Colloid science: principles, methods and applications
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| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Chichester
Wiley
2010
|
| Edition: | 2. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVIII, 375 S. Ill., graph. Darst. |
| ISBN: | 9781444320190 144432019X 9781444320206 1444320203 |
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Record in the Search Index
| _version_ | 1804143216079929344 |
|---|---|
| adam_text | Titel: Colloid science
Autor: Cosgrove, Terence
Jahr: 2010
Contents
Preface xv
Introduction xvii
Acknowledgements xix
List of Contributors xxi
1 An Introduction to Colloids I
Roy Hughes
1.1 Introduction 1
1.2 Basic Definitions 5
1.2.1 Concentration 5
1.2.2 Interfacial Area 10
1.2.3 Effective Concentrations 11
1.2.4 Average Separation 12
1.3 Stability 14
1.3.1 Quiescent Systems 15
1.3.2 Sedimentation or Creaming 16
1.3.3 Shearing Flows 17
1.3.4 Other Forms of Instability 17
1.4 Colloid Frontiers 18
References 20
2 Charge in Colloidal Systems 23
David Fermín and Jason Riley
2.1 Introduction 23
2.2 The Origin of Surface Charge 24
2.2.1 Ionisation of Surface Groups 24
2.2.2 Ion Adsorption 25
2.2.3 Dissolution of Ionic Solids 25
2.2.4 Isomorphous Substitution 25
2.2.5 Potential Determining Ions 25
2.3 The Electrochemical Double Layer 26
2.3.1 The Stern-Gouy-Chapman (SGC) Model of the Double Layer 26
2.3.2 The Double Layer at the Hg/Electrolyte Interface 30
2.3.3 Specific Adsorption 34
2.3.4 Interparticle Forces 36
viii Contents
2.4 Electrokinetic Properties 36
2.4.1 Electrolyte Flow 36
2.4.2 Streaming Potential Measurements 37
2.4.3 Electro-osmosis 38
2.4.4 Electrophoresis 39
2.4.5 Electroacoustic Technique 42
References 42
3 Stability of Charge-stabilised Colloids 45
John Eastman
3.1 Introduction 45
3.2 The Colloidal Pair Potential 46
3.2.1 Attractive Forces 46
3.2.2 Electrostatic Repulsion 47
3.2.3 Effect of Particle Concentration 49
3.2.4 Total Potential 50
3.3 Criteria for Stability 51
3.3.1 Salt Concentration 51
3.3.2 Counter-ion Valency 52
3.3.3 Zeta Potential 54
3.3.4 Particle Size 54
3.4 Kinetics of Coagulation 55
3.4.1 Diffusion-limited Rapid Coagulation 55
3.4.2 Interaction-limited Coagulation 56
3.4.3 Experimental Determination of c.c.c. 57
3.5 Conclusions 58
References 59
4 Surfactant Aggregation and Adsorption at Interfaces 61
Julian Eastoe
4.1 Introduction 61
4.2 Characteristic Features of Surfactants 61
4.3 Classification and Applications of Surfactants 62
4.3.1 Types of Surfactants 62
4.3.2 Surfactant Uses and Development 64
4.4 Adsorption of Surfactants at Interfaces 66
4.4.1 Surface Tension and Surface Activity 66
4.4.2 Surface Excess and Thermodynamics of Adsorption 67
4.4.3 Efficiency and Effectiveness of Surfactant Adsorption 71
4.5 Surfactant Solubility 73
4.5.1 The Krafft Temperature 73
4.5.2 The Cloud Point 74
4.6 Micellisation 75
4.6.1 Thermodynamics of Micellisation 75
Contents ix
4.6.2 Factors Affecting the CMC 78
4.6.3 Structure of Micelles and Molecular Packing 80
4.7 Liquid Crystalline Mesophases 82
4.7.1 Definition 82
4.7.2 Structures 83
4.7.3 Phase Diagrams 86
4.8 Advanced Surfactants 87
References 88
5 Microemulsions 91
Julian Eastoe
5.1 Introduction 91
5.2 Microemulsions: Definition and History 91
5.3 Theory of Formation and Stability 93
