Verfügbarkeit: Challenges in analytical quality assurance

Challenges in analytical quality assurance:

Gespeichert in:

Bibliographische Detailangaben
Hauptverfasser:	Reichenbächer, Manfred 1941- (VerfasserIn), Einax, Jürgen 1949- (VerfasserIn)
Format:	Buch
Sprache:	English
Veröffentlicht:	Heidelberg [u.a.] Springer 2011
Schlagworte:	Messfehler Analytische Chemie Methode Qualitative Analyse Qualitätskontrolle Statistischer Test Fehleranalyse
Online-Zugang:	Inhaltstext Inhaltsverzeichnis
Beschreibung:	XIX, 356 S. graph. Darst.
ISBN:	9783642165948 364216594X

Internformat

MARC


LEADER	00000nam a2200000 c 4500
001	BV037329076
003	DE-604
005	20120802
007	t
008	110408s2011 d\|\|\| \|\|\|\| 00\|\|\| eng d
016	7		\|a 1006975799 \|2 DE-101
020			\|a 9783642165948 \|9 978-3-642-16594-8
020			\|a 364216594X \|9 3-642-16594-X
035			\|a (OCoLC)838103023
035			\|a (DE-599)DNB1006975799
040			\|a DE-604 \|b ger \|e rakddb
041	0		\|a eng
049			\|a DE-11 \|a DE-19 \|a DE-634 \|a DE-Er8
082	0		\|a 543.015195 \|2 22/ger
084			\|a VG 5000 \|0 (DE-625)147169: \|2 rvk
084			\|a VG 5100 \|0 (DE-625)147179: \|2 rvk
084			\|a 540 \|2 sdnb
100	1		\|a Reichenbächer, Manfred \|d 1941- \|e Verfasser \|0 (DE-588)108842509 \|4 aut
245	1	0	\|a Challenges in analytical quality assurance \|c Manfred Reichenbächer ; Jürgen W. Einax
264		1	\|a Heidelberg [u.a.] \|b Springer \|c 2011
300			\|a XIX, 356 S. \|b graph. Darst.
336			\|b txt \|2 rdacontent
337			\|b n \|2 rdamedia
338			\|b nc \|2 rdacarrier
650	0	7	\|a Messfehler \|0 (DE-588)4133270-2 \|2 gnd \|9 rswk-swf
650	0	7	\|a Analytische Chemie \|0 (DE-588)4129906-1 \|2 gnd \|9 rswk-swf
650	0	7	\|a Methode \|0 (DE-588)4038971-6 \|2 gnd \|9 rswk-swf
650	0	7	\|a Qualitative Analyse \|0 (DE-588)4115680-8 \|2 gnd \|9 rswk-swf
650	0	7	\|a Qualitätskontrolle \|0 (DE-588)4047968-7 \|2 gnd \|9 rswk-swf
650	0	7	\|a Statistischer Test \|0 (DE-588)4077852-6 \|2 gnd \|9 rswk-swf
650	0	7	\|a Fehleranalyse \|0 (DE-588)4016608-9 \|2 gnd \|9 rswk-swf
689	0	0	\|a Analytische Chemie \|0 (DE-588)4129906-1 \|D s
689	0	1	\|a Qualitätskontrolle \|0 (DE-588)4047968-7 \|D s
689	0	2	\|a Fehleranalyse \|0 (DE-588)4016608-9 \|D s
689	0	3	\|a Statistischer Test \|0 (DE-588)4077852-6 \|D s
689	0		\|5 DE-604
689	1	0	\|a Analytische Chemie \|0 (DE-588)4129906-1 \|D s
689	1	1	\|a Qualitative Analyse \|0 (DE-588)4115680-8 \|D s
689	1	2	\|a Messfehler \|0 (DE-588)4133270-2 \|D s
689	1	3	\|a Methode \|0 (DE-588)4038971-6 \|D s
689	1		\|8 1\p \|5 DE-604
700	1		\|a Einax, Jürgen \|d 1949- \|e Verfasser \|0 (DE-588)1030500622 \|4 aut
856	4	2	\|m X:MVB \|q text/html \|u http://deposit.dnb.de/cgi-bin/dokserv?id=3537170&prov=M&dok_var=1&dok_ext=htm \|3 Inhaltstext
856	4	2	\|m DNB Datenaustausch \|q application/pdf \|u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022483051&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA \|3 Inhaltsverzeichnis
883	1		\|8 1\p \|a cgwrk \|d 20201028 \|q DE-101 \|u https://d-nb.info/provenance/plan#cgwrk
943	1		\|a oai:aleph.bib-bvb.de:BVB01-022483051

