Confocal Raman microscopy:
Saved in:
| Other Authors: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Berlin [u.a.]
Springer
2010
|
| Series: | Springer series in optical sciences
158 |
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XV, 289 S. Ill., graph. Darst. |
| ISBN: | 9783642125218 9783642125225 |
Staff View
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Record in the Search Index
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IMAGE 1
CONTENTS
1 HIGH-RESOLUTION OPTICAL AND CONFOCAL MICROSCOPY 1
OLAF HOLLRICHER AND WOLFRAM IBACH 1.1 INTRODUCTION 1
1.2 INTRODUCTION TO THEORETICAL CONSIDERATIONS IN HIGH-RESOLUTION
MICROSCOPY 3
1.3 INTRODUCTION TO CONFOCAL MICROSCOPY 3
1.4 ELECTROMAGNETIC SCATTERING IN OPTICAL SYSTEMS 4
1.5 3D-INTENSITY DISTRIBUTION IN THE FOCUS 5
1.5.1 LARGE APERTURE ANGLES 6
1.5.2 TRANSITION TO SMALL APERTURE ANGLES 9
1.6 THEORY OF IMAGE FORMATION 11
1.6.1 MICROSCOPE 11
1.6.2 CONFOCAL MICROSCOPE 12
1.6.3 CONFOCAL RAMAN MICROSCOPE 12
1.7 IMAGE FORMATION FOR LIGHT SCATTERING 13
1.7.1 SCATTERING POINT 13
1.7.2 REFLECTION AT A MIRROR 15
1.8 IMAGE FORMATION FOR RAMAN SCATTERING 16
1.8.1 RAMAN EMITTING POINT 16
1.8.2 RAMAN EMISSION OF A LAYER 17
1.9 PINHOLE SIZE 18
REFERENCES 20
2 INTRODUCTION TO THE FUNDAMENTALS OF RAMAN SPECTROSCOPY 21 BENJAMIN
DIETZEK, DANA CIALLA, MICHAEL SCHMITT, AND JUERGEN POPP 2.1 INTRODUCTION
21
2.2 CLASSICAL PICTURE OF LIGHT SCATTERING 22
2.2.1 FREQUENCY DEPENDENCE OF RAMAN SCATTERING 22 2.2.2 CLASSICAL
"SELECTION RULE" AND COMPARISON TO IR ABSORPTION 24
2.2.3 SCATTERED RAMAN INTENSITY 25
2.2.4 SHORTFALLS OF THE CLASSICAL PICTURE 27
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/1002586658
DIGITALISIERT DURCH
IMAGE 2
VIII CONTENTS
2.3 RAMAN CROSS-SECTION ENHANCEMENT MECHANISMS 27
2.3.1 RESONANT RAMAN SCATTERING 28
2.3.2 ADVANTAGES AND APPLICATIONS OF RESONANCE RAMAN SCATTERING 31
2.3.3 SURFACE-ENHANCED RAMAN SCATTERING 34
REFERENCES 40
3 RAMAN INSTRUMENTATION FOR CONFOCAL RAMAN MICROSCOPY 43 OLAFHOLLRICHER
3.1 INTRODUCTION 43
3.2 THE DEVELOPMENT OF RAMAN MICROSCOPES 44
3.3 CONFOCALITY 45
3.4 THROUGHPUT OF A CONFOCAL RAMAN MICROSCOPE 46
3.4.1 LASER WAVELENGTH 47
3.4.2 EXCITATION POWER 47
3.4.3 OBJECTIVE 48
3.4.4 MICROSCOPE THROUGHPUT 48
3.4.5 COUPLING BETWEEN MICROSCOPE AND SPECTROMETER 49 3.4.6 SPECTROMETER
THROUGHPUT 49
3.4.7 GRATINGS 50
3.4.8 CCD DETECTOR 51
3.5 CONCLUSION 60
REFERENCES 60
4 SOFTWARE REQUIREMENTS AND DATA ANALYSIS IN CONFOCAL RAMAN MICROSCOPY
61
THOMAS DIEING AND WOLFRAM IBACH 4.1 INTRODUCTION 61