5.3.1 Interfacial Tension in Microemulsions 93
5.3.2 Kinetic Instability 95
5.4 Physicochemical Properties 95
5.4.1 Predicting Microemulsion Type 95
5.4.2 Surfactant Film Properties 101
5.4.3 Phase Behaviour 107
5.5 Developments and Applications 110
5.5.1 Microemulsions with Green and Novel Solvents 110
5.5.2 Microemulsions as Reaction Media for Nanoparticles 113
References 114
Emulsions 117
Brian Vincent
6.1 Introduction 117
6.1.1 Definitions of Emulsion Type 117
6.1.2 Novel Features of Emulsion Systems, Compared to
Solid/Liquid Dispersions 120
6.2 Preparation 120
6.2.1 Comminution - Batch 120
6.2.2 Comminution - Continuous 124
6.2.3 Nucleation and Growth 124
6.3 Stability 126
6.3.1 Introduction 126
6.3.2 Sedimentation and Creaming 126
6.3.3 Aggregation 127
6.3.4 Coalescence 128
6.3.5 Ostwald Ripening 130
6.3.6 Phase Inversion 131
References 133
÷ Contents
7 Polymers and Polymer Solutions 135
Terence Cosgrove
7.1 Introduction 135
7.2 Polymerisation 135
7.2.1 Condensation 136
7.2.2 Free Radical 136
7.2.3 Ionic Methods 137
7.3 Copolymers 137
7.4 Polymer Physical Properties 138
7.4.1 Entanglements 138
7.5 Polymer Uses 138
7.6 Theoretical Models of Polymer Structure 138
7.6.1 Radius of Gyration 139
7.6.2 Worm-like Chains 141
7.6.3 Radius of Gyration in Ideal Solution 142
7.6.4 Excluded Volume 142
7.6.5 Scaling Theory: Blobs 143
7.6.6 Polyelectrolytes 144
7.7 Measuring Polymer Molecular Weight 144
7.7.1 Viscosity 146
7.8 Flory-Huggins Theory 146
7.8.1 Polymer Solutions 146
7.8.2 Polymer Melts 150
7.8.3 Copolymers 150
References 150
8 Polymers at Interfaces 151
Terence Cosgrove
8.1 Introduction 151
8.1.1 Steric Stability 152
8.1.2 The Size and Shape of Polymers in Solution 152
8.1.3 Adsorption of Small Molecules 154
8.2 Adsorption of Polymers 155
8.2.1 Configurational Entropy 155
8.2.2 The Flory Surface Parameter *s 155
8.3 Models and Simulations for Terminally Attached Chains 156
8.3.1 Atomistic Modelling 156
8.3.2 Exact Enumeration: Terminally Attached Chains 157
8.3.3 Approximate Methods: Terminally Attached Chains 160
8.3.4 Scaling Models for Terminally Attached Chains (Brushes) 160
8.3.5 Physically Adsorbed Chains: Scheutjens and Fleer Theory 161
8.3.6 Scaling Theory for Physical Adsorption 165
8.4 Experimental Aspects 166
8.4.1 Volume Fraction Profiles 166
8.4.2 Adsorption Isotherms 167
Contents xi
8.4.3 The Bound Fraction 170
8.4.4 The Layer Thickness 171
8.5 Copolymers 175
8.5.1 Liquid/Liquid Interfaces 176
8.6 Polymer Brashes 177
8.7 Conclusions 179
References 180
9 Effect of Polymers on Colloid Stability 181
Jeroen van Duijneveldt
9.1 Introduction 181
9.1.1 Colloid Stability 181
9.1.2 Limitations of Charge Stabilisation 182
9.1.3 Effect of Polymers on Interactions 182
9.2 Particle Interaction Potential 182
9.2.1 Measuring Surface Forces 183
9.3 Steric Stabilisation 183
9.3.1 Theory 183
9.3.2 Steric Stabiliser Design 186
9.3.3 Marginal Solvents 187
9.4 Depletion Interactions 189
9.5 Bridging Interactions 192
9.6 Conclusion 193
References 194
10 Wetting of Surfaces 197
Paul Reynolds
10.1 Introduction 197
10.2 Surfaces and Definitions 198
10.3 Surface Tension 198
10.4 Surface Energy 199
10.5 Contact Angles 199
10.6 Wetting 200
10.7 Liquid Spreading and Spreading Coefficients 202
10.8 Cohesion and Adhesion 203
10.9 Two Liquids on a Surface 204