Datensatz im Suchindex

_version_	1805095803283308544
adam_text	IMAGE 1 CONTENTS 1 INTRODUCTION 1 REFERENCES 6 2 TYPES OF ERRORS IN INSTRUMENTAL ANALYSIS 7 2.1 OVERVIEW 7 2.2 RANDOM ERRORS 10 2.2.1 DISTRIBUTION OF MEASURED VALUES 10 2.2.2 STANDARD DEVIATION 16 2.2.3 CONFIDENCE INTERVAL 19 2.2.4 CONFIDENCE INTERVAL AND QUALITY 22 2.2.5 PROPAGATION OF ERRORS 26 REFERENCES 35 3 STATISTICAL TESTS 37 3. 1 GENERAL REMARKS 37 3.2 TESTS FOR SERIES OF MEASUREMENTS 39 3.2.1 RAPID TEST FOR NORMAL DISTRIBUTION (DAVID TEST) 40 3.2.2 TEST FOR A TREND 40 3.2.3 TEST FOR OUTLIERS 43 3.3 COMPARISON OF TWO STANDARD DEVIATIONS 51 3.4 COMPARISON OF MORE THAN TWO STANDARD DEVIATIONS 56 3.5 COMPARISON OF TWO MEAN VALUES 59 3.6 COMPARISON OF MORE THAN TWO MEAN VALUES: ANALYSIS OF VARIANCE 67 REFERENCES 76 4 GENERAL ASPECTS OF LINEAR REGRESSION 79 4.1 CORRELATION, REGRESSION, AND CALIBRATION 79 4.2 LINEAR CALIBRATION MODEL 83 4.3 SIMPLIFICATION OF THE LINEAR CALIBRATION FUNCTION 100 4.4 QUADRATIC REGRESSION ANALYSIS 103 BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1006975799 DIGITALISIERT DURCH IMAGE 2 XII CONTENTS 4.5 WORKING RANGE AND CALIBRATION STANDARDS 108 REFERENCES 116 5 VALIDATION OF METHOD PERFORMANCE 117 5.1 GENERAL REMARKS 117 5.2 PRECISION 118 5.3 LINEARITY OF CALIBRATION LINES 132 5.3.1 GENERAL REMARKS 132 5.3.2 QUALITY COEFFICIENT 132 5.3.3 VISUAL EXAMINATIONS 134 5.3.4 MANDELTEST 136 5.3.5 THE LACK-OF-FIT TEST BY ANOVA 138 5.3.6 TEST OF THE SIGNIFICANCE OF THE QUADRATIC REGRESSION COEFFICIENT A 2 143 5.4 TEST FOR OUTLIERS IN THE LINEAR REGRESSION FUNCTION 146 5.5 HOMOGENEITY OF VARIANCES 155 5.6 WEIGHTED LINEAR LEAST SQUARES REGRESSION 160 5.7 TESTS FOR TRUENESS 166 5.7.1 SYSTEMATIC ERRORS IN THE LEAST SQUARES REGRESSION PROCEDURE 166 5.7.2 MEAN VALUE I-TEST 167 5.7.3 RECOVERYRATE 169 5.7.4 RECOVERY RATE OF STOCKED SAMPLES 172 5.7.5 RECOVERY FUNCTION 174 5.7.6 STANDARD ADDITION PROCEDURE 179 5.7.7 TEST BY METHOD COMPARISON 184 5.7.8 STANDARD ADDITION METHOD 202 5.8 LIMIT OF DETECTION AND LIMIT OF QUANTIFICATION 206 5.9 ROBUSTNESS, RUGGEDNESS 218 5.10 APPLICATION OF METHOD VALIDATION 226 REFERENCES 237 6 ASPECTS OF METHOD DEVELOPMENT 241 6.1 GENERAL REMARKS 241 6.2 SELECTIVITY AND SPECIFICITY 247 6.3 METHOD DEVELOPMENT OF HEADSPACE GAS CHROMATOGRAPHY 251 REFERENCES 267 7 PERFORMANCE VERIFICATION OF ANALYTICAL INSTRUMENTS AND TOOLS: SELECTED EXAMPLES 269 7.1 GENERAL REMARKS ON QUALIFICATION AND PERFORMANCE VERIFICATION OF LABORATORY INSTRUMENTS 269 7.2 UV-VIS SPECTROPHOTOMETERS 270 7.2.1 WAVELENGTH ACCURACY 270 7.2.2 STRAY LIGHT 271 IMAGE 3 CONTENTS XIII 7.2.3 RESOLUTION 272 7.2.4 PHOTOMETRIC ACCURACY 273 7.3 HPLC INSTRUMENTS 279 7.4 BALANCES 284 REFERENCES 285 8 CONTROL CHARTS IN THE ANALYTICAL LABORATORY 287 8.1 QUALITY CONTROL 287 8.2 SHEWHART CHARTS 288 8.3 CUSUMCHARTS 298 REFERENCES 304 9 INTERLABORATORY STUDIES 305 9.1 PURPOSE AND TYPES OF INTERLABORATORY STUDIES 305 9.2 METHOD PERFORMANCE STUDIES 306 9.3 PROFICIENCY TESTING 312 REFERENCES 317 10 MEASUREMENT UNCERTAINTY 319 10.1 PURPOSE, DEFINITIONS, AND TERMINOLOGY 319 10.2 STEPS IN MEASUREMENT UNCERTAINTY ESTIMATION 321 10.3 SPREADSHEET METHOD FOR UNCERTAINTY CALCULATION 325 10.4 PROCEDURE OF THE NORDTEST REPORT 333 REFERENCES 342 APPENDIX 345 INDEX 353
any_adam_object	1
author	Reichenbächer, Manfred 1941- Einax, Jürgen 1949-
author_GND	(DE-588)108842509 (DE-588)1030500622
author_facet	Reichenbächer, Manfred 1941- Einax, Jürgen 1949-
author_role	aut aut
author_sort	Reichenbächer, Manfred 1941-
author_variant	m r mr j e je
building	Verbundindex
bvnumber	BV037329076
classification_rvk	VG 5000 VG 5100
ctrlnum	(OCoLC)838103023 (DE-599)DNB1006975799
dewey-full	543.015195
dewey-hundreds	500 - Natural sciences and mathematics
dewey-ones	543 - Analytical chemistry
dewey-raw	543.015195
dewey-search	543.015195
dewey-sort	3543.015195
dewey-tens	540 - Chemistry and allied sciences
discipline	Chemie / Pharmazie
format	Book