4.2 REQUIREMENTS FOR DATA ACQUISITION SOFTWARE 62
4.2.1 DATA ACQUISITION 62
4.2.2 CORRELATION OF SPATIAL AND SPECTRAL DATA 63
4.3 DESCRIPTION OF THE DATA SETS ACQUIRED IN CONFOCAL RAMAN MICROSCOPY
65
4.4 PRE-PROCESSING OF RAMAN SPECTRA 66
4.4.1 COSMIC RAY REMOVAL 66
4.4.2 SMOOTHING 68
4.4.3 BACKGROUND SUBSTRACTION AND SUBTRACTION OF REFERENCE SPECTRA 70
4.5 IMAGE GENERATION 72
4.5.1 UNIVARIATE IMAGE GENERATION 72
4.5.2 MULTIVARIATE IMAGE GENERATION 75
4.6 IMAGE MASKS AND SELECTIVE AVERAGE CALCULATION 81
4.7 COMBINATION OF SINGLE SPECTRA WITH MULTI-SPECTRAL DATA SETS 82 4.7.1
BASIS SPECTRA 83
4.7.2 FITTING PROCEDURE 83
IMAGE 3
CONTENTS
4.8 COMBINATION OF VARIOUS IMAGES 84
4.9 THE LAW OF NUMBERS 85
4.10 MATERIALS AND METHODS 88
REFERENCES 89
5 NANO-SPECTROSCOPY OF INDIVIDUAL CARBON NANOTUBES AND ISOLATED GRAPHENE
SHEETS 91
ALAIN JUNGEN 5.1 INTRODUCTION 91
5.2 INDIVIDUAL CARBON NANOTUBES 92
5.2.1 PHONONS 92
5.2.2 THEORY 95
5.2.3 EXPERIMENT 96
5.2.4 MICROSCOPY 98
5.2.5 THERMOGRAPHY 100
5.3 ISOLATED GRAPHENE SHEETS 101
5.3.1 THEORY 101
5.3.2 EXPERIMENT 102
5.3.3 CHARGE DISTRIBUTIONS 105
5.4 CONCLUSION 107
REFERENCES 108
6 RAMAN SPECTROSCOPY AND CONFOCAL RAMAN IMAGING IN MINERALOGY AND
PETROGRAPHY I LL
MARC FRIES AND ANDREW STEELE 6.1 INTRODUCTION I LL
6.2 RAMAN SPECTROSCOPY AND IMAGING AS A MINERALOGY/PETROGRAPHY TOOL 112
6.2.1 WORKING WITH THIN SECTIONS 114
6.2.2 CONTROL OF LASER POWER 116
6.3 "RAMAN MINERALOGY" USING IMAGING RAMAN TECHNIQUES 119 6.3.1 MINERAL
PHASE IMAGING 120
6.3.2 CRYSTALLOGRAPHIC ORIENTATION IMAGING 122
6.3.3 PHASE COMPOSITION IMAGING 123
6.4 EXAMPLES OF "RAMAN PETROGRAPHY" APPLICATIONS 124
6.4.1 RAMAN ANALYSIS OF SHOCKED MINERALS 124
6.4.2 CONTEXTUAL IMAGING OF CARBONACEOUS MATERIALS 126 6.4.3 FLUID
INCLUSIONS 129
6.4.4 ANCIENT TERRESTRIAL CARBONACEOUS MATERIALS 130 6.5 RAMAN
MINERALOGY IN FIELD GEOLOGY STUDIES 130
6.5.1 EXTRATERRESTRIAL EXPLORATION 132
6.6 CONCLUSION 133
REFERENCES 133
IMAGE 4
X CONTENTS
7 RAMAN MICRO-SPECTRAL IMAGING OF CELLS AND INTRACELLULAR DRUG DELIVERY
USING NANOCARRIER SYSTEMS 137
CHRISTIAN MATTHAEUS, TATYANA CHERNENKO, LUIS QUINTERO, MILOS" MILJKOVIC,
LARA MILANE, AMIT KALE, MANSOOR AMIJI, VLADIMIR TORCHILIN, AND MAX DIEM
7.1 INTRODUCTION 137
7.2 METHOD 140
7.2.1 DATA ACQUISITION 140
7.2.2 INTRODUCTION TO DATA PROCESSING METHODS 140
7.2.3 EXPERIMENTAL 144
7.3 RESULTS 145
7.3.1 CELL IMAGING 145
7.3.2 DRUG DELIVERY SYSTEMS 152
7.4 DISCUSSION 161
REFERENCES 162
8 CONFOCAL RAMAN MICROSCOPY IN PHARMACEUTICAL DEVELOPMENT 165 THOMAS F.
HAEFELE AND KURT PAULUS 8.1 INTRODUCTION 165