10.10 Detergency 207
10.11 Spreading of a Liquid on a Liquid 207
10.12 Characterisation of a Solid Surface 210
10.13 Polar and Dispersive Components 210
10.14 Polar Materials 211
10.15 Wettability Envelopes 212
10.16 Measurement Methods 214
10.17 Conclusions 216
References 216
x/7 Contents
11 Aerosols 219
Nana-Owusua A. Kwamena and Jonathan P. Reid
11.1 Introduction 219
11.2 Generating and Sampling Aerosols 222
11.2.1 Generating Aerosols 222
11.2.2 Sampling Aerosol 224
11.3 Determining the Particle Concentration and Size 225
11.3.1 Determining the Number Concentration 226
11.3.2 Determining the Mass Concentration 226
11.3.3 Determining Particle Size 227
11.4 Determining Particle Composition 230
11.4.1 Off-line Analysis 230
11.4.2 Real-time Analysis 231
11.5 The Equilibrium State of Aerosols 234
11.5.1 Deliquescence and Efflorescence 234
11.5.2 Köhler Theory 235
11.5.3 Measurements of Hygroscopic Growth 237
11.5.4 Other Phases 238
11.6 The Kinetics of Aerosol Transformation 238
11.6.1 Steady and Unsteady Mass and Heat Transfer 239
11.6.2 Uptake of Trace Species and Heterogeneous Chemistry 240
11.7 Concluding Remarks 242
References 242
12 Practical Rheology 245
245
245
246
248
250
252
254
256
256
257
258
259
261
263
264
267
268
268
271
References 272
Practical Rheology
Roy Hughes
12.1 Introduction
12.2 Making ; Measurements
12.2.1 Definitions
12.2.2 Designing an Experiment
12.2.3 Geometries
12.2.4 Viscometry
12.2.5 Shear Thinning and Thickening Behaviour
12.3 Rheometry and Viscoelasticity
12.3.1 Viscoelasticity and Deborah Number
12.3.2 Oscillation and Linearity
12.3.3 Creep Compliance
12.3.4 Liquid and Solid Behaviour
12.3.5 Sedimentation and Storage Stability
12.4 Examples of Soft Materials
12.4.1 Simple Particles and Polymers
12.4.2 Networks and Functionalisation
12.4.3 Polymeric Additives
12.4.4 Particle Additives
12.5 Summary
Contents xiii
13 Scattering and Reflection Techniques 273
Robert Richardson
13.1 Introduction 273
13.2 The Principle of a Scattering Experiment 274
13.3 Radiation for Scattering Experiments 275
13.4 Light Scattering 276
13.5 Dynamic Light Scattering 278
13.6 Small Angle Scattering 279
13.7 Sources of Radiation 279
13.8 Small Angle Scattering Apparatus 280
13.9 Scattering and Absorption by Atoms 282
13.10 Scattering Length Density 283
13.11 Small Angle Scattering from a Dispersion 284
13.12 Form Factor for Spherical Particles 285
13.13 Determining Particle Size from SANS and S AXS 285
13.14 Guinier Plots to Determine Radius of Gyration 286
13.15 Determination of Particle Shape 286
13.16 Polydispersity 287
13.17 Determination of Particle Size Distribution 288
13.18 Alignment of Anisotropie Particles 289
13.19 Concentrated Dispersions 289
13.20 Contrast Variation Using SANS 290
13.21 High â Limit: Porod Law 292
13.22 Introduction to X-Ray and Neutron Reflection 294
13.23 Reflection Experiment 295
13.24 A Simple Example of a Reflection Measurement 295
13.25 Conclusion 297
References 297
14 Optical Manipulation 299
Paul Bartlett
14.1 Introduction 299
14.2 Manipulating Matter with Light 299
14.3 Force Generation in Optical Tweezers 302
14.4 Nanofabrication 304
14.5 Single Particle Dynamics 305
14.5.1 Measuring Nanometer Displacements 305
14.5.2 Brownian Fluctuations in an Optical Trap 306
14.5.3 Dynamical Complexity in Colloidal Gels 307