fullrecord	<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>00000nam a2200000 c 4500</leader><controlfield tag="001">BV037329076</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20120802</controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">110408s2011 d\|\|\| \|\|\|\| 00\|\|\| eng d</controlfield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">1006975799</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9783642165948</subfield><subfield code="9">978-3-642-16594-8</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">364216594X</subfield><subfield code="9">3-642-16594-X</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)838103023</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)DNB1006975799</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakddb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-11</subfield><subfield code="a">DE-19</subfield><subfield code="a">DE-634</subfield><subfield code="a">DE-Er8</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">543.015195</subfield><subfield code="2">22/ger</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VG 5000</subfield><subfield code="0">(DE-625)147169:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VG 5100</subfield><subfield code="0">(DE-625)147179:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">540</subfield><subfield code="2">sdnb</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Reichenbächer, Manfred</subfield><subfield code="d">1941-</subfield><subfield code="e">Verfasser</subfield><subfield code="0">(DE-588)108842509</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Challenges in analytical quality assurance</subfield><subfield code="c">Manfred Reichenbächer ; Jürgen W. Einax</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Heidelberg [u.a.]</subfield><subfield code="b">Springer</subfield><subfield code="c">2011</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XIX, 356 S.</subfield><subfield code="b">graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Messfehler</subfield><subfield code="0">(DE-588)4133270-2</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Analytische Chemie</subfield><subfield code="0">(DE-588)4129906-1</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Methode</subfield><subfield code="0">(DE-588)4038971-6</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Qualitative Analyse</subfield><subfield code="0">(DE-588)4115680-8</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Qualitätskontrolle</subfield><subfield code="0">(DE-588)4047968-7</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Statistischer Test</subfield><subfield code="0">(DE-588)4077852-6</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Fehleranalyse</subfield><subfield code="0">(DE-588)4016608-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Analytische Chemie</subfield><subfield code="0">(DE-588)4129906-1</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Qualitätskontrolle</subfield><subfield code="0">(DE-588)4047968-7</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="2"><subfield code="a">Fehleranalyse</subfield><subfield code="0">(DE-588)4016608-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="3"><subfield code="a">Statistischer Test</subfield><subfield code="0">(DE-588)4077852-6</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="689" ind1="1" ind2="0"><subfield code="a">Analytische Chemie</subfield><subfield code="0">(DE-588)4129906-1</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="1"><subfield code="a">Qualitative Analyse</subfield><subfield code="0">(DE-588)4115680-8</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="2"><subfield code="a">Messfehler</subfield><subfield code="0">(DE-588)4133270-2</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="3"><subfield code="a">Methode</subfield><subfield code="0">(DE-588)4038971-6</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2=" "><subfield code="8">1\p</subfield><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Einax, Jürgen</subfield><subfield code="d">1949-</subfield><subfield code="e">Verfasser</subfield><subfield code="0">(DE-588)1030500622</subfield><subfield code="4">aut</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">X:MVB</subfield><subfield