Holdings: Optically stimulated luminescence dosimetry

Optically stimulated luminescence dosimetry:

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Bibliographic Details
Main Authors:	Bøtter-Jensen, Lars (Author), McKeever, Stephen W. S. (Author), Wintle, Ann G. (Author)
Format:	Book
Language:	English
Published:	Amsterdam [u.a.] Elsevier 2006
Edition:	1. ed., transferred to digital printed version
Subjects:	Dosimetrie Lumineszenz
Online Access:	Inhaltsverzeichnis
Physical Description:	XVII, 355 S. graph. Darst.
ISBN:	0444506845

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adam_text	TABLE OF CONTENTS PREFACE xv CHAPTER 1: INTRODUCTION .......................................... I 1. ! Optically stimulated luminescence ....................................... I 1.2 Historical development of OSL dosimetry ............................... 2 1.3 OSL dosimetry ......................................................... 5 1.3.1 Personal dosimetry ............................................... 7 1.3.2 Environmental dosimetry ......................................... 9 1.3.3 Medical dosimetry ............................................... 9 1.3.4 Retrospective dosimetry .......................................... 9 1.4 This book ............................................................. 1 1 CHAPTER 2: OPTICALLY STIMULATED LUMINESCENCE THEORY .................................................. 15 2.1 Stimulated luminescence ............................................... 15 2.2 Generalised mathematical description of optically stimulated luminescence ........................................................... 17 2.3 The photoionisation cross-section ...................................... 19 2.3.1 Optical transitions .............................................. 19 2.3.2 Wavelength dependence ......................................... 21 2.3.3 Measurement of the photoionisation cross-section ................. 23 2.4 CW-OSL .............................................................. 27 2.4.1 Models and rate equations ....................................... 27 2.4.2 The one-trap/one-centre model ................................... 27 2.4.3 Models containing multiple-traps and centres ..................... 30 2.4.4 A more generalised model ....................................... 34 2.4.5 Temperature dependence effects .................................. 37 2.4.6 Thermal quenching .............................................. 44 2.5 LM-OSL .............................................................. 47 2.5.1 First- and general-order-kinetics ................................. 47 2.5.2 Relationship between LM-OSL and CW-OSL .................... 52 2.5.3 Wavelength dependence of LM-OSL ............................. 52 2.5.4 Photoconductivity ............................................... 54 viii Table of Contents 2.6 Pulsed OSL ............................................................ 56 2.6.1 Principles of pulsed OSL ........................................ 56 2.6.2 Delayed OSL ................................................... 59 2.7 Phototransferred effects ................................................ 60 2.7.1 Procedure ...................................................... 60 2.7.2 Mathematical description and typical data ........................ 61 2.8 Radiophotoluminescence ............................................... 65 2.8.1 Procedure ...................................................... 65 CHAPTERS: OSL PROPERTIES OF SYNTHETIC MATERIALS ...... 71 3.1 AbOvC ............................................................... 71 3.1.1 Introduction .................................................... 71 3.1.2 Crystal growth .................................................. 71 3.1.3 OSL stimulation and emission characteristics of A12O¡:C ......... 73 3.1.4 The OSL response of AljOy.C to radiation exposure .............. 75 3.1.5 The temperature dependence of OSL from AUOy.C ............... 77 3.1.6 Zeroing of the OSL signal from AhOj.C ......................... 79 3.2 Halides ................................................................ 81 3.2.1 KCI ............................................................ 81 3.2.2 KBr ............................................................ 82 3.2.3 NaCI ........................................................... 84 3.2.4 Rbl ............................................................ 85 3.2.5 CaF, ........................................................... 86 3.2.6 BaFX(X=Br,CI,I) ........................................... 87 3.3 Sulphates .............................................................. 90 3.3.1 MgS04 ......................................................... 90 3.3.2 CaSO4 ......................................................... 90 3.4 Sulphides .............................................................. 