14.6 Conclusions 308
References 308
15 Electron Microscopy 311
Sean Davis
15.1 General Features of (Electron) Optical Imaging Systems 311
x/V Contents
15.2 Conventional TEM
15.2.1 Background
15.2.2 Practical Aspects
15.2.3 Polymer Latex Particles
15.2.4 Core/Shell Particles
15.2.5 Internal Structure
15.3 Conventional SEM
15.3.1 Background
15.3.2 Types of Signal
15.3.3 Practical Aspects
15.4 Summary
References
16 Surface Forces
Wuge Briscoe
313
313
314
315
316
317
321
321
321
321
327
327
329
16.1 Introduction 329
16.1.1 Intermolecular Forces 329
16.1.2 From Intermolecular Forces to Surface Forces 330
16.1.3 Why Measure Surface Forces? 333
16.2 Forces and Energy; Size and Shape 334
16.2.1 Pressure, Force and Energy 334
16.2.2 The Derjaguin Approximation 335
16.3 Surface Force Measurement Techniques 339
16.3.1 Optical Tweezers 339
16.3.2 Total Internal Reflection Microscopy (TIRM) 340
16.3.3 Atomic Force Microscope (AFM) 340
16.3.4 Surface Force Apparatus (SEA) 341
16.3.5 Other Techniques 341
16.4 Different Types of Surface Forces 342
16.4.1 van der Waals Forces 343
16.4.2 Electric Double Layer Forces in a Polar Liquid 344
16.4.3 The DLVO Theory 345
16.4.4 Non-DLVO Forces 345
16.4.5 Neutral Polymer-mediated Surface Forces 352
16.4.6 Surface Forces in Surfactant Solutions 355
16.5 Recent Examples of Surface Force Measurement 356
16.5.1 Counter-ion Only (CIO) Electric Double Layer Interactions
in a Non-polar Liquid 357
16.5.2 Interactions Between Surface-grown Biomimetic
Polymer Brushes in Aqueous Media 358
16.5.3 Boundary Lubrication Under Water 358
16.6 Future Challenges 360
References 361
Index 363
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| indexdate | 2024-07-09T22:44:08Z |
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| spelling | Colloid science principles, methods and applications ed. by Terence Cosgrove 2. ed. Chichester Wiley 2010 XVIII, 375 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Kolloidphysik (DE-588)4713763-0 gnd rswk-swf Kolloidchemie (DE-588)4134420-0 gnd rswk-swf Colloids. Kolloidchemie (DE-588)4134420-0 s DE-604 Kolloidphysik (DE-588)4713763-0 s Cosgrove, Terence Sonstige oth HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020530942&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Colloid science principles, methods and applications Kolloidphysik (DE-588)4713763-0 gnd Kolloidchemie (DE-588)4134420-0 gnd |
| subject_GND | (DE-588)4713763-0 (DE-588)4134420-0 |
| title | Colloid science principles, methods and applications |
| title_auth | Colloid science principles, methods and applications |
| title_exact_search | Colloid science principles, methods and applications |
| title_full | Colloid science principles, methods and applications ed. by Terence Cosgrove |
| title_fullStr | Colloid science principles, methods and applications ed. by Terence Cosgrove |
| title_full_unstemmed | Colloid science principles, methods and applications ed. by Terence Cosgrove |
| title_short | Colloid science |
| title_sort | colloid science principles methods and applications |
| title_sub | principles, methods and applications |
| topic | Kolloidphysik (DE-588)4713763-0 gnd Kolloidchemie (DE-588)4134420-0 gnd |
| topic_facet | Kolloidphysik Kolloidchemie |
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