Rare earth coordination chemistry: fundamentals and applications
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| Format: | Book |
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| Language: | English |
| Published: |
Singapore
Wiley
2010
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XI, 575 S. Ill., graph. Darst. |
| ISBN: | 9780470824856 |
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| 245 | 1 | 0 | |a Rare earth coordination chemistry |b fundamentals and applications |c ed. by Chunhui Huang |
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|---|---|
| adam_text | Titel: Rare earth coordination chemistry
Autor: Huang, Chunhui
Jahr: 2010
Contents
Author Biographies xiii
Foreword xxi
Preface xxiii
1 Introduction 1
Chunhui Huang and Zuqiang Bian
1.1 Electronic Configuration of Lanthanide Atoms in the Ground State 1
1.2 Lanthanide Contraction 2
1.3 Specificity of the Photophysical Properties of Rare Earth Compounds 6
1.3.1 Spectral Terms 7
1.3.2 Selection Rules for Atomic Spectra 8
1.3.3 Lifetime 9
1.3.4 Absorption Spectra 10
1.3.5 The Emission Spectra of Rare Earth Compounds 11
1.4 Specificities of Rare Earth Coordination Chemistry 13
1.4.1 Valence State of Rare Earth Elements 14
1.4.2 Chemical Bonding of Rare Earth Elements 15
1.4.3 Coordination Numbers of Rare Earth Complexes 15
1.4.4 Tetrad Effect of Lanthanide Elements - Changing
Gradation Rules in Lanthanide Coordination Chemistry 21
1.5 Coordination Chemistry of Inorganic Compounds 25
1.5.1 Rare Earth Hydroxides 25
1.5.2 Rare Earth Halide and Perchlorate Compounds 26
1.5.3 Rare Earth Cyanide and Thiocyanate Compounds 27
1.5.4 Rare Earth Carbonate Compounds 28
1.5.5 Rare Earth Oxalate Compounds 30
1.5.6 Rare Earth Nitrate Compounds 31
1.5.7 Rare Earth Phosphate Compounds 32
1.5.8 Rare Earth Sulfate Compounds 34
1.5.9 Rare Earth Borate Compounds 36
1.6 Outlook 36
Acknowledgments 38
References 38
2 ß-Diketonate Lanthanide Complexes 41
Kezhi Wang
2.1 Introduction 41
2.2 Types of ß-Diketones Used for Lanthanide Complexes 42
Contents
2.2.1 Mono(ß-Diketone) Ligands 42
2.2.2 Bis(ß-Diketones) Ligands 44
2.2.3 Dendritic ß-Diketones Ligands 44
2.3 ß-Diketonate Lanthanide Complexes 47
2.3.1 Mononuclear Lanthanide Complexes with ß-Diketones 47
2.3.2 Polynuclear ß-Diketonate Lanthanide Complexes 71
2.4 Summary and Outlook 83
Acknowledgments 85
References 85
Rare Earth Complexes with Carboxylic Acids,
Polyaminopolycarboxylic Acids, and Amino Acids 91
Ruiyao Wang and Zhiping Zheng
3.1 Introduction 91
3.2 Rare Earth Complexes with Carboxylic Acids 92
3.2.1 Preparation of Rare Earth Complexes with Carboxylic Acids 92
3.2.2 Structural Chemistry of Rare Earth Complexes with
Carboxylic Acids 94
3.2.3 Solution Chemistry of Rare Earth Complexes with
Carboxylic Acids 114
3.3 Rare Earth Complexes with Polyaminopolycarboxylic Acids 115
3.3.1 Preparation of Rare Earth Complexes with
Polyaminopolycarboxylic Acids 116
3.3.2 Structural Chemistry of Rare Earth Complexes with
Polyaminopolycarboxylic Acids 116
3.3.3 Solution Chemistry of Rare Earth Complexes with
Polyaminopolycarboxylic Acids 120
3.4 Rare Earth Complexes with Amino Acids 122
3.4.1 Preparation of Rare Earth Complexes with Amino Acids 122