90 3.4.1 AS (A = Mg, Sr, Ca, Ba) ....................................... 90 3.5 Oxides ................................................................. 92 3.5.1 BeO ............................................................ 92 3.5.2 Fused quartz .................................................... 95 CHAPTER 4: PASSIVE OPTICALLY STIMULATED LUMINESCENCE DOSIMETRY ............................................. 101 4.1 Personal dosimetry ................................................... 101 4.1.1 Introduction ................................................... 101 4.1.2 Landauer s Luxei™ personal dosimetry system .................. 102 4.1.3 Landauer s InLight™ personal dosimetry system ................. 102 4.1.4 Beta dosimetry ................................................. 104 4.1.5 POSL imaging ................................................. 104 Table of Contents ix 4.2 Environmental OSL dosimetry using AbOţiC ......................... 107 4.2.1 Measurement of the natural terrestrial background radiation ..... 107 4.2.2 Measurement of the natural space background radiation ......... 107 4.3 UV dosimetry ........................................................ 110 4.4 OSL and RL remote optical fibre dosimetry in medical applications ___ 112 4.4.1 Real-time ( RT) in vivo monitoring of doses during radiotherapy .. 112 4.4.2 Optical fibre dosimeters ........................................ 112 CHAPTERS: OSL PROPERTIES OF NATURAL MATERIALS ........ 119 5.1 Quartz ............................................................... 119 5.1.1 Crystal structure and point defects .............................. 119 5.1.2 Decay curve shapes obtained under continuous stimulation — CW-OSL ...................................................... 123 5.1.2. 1 Stimulation sources ................................... 123 5.1.2.2 Effect of the 1 10° С trap ............................... 123 5.1.2.3 Dependence on power ................................. 125 5.1.2.4 Three components .................................... 126 5.1.2.5 Effect of stimulation wavelength ....................... 127 5.1.2.6 Effect of stimulation temperature ...................... 130 5.1.3 Linear modulation OSL—LM-OSL ............................. 130 5.1.3.1 LM-OSL at 160° С with 470 nm stimulation ............ 1 30 5.1.3.2 LM-OSL at different temperatures with 526 nm stimulation ................................... 135 5.1.3.3 LM-OSL from single grains using 532 nm ............. 135 5.1.4 PulsedOSL ................................................... 136 5.1.4. 1 Time resolved luminescence ........................... 137 5.1.4.2 Delayed optically stimulated luminescence or optically stimulated afterglow .................................. 140 5.1.5 Excitation spectra .............................................. 141 5.1.5.1 Bleaching response spectrum .......................... 141 5.1.5.2 Excitation spectra after bleaching by 514 ± 25 nm light ................................................. 143 5.1.5.3 Continuous scanning of stimulation wavelengths ........ 143 5.1.5.4 Excitation using interference filters and xenon lamp — 145 5.1.5.5 Excitation using laser lines from 458 to 645 nm ........ 147 5.1.5.6 Stimulation in the infra-red 780-920 nm ............... 147 5.1.6 Emission spectra ............................................... 149 5.1.6.1 OSL emission spectra ................................. 149 5.1.6.2 TL emission spectra .................................. 150 5.1.6.2.1 360-420 nm (near UV to violet) ........... 150 5.1.6.2.2 420-490 nm (blue) ........................ 153 5.1.6.2.3 590-650 nm (orange-red) .................. 153 5.1.6.3 Radiolumine scence .................................... 155 x Table of Contents 5.1.7 Dose dependence ............................................... 157 5.1.7.1 Fast component ....................................... 157 5.1.7.1.1 Multiple aliquot data ....................... 157 5.1.7.1.2 Single aliquot data ......................... 159 5.1.7.1.3 Single grain data .......................... 160 5.1.7.2 Low doses ............................................ 160 5.1.8 Effects of previous thermal treatment ............................ 162 5.1.8.1 High temperature annealing — above 500°C ............ 162 5.1.8.1.1 Comparison of LM-OSL, TL, RL and EPR .................................. 162 5.1.8.1.2 CW-OSL growth curves after annealing ..... 165 5.1.8.2 Low temperature annealing —160 to 280 C ............ 167 5.1.8.3 Thermal stability ..................................... 169 5.1.8.3.1 Isothermal decay ........................... 169 5.1.8.3.2 Pulse annealing ............................ 170 5.1.8.4 irradiation at elevated temperatures ................... 173 5.1.8.5 Thermal transfer ..................................... 174 5.1.9 Raised temperature OSL ....................................... 