8.1.1 VIBRATIONAL SPECTROSCOPY IN PHARMACEUTICAL DEVELOPMENT 166
8.1.2 IMAGING IN PHARMACEUTICAL DEVELOPMENT 169
8.1.3 CHEMICAL IMAGING IN PHARMACEUTICAL DEVELOPMENT 172 8.1.4 CONFOCAL
RAMAN MICROSCOPY IN PHARMACEUTICAL DEVELOPMENT 176
8.2 APPLICATIONS OF CONFOCAL RAMAN MICROSCOPY IN PHARMACEUTICAL
DEVELOPMENT 179
8.2.1 PRACTICAL CONSIDERATIONS 179
8.2.2 INVESTIGATION OF SOLID DOSAGE FORMS BY CHEMICAL IMAGING 185
8.3 CONCLUSIONS 198
8.4 MATERIALS AND METHODS 198
REFERENCES 199
9 CHARACTERIZATION OF THERAPEUTIC COATINGS ON MEDICAL DEVICES 203 KLAUS
WORMUTH 9.1 BACKGROUND 203
9.2 PASSIVE THERAPEUTIC COATINGS 205
9.2.1 COATING THICKNESS 205
9.2.2 SWELLING OF HYDROPHILIC GEL COATINGS 208
9.3 ACTIVE THERAPEUTIC COATINGS 210
9.3.1 COATING MORPHOLOGY 210
9.3.2 DRUG MIXED WITH SINGLE POLYMER: MORPHOLOGY AND ELUTION 211
IMAGE 5
CONTENTS XI
9.3.3 DRUG MIXED WITH TWO POLYMERS: BLENDING AND LAYERING 216
9.3.4 DRUG MIXED WITH TWO POLYMERS: EXPOSURE TO WATER 219 9.3.5 DRUG
MIXED WITH BIODEGRADABLE POLYMER: DRUG ELUTION WITH POLYMER DEGRADATION
220
9.4 SUMMARY 223
REFERENCES 223
10 RAMAN IMAGING OF PLANT CELL WALLS 225
NOTBURGA GIERLINGER 10.1 INTRODUCTION 225
10.2 PLANT CELL WALLS 226
10.3 MICRO-RAMAN SPECTROSCOPY OF PLANT FIBERS 227
10.4 PLANT CELL WALL IMAGING BY CONFOCAL RAMAN MICROSCOPY 228 10.4.1
IMAGING CELLULOSE ORIENTATION AND LIGNIN DISTRIBUTION IN WOODEN CELL
WALLS 228
10.4.2 SILICA AND CELL WALL COMPOSITION IN HORSETAIL (E. HYEMALE) 232
10.5 OUTLOOK 234
10.6 MATERIAL AND METHODS 234
REFERENCES 235
11 CONFOCAL RAMAN IMAGING OF POLYMERIC MATERIALS 237
UTE SCHMIDT, JOERG MUELLER, AND JOACHIM KOENEN 11.1 INTRODUCTION 237
11.2 RAMAN IMAGING OF ISOTACTIC POLYPROPYLENE (IPP) 239 11.3 RAMAN
IMAGING OF POLYMER BLENDS 244
11.3.1 RAMAN IMAGING OF THIN FILMS OF THE POLYMER BLEND: POLYSTYRENE
(PS)- ETHYL-HEXYL-ACRYLATE (EHA) 245 11.3.2 RAMAN IMAGING OF THIN FILMS
OF THE POLYMER BLEND ETHYL-HEXYL-ACRYLATE (EHA)-STYRENE-BUTADIENE
RUBBER (SBR) 247
11.3.3 RAMAN IMAGING OF THIN FILMS OF THE POLYMER BLEND PS-EHA-SBR 249
11.4 POLYMER COATINGS 251
11.4.1 ACRYLIC PAINTS 251
11.4.2 ADHESIVES 253
11.5 ADDITIVES IN POLYMER MATRICES 253
11.6 SUMMARY 257
REFERENCES 257
12 STRESS ANALYSIS BY MEANS OF RAMAN MICROSCOPY 259
THOMAS WERMELINGER AND RALPH SPOLENAK 12.1 INTRODUCTION 259
IMAGE 6
XUE CONTENTS
12.1.1 THEORETICAL BACKGROUND 260
12.1.2 MEASURING IN CONVENTIONAL BACK-SCATTERING CONFIGURATION 261
12.1.3 OFF-AXIS RAMAN SPECTROSCOPY 263
12.1.4 STRESS TENSOR ANALYSIS IN BACK-SCATTERING RAMAN MICROSCOPY 266