3.4.2 Structural Chemistry of Rare Earth Complexes with Amino Acids 122
3.4.3 Solution Chemistry of Rare Earth Complexes with Amino Acids 127
3.5 Summary and Outlook 129
References 130
N-Based Rare Earth Complexes 137
Xiaomei Zhang and Jianzhuang Jiang
4.1 Introduction 137
4.2 Rare Earth Complexes with Amide Type Ligands 137
4.2.1 Rare Earth Complexes with Aliphatic Amide Type Ligands 137
4.2.2 Rare Earth Complexes with Silyl Amide Type Ligands 142
4.3 Rare Earth Complexes with N-Heterocyclic Type Ligands 146
4.3.1 Rare Earth Complexes with Pyridine Type Ligands 146
4.3.2 Rare Earth Complexes with Imidazole Type Ligands 153
4.3.3 Rare Earth Complexes with Porphyrin Type Ligands 158
4.3.4 Rare Earth Complexes with Phthalocyanine Type Ligands 168
Contents
4.4 Rare Earth Complexes with Schiff Base Type Ligands 173
4.4.1 Rare Earth Complexes with Imine Type Ligands 174
4.4.2 Rare Earth Complexes with H2Salen (30) Type Ligands 180
4.5 Outlook 185
List of Abbreviations 185
Acknowledgments 186
References 186
5 Rare Earth Polyoxometalate Complexes 193
Ying Lu and Enbo Wang
5.1 Synthesis 193
5.2 Types and Structure Features 194
5.2.1 RE-POM Clusters 194
5.2.2 Extending Structural RE-POMs Complexes 208
5.2.3 RE-Organo Cation POM Supermolecule Complexes 217
5.3 Applications 218
5.3.1 Luminescence 218
5.3.2 Magnetism 221
5.3.3 Catalysis 221
5.3.4 Medicine 223
5.4 Outlook 223
References 223
6 Coordination Chemistry of Rare Earth Alkoxides,
Aryloxides, and Hydroxides 229
Zhiping Zheng and Ruiyao Wang
6.1 Introduction 229
6.2 Lanthanide Alkoxides, Aryloxides, and Macrocyclic Polyaryloxides 230
6.2.1 Preparative Methods 231
6.2.2 Structural Chemistry of Lanthanide Alkoxide Complexes 232
6.2.3 Applications of Lanthanide Alkoxides 246
6.3 Lanthanide Hydroxide Complexes 249
6.3.1 Rational Synthetic Methodologies for Lanthanide
Hydroxide Complexes 250
6.3.2 Coordination Modes of Hydroxo Ligands and Key
Lanthanide-HydroxoMotifs 251
6.3.3 Properties and Possible Applications 263
6.4 Summary and Outlook 265
Acknowledgments 265
References 265
7 Rare Earth Metals Trapped Inside Fullerenes - Endohedral
Metallofullerenes (EMFs) 273
Xing Lu, Takeshi Akasaka, and Shigeru Nagase
7.1 Introduction 273
7.1.1 Historyof Discovery 273
viii Contents
7.1.2 What Can Be Encapsulated Inside Fullerenes? 274
7.2 Preparation and Purification of EMFs 277
7.2.1 Production Methods 277
7.2.2 Extraction of EMFs from Raw Soot 279
7.2.3 Separation and Purification of EMFs 280
7.3 General Structures and Properties of EMFs Encapsulating
Rare Earth Metals 282
7.3.1 Geometrical Structures 283
7.3.2 Electronic Structures of EMFs: Intramolecular Charge Transfer 284
7.4 Chemistry of EMFs 286
7.4.1 Chemical Reactions of EMFs: An Overview 286
7.4.2 Positional Control of Encapsulated Metals by
Exohedral Modifications 292
7.4.3 Chemical Properties of Cage Carbons Dictated by the
Encapsulated Metals 292
7.4.4 Chemical Behaviors of EMFs Bearing Fused Pentagons 293
7.5 Applications of EMFs and Their Derivatives 294
7.5.1 Applications in Biology and Medicine 295
7.5.2 Applications in Material Science 297
7.6 Perspectives: Challenge and Chance 299
Acknowledgments 299
References 300
8 Organometallic Chemistry of the Lanthanide Metals 309