177 5.1.9.1 Thermal quenching ................................... 177 5.1.9.2 Thermal assistance ................................... 179 5.1.10 The slow component ............................................ 180 5.1.10.1 Thermal stability .......................... 181 5.1.10.2 Growth curve .............................. 183 5.1.10.3 Optical bleaching .......................... 184 5.1.10.4 TRL ...................................... 184 5.1.11 Photoionisation cross-section ................................... 184 5.1.12 Modelling processes giving rise to OSL in quartz ................ 186 5.1.13 Summary ...................................................... 188 5.2 Feldspars ............................................................. 188 5.2.1 Crystal structure ............................................... 188 5.2.2 Decay curve shape obtained under continuous stimulation — CW-OSL and CW-IRSL ................................................. 189 5.2.2.1 Stimulation sources ................................... 189 5.2.2.2 Effect of stimulation temperature ...................... 189 5.2.2.2.1 Initial part of signal ........................ 189 5.2.2.2.2 Decay curve shape ......................... 194 5.2.3 Linear modulation IRSL ....................................... 194 5.2.4 Pulsed OSL and IRSL ......................................... 197 5.2.4.1 Pulsed OSL .......................................... 197 5.2.4.2 Pulsed IRSL ......................................... 197 5.2.4.3 Optically stimulated afterglow ......................... 197 5.2.5 Excitation spectra .............................................. 199 5.2.5.1 Direct measurements .................................. 199 Table of Contents xi 5.2.5.2 Bleaching response spectrum .......................... 201 5.2.6 Emission spectra ............................................... 201 5.2.6.1 IRSL emission spectra ................................ 201 5.2.6.1.1 280-290 nm (near UV) .................... 201 5.2.6.1.2 320-340 nm (near UV) .................... 202 5.2.6.1.3 390-440 nm (violet/blue) .................. 203 5.2.6.1.4 550-570 nm (yellow/green) ................ 203 5.2.6.1.5 600-750 nm (red/far red) .................. 203 5.2.6.2 TL emission spectra .................................. 203 5.2.6.3 RL emission spectra .................................. 203 5.2.6.3.1 Under X-ray stimulation at low temperature ............................... 203 5.2.6.3.2 Under X-ray stimulation above room temperature ............................... 205 5.2.6.3.3 Under beta stimulation from a LUCs source . 205 5.2.6.4 Photoluminescence emission spectra ................... 205 5.2.7 Effects of previous optical treatment ............................ 207 5.2.7.1 Bleaching at ambient temperature ..................... 207 5.2.7.2 IR bleaching at elevated temperature .................. 208 5.2.8 Effects of previous thermal treatment ............................ 211 5.2.8.1 Pre-heating of laboratory and naturally irradiated samples .................................... 211 5.2.8.2 Pulse annealing ....................................... 212 5.2.8.3 irradiation at elevated temperature .................... 215 5.2.9 Raised temperature IRSL and OSL ............................. 215 5.2.9.1 Thermal quenching ................................... 215 5.2.9.2 Thermal assistance ................................... 216 5.2.9.2.1 Above room temperature ................... 216 5.2.9.2.2 Below room temperature ................... 216 5.2.9.2.3 Wavelength dependence .................... 217 5.2.9.2.4 Link to anomalous fading .................. 218 5.2.10 Anomalous fading .............................................. 219 5.2.10.1 TL. OSL and IRSL .................................. 219 5.2.10.2 Attempts to remove anomalous fading ................. 219 5.2.10.2.1 Using a preheat ............................ 219 5.2.10.2.2 Using an optical treatment ................. 220 5.2.10.3 A ttempts to avoid anomalous fading ................... 220 5.2.10.3.1 Using time-resolved measurements .......... 220 5.2.10.3.2 Using different detection wavelengths ....... 220 5.2.10.4 C L and TL spectra of fading feldspars ................. 220 5.2.10.5 Low temperature phosphorescence ..................... 221 5.2.10.6 Single grain IRSL fading and f adia plots ............... 223 5.2.10.7 Logarithmic signal decay .............................. 224 xii Table of Contents 5.2.10.8 Correcting for anomalous fading ....................... 224 5.2.11 Radioluminescence ............................................. 227 5.2. ¡I.I A new dating method ................................. 227 5.2.11.2 Practical considerations ............................... 229 5.2.11.3 Methods of Dv determination .......................... 229 5.2.11.4 Thermal stability ..................................... 229 5.2.11.5 Single grain measurements ............................ 