code="q">text/html</subfield><subfield code="u">http://deposit.dnb.de/cgi-bin/dokserv?id=3537170&prov=M&dok_var=1&dok_ext=htm</subfield><subfield code="3">Inhaltstext</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022483051&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="883" ind1="1" ind2=" "><subfield code="8">1\p</subfield><subfield code="a">cgwrk</subfield><subfield code="d">20201028</subfield><subfield code="q">DE-101</subfield><subfield code="u">https://d-nb.info/provenance/plan#cgwrk</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-022483051</subfield></datafield></record></collection>
id	DE-604.BV037329076
illustrated	Illustrated
indexdate	2024-07-20T11:05:04Z
institution	BVB
isbn	9783642165948 364216594X
language	English
oai_aleph_id	oai:aleph.bib-bvb.de:BVB01-022483051
oclc_num	838103023
open_access_boolean
owner	DE-11 DE-19 DE-BY-UBM DE-634 DE-Er8
owner_facet	DE-11 DE-19 DE-BY-UBM DE-634 DE-Er8
physical	XIX, 356 S. graph. Darst.
publishDate	2011
publishDateSearch	2011
publishDateSort	2011
publisher	Springer
record_format	marc
spelling	Reichenbächer, Manfred 1941- Verfasser (DE-588)108842509 aut Challenges in analytical quality assurance Manfred Reichenbächer ; Jürgen W. Einax Heidelberg [u.a.] Springer 2011 XIX, 356 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Messfehler (DE-588)4133270-2 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Methode (DE-588)4038971-6 gnd rswk-swf Qualitative Analyse (DE-588)4115680-8 gnd rswk-swf Qualitätskontrolle (DE-588)4047968-7 gnd rswk-swf Statistischer Test (DE-588)4077852-6 gnd rswk-swf Fehleranalyse (DE-588)4016608-9 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s Qualitätskontrolle (DE-588)4047968-7 s Fehleranalyse (DE-588)4016608-9 s Statistischer Test (DE-588)4077852-6 s DE-604 Qualitative Analyse (DE-588)4115680-8 s Messfehler (DE-588)4133270-2 s Methode (DE-588)4038971-6 s 1\p DE-604 Einax, Jürgen 1949- Verfasser (DE-588)1030500622 aut X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3537170&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022483051&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk
spellingShingle	Reichenbächer, Manfred 1941- Einax, Jürgen 1949- Challenges in analytical quality assurance Messfehler (DE-588)4133270-2 gnd Analytische Chemie (DE-588)4129906-1 gnd Methode (DE-588)4038971-6 gnd Qualitative Analyse (DE-588)4115680-8 gnd Qualitätskontrolle (DE-588)4047968-7 gnd Statistischer Test (DE-588)4077852-6 gnd Fehleranalyse (DE-588)4016608-9 gnd
subject_GND	(DE-588)4133270-2 (DE-588)4129906-1 (DE-588)4038971-6 (DE-588)4115680-8 (DE-588)4047968-7 (DE-588)4077852-6 (DE-588)4016608-9
title	Challenges in analytical quality assurance
title_auth	Challenges in analytical quality assurance
title_exact_search	Challenges in analytical quality assurance
title_full	Challenges in analytical quality assurance Manfred Reichenbächer ; Jürgen W. Einax
title_fullStr	Challenges in analytical quality assurance Manfred Reichenbächer ; Jürgen W. Einax
title_full_unstemmed	Challenges in analytical quality assurance Manfred Reichenbächer ; Jürgen W. Einax
title_short	Challenges in analytical quality assurance
title_sort	challenges in analytical quality assurance
topic	Messfehler (DE-588)4133270-2 gnd Analytische Chemie (DE-588)4129906-1 gnd Methode (DE-588)4038971-6 gnd Qualitative Analyse (DE-588)4115680-8 gnd Qualitätskontrolle (DE-588)4047968-7 gnd Statistischer Test (DE-588)4077852-6 gnd Fehleranalyse (DE-588)4016608-9 gnd
topic_facet	Messfehler Analytische Chemie Methode Qualitative Analyse Qualitätskontrolle Statistischer Test Fehleranalyse
url	http://deposit.dnb.de/cgi-bin/dokserv?id=3537170&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=022483051&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT reichenbachermanfred challengesinanalyticalqualityassurance AT einaxjurgen challengesinanalyticalqualityassurance

Verfügbarkeit

Es ist kein Print-Exemplar vorhanden.

Fernleihe Bestellen Achtung: Nicht im THWS-Bestand! Beschreibung

MARC

Datensatz im Suchindex

Es ist kein Print-Exemplar vorhanden.

Ähnliche Einträge