Yingming Yao and Qi Shen
8.1 Introduction 309
8.2 Synthesis and Reactivity of Organolanthanide Complexes
Containing Ln-C Bonds 310
8.2.1 Synthesis and Reactivity of Organolanthanide Tt-Complexes 310
8.2.2 Synthesis and Reactivity of Lanthanide Complexes Containing
Ln-Ca-Bonds 314
8.2.3 Synthesis and Reactivity of Lanthanide N-Heterocyclic
Carbene Complexes 320
8.2.4 Synthesis ofCationic Lanthanide Complexes 322
8.3 Synthesis and Reactivity of Lanthanide Hydride Complexes 325
8.3.1 Synthesis 325
8.3.2 Reactivity 328
8.4 Synthesis and Reactivity of Divalent Lanthanide Complexes 330
8.4.1 Synthesis of Classical Divalent Lanthanide Complexes 330
8.4.2 Synthesis of Non-classical Divalent Lanthanide Complexes 331
8.4.3 Reductive Reactivity 333
8.5 Organometallic Ce(IV) Complexes 334
8.6 Application in Homogeneous Catalysis 337
8.6.1 Organic Transformation 337
8.6.2 Polymerization 339
Contents
8.7 Summary and Outlook 345
References 346
9 Lanthanide Based Magnetic Molecular Materials 355
Bingwu Wang, Shangda Jiang, Xiuteng Wang, and Song Gao
9.1 Introduction 355
9.2 Magnetic Coupling in Lanthanide Containing Molecular Materials 357
9.2.1 Magnetic Coupling Mechanism of Gd(III) Systems 357
9.2.2 Magnetic Coupling in Ln(III) Containing Systems with Orbital
Moment Contribution 363
9.3 Magnetic Ordering in Lanthanide Based Molecular Materials 367
9.3.1 Lanthanide-Organic Radical Systems 367
9.3.2 4f-3d Heterometallic Systems 370
9.4 Magnetic Relaxation in Lanthanide Containing Molecular Materials 378
9.4.1 Introduction to Magnetic Relaxation 378
9.4.2 Magnetic Relaxation in Lanthanide Containing Complexes 381
9.5 Outlook 396
Acknowledgments 397
References 397
10 Gadolinium Complexes as MRI Contrast Agents for Diagnosis 407
Wingtak Wong and Kannie Waiyan Chan
10.1 Clinical Magnetic Resonance Imaging (MRI) Contrast Agents 407
10.1.1 Development of Clinical Contrast Agents 408
10.1.2 Clinical Contrast Agents 409
10.2 Chemistry of Gadolinium Based Contrast Agents 412
10.2.1 Relaxivity 412
10.2.2 Biomolecular Interactions 418
10.2.3 Toxicity and Safety Issues 420
10.3 Contrast Enhanced MRI for Disease Diagnosis 421
10.3.1 Magnetic Resonance Angiography (MRA) 422
10.3.2 Liver Disease 423
10.3.3 Oncology 424
10.4 Outlook 425
References 426
11 Electroluminescence Based on Lanthanide Complexes 435
Zuqiang Bian and Chunhui Huang
11.1 Introduction 435
11.1.1 Operating Principles in OLEDs 436
11.1.2 Historyof OLEDs 438
11.1.3 Potential Advantagesof Lanthanide Complexes Used in OLEDs 440
11.2 Lanthanide Complexes Used in OLEDs 441
11.2.1 Europium Complexes 442
x Contents
11.2.2 Terbium Complexes 455
11.2.3 Other Lanthanide Complexes 464
11.3 Outlook 468
Acknowledgments 468
References 468
12 Near-Infrared (NIR) Luminescence from Lanthanide(III) Complexes 473
Zhongning Chen and Haibing Xu
12.1 Introduction 473
12.2 Organic Antenna Chromophores as Sensitizers 475
12.2.1 Acyclic Ligands as Antenna Chromophores 476
12.2.2 Macrocyclic Ligands as Antenna Chromophores 492
12.3 Metal-Organic Chromophores as Sensitizers 500
12.3.1 d-Block Chromophores 500
12.3.2 f-Block Chromophores 516
12.4 Outlook 517
List of Abbreviations 518
Acknowledgments 519
References 519