229 5.2.12 Models for ¡RSL, OSL. IR-RL in feldspars ..................... 230 5.2.¡2. i IRSL ................................................ 230 5.2.12.2 OSL ................................................. 231 5.2.12.3 IR-RL ............................................... 231 5.2.12.4 Comparison of IR-RL and IRSL (or OSL) ............ 233 5.3 Conclusions .......................................................... 234 CHAPTER 6: RETROSPECTIVE OSL DOSIMETRY .................. 245 Part I: RETROSPECTIVE ACCIDENT DOSIMETRY .................... 245 6.1 Introduction .......................................................... 245 6.2 Materials and sampling ............................................... 246 6.3 Sample preparation and experimental details .......................... 247 6.4 Determination of the accident dose .................................... 247 6.4.1 Retrospective assessment of environmental dose rates ............ 247 6.4.2 Estimation of the accident dose ................................. 249 6.5 Analytical protocols .................................................. 250 6.5.1 Introduction ................................................... 250 6.5.2 Multiple-aliquot protocols ...................................... 250 6.5.3 The single aliquot regeneration and added dose protocol .......... 250 6.5.4 True single-aliquot protocols .................................... 252 6.5.4.1 Introduction ......................................... 252 6.5.4.2 Variation of OSL signal with pre-heat .................. 253 6.5.4.3 Choice of OSL signal ................................. 253 6.5.4.4 Sensitivity changes with regeneration cycles ............ 255 6.5.4.5 The SAR protocol ..................................... 255 6.6 Evaluation of dose-depth profiles in bricks ............................ 257 6.6.1 Continuous OSL scanning ...................................... 258 6.6.2 Determination of dose-depth profiles from Chernobyl bricks ..... 259 6.6.3 Absolute errors and estimated precision of the equivalent dose in bricks ....................................................... 259 6.7 Retrospective OSL dosimetry using unheated quartz ................... 260 6.7.1 Dose distributions .............................................. 261 6.7.2 Thermal transfer and sensitivity changes ........................ 263 Table of Contents xiii 6.8 Retrospective OSL dosimetry using household and workplace chemicals ............................................................. 265 6.9 Retrospective OSL dosimetry using porcelain .......................... 267 6.9.1 Introduction ................................................... 267 6.9.2 The origin of OSL in porcelain ................................. 267 6.9.2.1 Time-decaying dose-dependent OSL signals ............ 267 6.9.2.2 Time-steady PL emission spectra from porcelain ....... 270 6.9.2.3 OSL stimulation spectra .............................. 271 6.9.3 OSL dose response of porcelain ................................. 271 6.9.4 Dose-depth profiles in porcelain and the effect of transparency ... 272 6.9.5 OSL dosimetry using porcelain dental crowns .................... 273 6.10 Retrospective accident dosimetry — conclusions ........................ 275 Part II: GEOLOGICAL AND ARCHAEOLOGICAL DATING ........... 276 6.11 Measurement procedures .............................................. 276 6.11.1 Multiple-aliquot methods ....................................... 277 6.11.2 Single-aliquot methods ......................................... 280 6.11.2.1 Feldspars ............................................. 280 6.11.2.1.1 Additive dose .............................. 281 6.11.2.1.2 Regenerative dose .......................... 281 6.11.2.2 Quartz ............................................... 281 6.11.2.2.1 Additive dose .............................. 281 6.11.2.2.2 Regenerative dose .......................... 285 6.11.2.3 Luminescence sensitivity .............................. 287 6.11.2.4 Reliability of OSL monitoring of sensitivity change ..... 291 6.11.3 Dose distributions for single aiiquots ............................ 293 6.11.3.1 Histograms ........................................... 293 6.11.3.2 Probability density plots .............................. 295 6.11.3.3 Radial plots .......................................... 296 6.11.3.4 Calculation of Ą ...................................... 297 6.12 Single grains .......................................................... 298 6.12.1 Measurements ................................................. 298 6.12.1.1 Feldspars ............................................. 298 6.12.1.2 Quartz ............................................... 299 6.12.2 Dose distributions for single grains .............................. 299 6.12.2.1 Histograms ........................................... 