12.2 CASE STUDIES 268
12.2.1 3D RAMAN SPECTROSCOPY MEASUREMENTS 268
12.2.2 ZNO 271
12.2.3 THE INFLUENCE OF STRESS ON THE PEAK POSITION OF POLYMERS 273
12.3 DISCUSSION 276
REFERENCES 277
INDEX 279 |
| any_adam_object | 1 |
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| indexdate | 2024-07-20T10:58:29Z |
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| isbn | 9783642125218 9783642125225 |
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| physical | XV, 289 S. Ill., graph. Darst. |
| publishDate | 2010 |
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| publisher | Springer |
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| series | Springer series in optical sciences |
| series2 | Springer Series in Optical Sciences |
| spelling | Confocal Raman microscopy Thomas Dieing ... eds. Berlin [u.a.] Springer 2010 XV, 289 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Springer Series in Optical Sciences 158 Raman-Spektroskopie (DE-588)4176916-8 gnd rswk-swf Konfokale Mikroskopie (DE-588)4336446-9 gnd rswk-swf 1\p (DE-588)4143413-4 Aufsatzsammlung gnd-content Konfokale Mikroskopie (DE-588)4336446-9 s Raman-Spektroskopie (DE-588)4176916-8 s DE-604 Dieing, Thomas (DE-588)143423193 edt Springer series in optical sciences 158 (DE-604)BV000000237 158 text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3478423&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=021133326&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Confocal Raman microscopy Springer series in optical sciences Raman-Spektroskopie (DE-588)4176916-8 gnd Konfokale Mikroskopie (DE-588)4336446-9 gnd |
| subject_GND | (DE-588)4176916-8 (DE-588)4336446-9 (DE-588)4143413-4 |
| title | Confocal Raman microscopy |
| title_auth | Confocal Raman microscopy |
| title_exact_search | Confocal Raman microscopy |
| title_full | Confocal Raman microscopy Thomas Dieing ... eds. |
| title_fullStr | Confocal Raman microscopy Thomas Dieing ... eds. |
| title_full_unstemmed | Confocal Raman microscopy Thomas Dieing ... eds. |
| title_short | Confocal Raman microscopy |
| title_sort | confocal raman microscopy |
| topic | Raman-Spektroskopie (DE-588)4176916-8 gnd Konfokale Mikroskopie (DE-588)4336446-9 gnd |
| topic_facet | Raman-Spektroskopie Konfokale Mikroskopie Aufsatzsammlung |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=3478423&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=021133326&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000000237 |
| work_keys_str_mv | AT dieingthomas confocalramanmicroscopy |