13 Luminescent Rare Earth Complexes as Chemosensors and
Bioimaging Probes 529
Fuyou Li, Hong Yang, and He Hu
13.1 Introduction 529
13.2 Rare Earth Complexes as Luminescent Chemosensors 531
13.2.1 Basic Concept 531
13.2.2 Rare Earth Complexes as Luminescent pH Chemosensors 532
13.2.3 Rare Earth Complexes as Luminescent Chemosensors
for Cations 534
13.2.4 Rare Earth Complexes as Luminescent Chemosensors
forAnions 537
13.2.5 Rare Earth Complexes as Luminescent Chemosensors for
Small Molecules 540
13.3 Bioimaging Based on Luminescent Rare Earth Complexes 542
13.3.1 Time-Resolved Luminescence Imaging 542
13.3.2 Types of Luminescent Rare Earth Complexes for Bioimaging 543
13.3.3 Luminescent Rare Earth Complexes with Privileged Cyclen
Core Structures as Bioimaging Probes 544
13.3.4 Luminescent Rare Earth Complexes with Bis(benzimidazole)
Pyridine Tridentate Units as Bioimaging Probes 549
13.3.5 Hybrid Rare Earth Complexes as Luminescent Probes
in Bioimaging 552
13.4 Rare Earth Luminescent Chemosensors as Bioimaging Probes 552
13.4.1 Rare Earth Luminescent Chemosensors as Bioimaging
Probes ofZn2+ 553
Contents
13.4.2 Rare Earth Luminescent Chemosensors as Bioimaging
Probes of 02 554
13.5 Rare Earth Complexes as Multiphoton Luminescence Probes
for Bioimaging 556
13.6 Rare Earth Materials with Upconversion Luminescence for Bioimaging 558
13.6.1 General Concept of Upconversion Luminescence 558
13.6.2 Rare Earth Complexes with Upconversion Luminescence 558
13.6.3 Rare Earth Nanophosphors with Upconversion Luminescence 560
13.6.4 Rare Earth Upconversion Luminescence Nanophosphors as
Bioimaging Nanoprobes 562
13.7 Outlook 565
References 565
Index 571
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| spelling | Rare earth coordination chemistry fundamentals and applications ed. by Chunhui Huang Singapore Wiley 2010 XI, 575 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Seltenerdmetall (DE-588)4132099-2 gnd rswk-swf Seltenerdmetallkomplexe (DE-588)4386077-1 gnd rswk-swf Koordinationslehre (DE-588)4133952-6 gnd rswk-swf Seltenerdmetallkomplexe (DE-588)4386077-1 s DE-604 Seltenerdmetall (DE-588)4132099-2 s Koordinationslehre (DE-588)4133952-6 s Huang, Chunhui Sonstige oth HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020327343&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
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| subject_GND | (DE-588)4132099-2 (DE-588)4386077-1 (DE-588)4133952-6 |
| title | Rare earth coordination chemistry fundamentals and applications |
| title_auth | Rare earth coordination chemistry fundamentals and applications |
| title_exact_search | Rare earth coordination chemistry fundamentals and applications |
| title_full | Rare earth coordination chemistry fundamentals and applications ed. by Chunhui Huang |
| title_fullStr | Rare earth coordination chemistry fundamentals and applications ed. by Chunhui Huang |
| title_full_unstemmed | Rare earth coordination chemistry fundamentals and applications ed. by Chunhui Huang |
| title_short | Rare earth coordination chemistry |
| title_sort | rare earth coordination chemistry fundamentals and applications |
| title_sub | fundamentals and applications |
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