6.4.3 RESULT SUMMARY 170 6.5
DISCUSSION 171 6.6 CONCLUSION AND OUTLOOK 172 NOMENCLATURE 174
REFERENCES 176 IV TABLE OF CONTENTS APPENDIX ENGLISH SUMMARY 181
NEDERLANDSE SAMENVATTING 187 GERMAN SUMMARY 193 ACKNOWLEDGEMENTS 199
CURRICULUM VITAE 203 PATENT APPLICATION - WO2009130085A1 207 V
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| author | Hengstermann, Axel 1978- |
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| dewey-full | 661.86 660.284298 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 661 - Technology of industrial chemicals 660 - Chemical engineering |
| dewey-raw | 661.86 660.284298 |
| dewey-search | 661.86 660.284298 |
| dewey-sort | 3661.86 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| spelling | Hengstermann, Axel 1978- Verfasser (DE-588)14285932X aut A new approach to industrial melt crystallization of acrylic acid Axel Hengstermann Aachen Shaker 2010 VI, 208 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Zugl.: Delft, Techn. Univ., Diss., 2010 Schmelzkristallisation (DE-588)4243444-0 gnd rswk-swf Prozessentwicklung Technik (DE-588)4278925-4 gnd rswk-swf Acrylsäure (DE-588)4141321-0 gnd rswk-swf Suspension (DE-588)4058671-6 gnd rswk-swf Produktaufarbeitung (DE-588)4310202-5 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Acrylsäure (DE-588)4141321-0 s Produktaufarbeitung (DE-588)4310202-5 s Suspension (DE-588)4058671-6 s Schmelzkristallisation (DE-588)4243444-0 s Prozessentwicklung Technik (DE-588)4278925-4 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022533660&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hengstermann, Axel 1978- A new approach to industrial melt crystallization of acrylic acid Schmelzkristallisation (DE-588)4243444-0 gnd Prozessentwicklung Technik (DE-588)4278925-4 gnd Acrylsäure (DE-588)4141321-0 gnd Suspension (DE-588)4058671-6 gnd Produktaufarbeitung (DE-588)4310202-5 gnd |
| subject_GND | (DE-588)4243444-0 (DE-588)4278925-4 (DE-588)4141321-0 (DE-588)4058671-6 (DE-588)4310202-5 (DE-588)4113937-9 |
| title | A new approach to industrial melt crystallization of acrylic acid |
| title_auth | A new approach to industrial melt crystallization of acrylic acid |
| title_exact_search | A new approach to industrial melt crystallization of acrylic acid |
| title_full | A new approach to industrial melt crystallization of acrylic acid Axel Hengstermann |
| title_fullStr | A new approach to industrial melt crystallization of acrylic acid Axel Hengstermann |
| title_full_unstemmed | A new approach to industrial melt crystallization of acrylic acid Axel Hengstermann |
| title_short | A new approach to industrial melt crystallization of acrylic acid |
| title_sort | a new approach to industrial melt crystallization of acrylic acid |
| topic | Schmelzkristallisation (DE-588)4243444-0 gnd Prozessentwicklung Technik (DE-588)4278925-4 gnd Acrylsäure (DE-588)4141321-0 gnd Suspension (DE-588)4058671-6 gnd Produktaufarbeitung (DE-588)4310202-5 gnd |
| topic_facet | Schmelzkristallisation Prozessentwicklung Technik Acrylsäure Suspension Produktaufarbeitung Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022533660&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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