4D electron microscopy: imaging in space and time
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| Main Authors: | , |
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| Format: | Book |
| Language: | English |
| Published: |
London
Imperial College Press
2010
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 341 S. zahlr. Ill., graph. Darst. 25 cm |
| ISBN: | 9781848163904 1848163908 9781848164000 1848164009 |
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| 246 | 1 | 3 | |a Four dimensional electron microscopy |
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Record in the Search Index
| _version_ | 1804140997459836928 |
|---|---|
| adam_text | Titel: 4D electron microscopy
Autor: Zewail, Ahmed H.
Jahr: 2010
Contents
Acknowledgements v
Preface vii
1. Historical Perspectives: From Camera Obscura to 4D Imaging 1
2. Concepts of Coherence: Optics, Diffraction, and Imaging 15
2.1 Coherence ? A Simplified Prelude 15
2.2 Optical Coherence and Decoherence 18
2.3 Coherence in Diffraction 22
2.3.1 Rayleigh criterion and resolution 22
2.3.2 Diffraction from atoms and molecules 27
2.4 Coherence and Diffraction in Crystallography 29
2.5 Coherence in Imaging 34
2.5.1 Basic concepts 34
2.5.2 Coherence of the source, lateral and temporal 40
2.5.3 Imaging in electron microscopy 42
2.6 Instrumental Factors Limiting Coherence 48
3. From 2D to 3D Structural Imaging: Salient Concepts 53
3.1 2D and 3D Imaging 55
3.2 Electron Crystallography: Combining Diffraction and Imaging 61
3.3 High-Resolution Scanning Transmission Electron Microscopy 63
3.3.1 Use of STEM for electron tomography of inorganic
materials 67
3.4 Biological and Other Organic Materials 69
3.4.1 Macromolecular architecture visualized by
cryo-electron tomography 70
3.5 Electron-Energy-Loss Spectroscopy and Imaging by
Energy-Filtered TEM 73
3.5.1 Combined EELS and ET in cellular biology 75
3.6 Electron Holography 77
4. Applications of 2D and 3D Imaging and Related Techniques 83
4.1 Introduction 83
4.2 Real-Space Crystallography via HRTEM and HRSTEM 83
4.2.1 Encapsulated nanocrystalline structures 83
4D Electron Microscopy: Imaging in Space and Time
4.2.2 Nanocrystalline catalyst particles of platinum 84
4.2.3 Microporous catalysts and molecular sieves 86
4.2.4 Other zeolite structures 88
4.2.5 Structures of complex catalytic oxides solved by
HRSTEM 89
4.2.6 The value of electron diffraction in solving 3D structures 92
4.3 Electron Tomography 94
4.4 Electron Holography 95
4.5 Electron Crystallography 100
4.5.1 Other complex inorganic structures 101
4.5.2 Complex biological structures 103
4.6 Electron-Energy-Loss Spectroscopy and Imaging 107
4.7 Atomic Resolution in an Environmental TEM 111
4.7.1 Atomic-scale electron microscopy at ambient pressure
by exploiting the technology of microelectromechanical
systems 116
5. 4D Electron Imaging in Space and Time: Principles 123
5.1 Atomic-Scale Resolution in Time 123
5.1.1 Matter particle-wave duality 123
5.1.2 Analogy with light 126
5.1.3 Classical atoms: Wave packets 127
5.1.4 Paradigm case study: Two atoms 130
5.2 From Stop-Motion Photography to Ultrafast Imaging 134
5.2.1 High-speed shutters 134
5.2.2 Stroboscopy 138
5.2.3 Ultrafast techniques 139
5.2.4 Ultrafast lasers 143
5.3 Single-Electron Imaging 147
5.3.1 Coherence of ultrafast packets 147
5.3.2 The double-slit experiment revisited 152
5.3.3 Ultrafast versus fast imaging 154
5.3.4 The velocity mismatch and attosecond regime 157
5.4 4D Microscopy: Brightness, Coherence and Degeneracy 162
5.4.1 Coherence volume and degeneracy 164
5.4.2 Brightness and degeneracy 168
5.4.3 Coherence and Contrast 172
5.4.4 Contrast, dose, and resolution 174
6. 4D Ultrafast Electron Imaging: Developments and Applications 179
6.1 Developments at Caltech ? A Brief History 179
Contents
6.2 Instruments and Techniques 181
6.3 Structure, Morphology, and Mechanics 195
6.3.1 Selected-area image (diffraction) dynamics 195
6.3.2 Dynamical morphology: Time-dependent warping 196
6.3.3 Proof of principle: Gold dynamics 199
6.3.4 Prototypical case: Graphite in 4D space 204
6.3.4.1 Atomic motions 204
6.3.4.2 Coherent resonances in diffraction:
Longitudinal Young s modulus 208