299 6.12.2.2 Probability density plots .............................. 300 6.12.2.3 Radialplots .......................................... 300 6.12.2.4 Calculation of D, ...................................... 301 6.13 Geological and archaeological dating-conclusions ..................... 302 xiv Table of Contents CHAPTER?: OSL MEASUREMENT TECHNOLOGY ................. 311 7.1 Stimulation modes .................................................... 311 7.1.1 CW-OSL ...................................................... 311 7.1.2 LM-OSL ...................................................... 311 7.1.3 POSL ......................................................... 3U 7.2 The light detection system ............................................. 312 7.2.1 Photomultiplier tubes ........................................... 312 7.2.2 Imaging photon detectors ....................................... 313 7.2.3 Solid-state detectors ............................................ 314 7.3 Automated OSL readers .............................................. 315 7.4 Development of optical stimulation sources ............................ 316 7.4.1 Laser stimulation .............................................. 316 7.4.2 IR LED stimulation ............................................ 316 7.4.3 IR laser diode stimulation ...................................... 317 7.4.4 Broad-band light stimulation .................................... 318 7.4.5 Optimisation of OSL detection .................................. 320 7.4.6 Green LED stimulation ......................................... 321 7.4.7 Blue LED stimulation .......................................... 323 7.4.8 Blue LED and cut-off filter characteristics ....................... 325 7.4.9 Ramping the LEDs ............................................. 325 7.4.10 Pulsed and time-resolved OSL .................................. 326 7.5 Wavelength resolved OSL ............................................. 330 7.5.1 Stimulation spectrometry ....................................... 330 7.5.2 Emission spectrometry ......................................... 332 7.6 Imaging systems ...................................................... 334 7.7 Single grain OSL systems ............................................. 334 7.7.1 Introduction ................................................... 334 7.7.2 CCD luminescence imaging systems ............................. 335 7.7.3 Single grain laser OSL systems ................................. 335 7.8 OSL scanners ......................................................... 338 7.9 Portable systems for OSL measurements in the field ................... 340 7.10 The measurement of RL .............................................. 340 7.11 Commercially available OSL apparatus ................................ 343 7.12 Future developments .................................................. 345 SUBJECT INDEX ........................................................ 351
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spelling	Bøtter-Jensen, Lars Verfasser aut Optically stimulated luminescence dosimetry L. Bøtter-Jensen ; S. W. S. McKeever ; A. G. Wintle 1. ed., transferred to digital printed version Amsterdam [u.a.] Elsevier 2006 XVII, 355 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Dosimetrie (DE-588)4127470-2 gnd rswk-swf Lumineszenz (DE-588)4135964-1 gnd rswk-swf Lumineszenz (DE-588)4135964-1 s Dosimetrie (DE-588)4127470-2 s DE-604 McKeever, Stephen W. S. Verfasser aut Wintle, Ann G. Verfasser aut Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020873142&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Bøtter-Jensen, Lars McKeever, Stephen W. S. Wintle, Ann G. Optically stimulated luminescence dosimetry Dosimetrie (DE-588)4127470-2 gnd Lumineszenz (DE-588)4135964-1 gnd
subject_GND	(DE-588)4127470-2 (DE-588)4135964-1
title	Optically stimulated luminescence dosimetry
title_auth	Optically stimulated luminescence dosimetry
title_exact_search	Optically stimulated luminescence dosimetry
title_full	Optically stimulated luminescence dosimetry L. Bøtter-Jensen ; S. W. S. McKeever ; A. G. Wintle
title_fullStr	Optically stimulated luminescence dosimetry L. Bøtter-Jensen ; S. W. S. McKeever ; A. G. Wintle
title_full_unstemmed	Optically stimulated luminescence dosimetry L. Bøtter-Jensen ; S. W. S. McKeever ; A. G. Wintle
title_short	Optically stimulated luminescence dosimetry
title_sort	optically stimulated luminescence dosimetry
topic	Dosimetrie (DE-588)4127470-2 gnd Lumineszenz (DE-588)4135964-1 gnd
topic_facet	Dosimetrie Lumineszenz
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020873142&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT bøtterjensenlars opticallystimulatedluminescencedosimetry AT mckeeverstephenws opticallystimulatedluminescencedosimetry AT wintleanng opticallystimulatedluminescencedosimetry

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