6.3.4.3 Resonances in images: Longitudinal elasticity 211
6.3.4.4 Emergence of mechanical drumming:
Transverse ellasticity 213
6.3.4.5 Moire fringe dynamics 216
6.3.4.6 FEELS: Femtosecond EELS and chemical
bonding 218
6.4 Selected Other Applications 221
6.4.1 Structural phase transitions 223
6.4.1.1 Metal-insulator transformation 223
6.4.1.2 Transient phases of superconducting cuprates 227
6.4.2 Nucleation and crystallization phenomena 230
6.4.3 Interfaces and biological assemblies 234
6.4.3.1 Water on hydrophobic and hydrophilic
substrates 234
6.4.3.2 Bilayers, phospholipids, and cells 237
6.4.4 Nanomechanical and optoelectronic systems 242
6.4.4.1 Channel gating 242
6.4.4.2 Functional cantilevers 245
6.4.4.3 Optoelectronic nanorods 249
6.4.4.4 Diffraction and materials surface charging 253
6.5 4D Convergent Beam UEM: Nanodiffraction 256
6.6 4D Near-Field UEM: Nanostructures and Plasmonics 263
The Electron Microscope and the Synchrotron: A Comparison 275
7.1 Introduction 275
7.2 Transmission X-ray Microscopy and X-ray Microscopic
Tomography 277
7.2.1 X-ray tomography of biological cells 281
7.3 Coherent X-ray Diffraction Imaging 283
7.4 Extraction of Structures from Powdered Specimens 287
7.4.1 Extraction of structures from ultramicrocrystalline
specimens 288
4D Electron Microscopy: Imaging in Space and Time
7.4.2 Energy-dispersive X-ray diffraction 288
7.4.3 X-ray absorption fine structure spectroscopy 290
7.4.4 Combined X-ray absorption and X-ray diffraction for
in situ studies of powdered catalysts 293
7.5 Studies of Species in Solution 294
7.6 Laue Crystallography: Static and Dynamic 297
7.7 The Perennial Problem of Radiation Damage 299
7.8 Summarizing Assessment 301
8. 4D Visualization: Past, Present, and Future 309
8.1 Visualization and Complexity 309
8.2 Complexity Paradox: Coherence and Creative Chaos 314
8.3 From 2(3)D to 4D Microscopy 316
8.4 Emerging Developments 321
8.4.1 Materials science 321
8.4.2 Biological UEM 323
8.4.3 Structural dynamics: Theory and experiment 324
8.4.4 Aligned- and single-molecule imaging 330
8.4.5 Imaging with attosecond electrons 333
8.5 Epilogue 337
Biographical Profiles 343
? XII
|
| any_adam_object | 1 |
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| isbn | 9781848163904 1848163908 9781848164000 1848164009 |
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| spelling | Zewail, Ahmed H. 1946-2016 Verfasser (DE-588)128714743 aut 4D electron microscopy imaging in space and time Ahmed H. Zewail ; John M. Thomas Four dimensional electron microscopy London Imperial College Press 2010 XII, 341 S. zahlr. Ill., graph. Darst. 25 cm txt rdacontent n rdamedia nc rdacarrier Electron microscopy Hyperspace Space and time Three-dimensional imaging Vierdimensionaler Raum (DE-588)4138351-5 gnd rswk-swf Elektronenmikroskopie (DE-588)4014327-2 gnd rswk-swf Elektronenmikroskopie (DE-588)4014327-2 s Vierdimensionaler Raum (DE-588)4138351-5 s DE-604 Thomas, John M. Verfasser aut HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018867246&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zewail, Ahmed H. 1946-2016 Thomas, John M. 4D electron microscopy imaging in space and time Electron microscopy Hyperspace Space and time Three-dimensional imaging Vierdimensionaler Raum (DE-588)4138351-5 gnd Elektronenmikroskopie (DE-588)4014327-2 gnd |
| subject_GND | (DE-588)4138351-5 (DE-588)4014327-2 |
| title | 4D electron microscopy imaging in space and time |
| title_alt | Four dimensional electron microscopy |
| title_auth | 4D electron microscopy imaging in space and time |
| title_exact_search | 4D electron microscopy imaging in space and time |
| title_full | 4D electron microscopy imaging in space and time Ahmed H. Zewail ; John M. Thomas |
| title_fullStr | 4D electron microscopy imaging in space and time Ahmed H. Zewail ; John M. Thomas |
| title_full_unstemmed | 4D electron microscopy imaging in space and time Ahmed H. Zewail ; John M. Thomas |
| title_short | 4D electron microscopy |
| title_sort | 4d electron microscopy imaging in space and time |
| title_sub | imaging in space and time |
| topic | Electron microscopy Hyperspace Space and time Three-dimensional imaging Vierdimensionaler Raum (DE-588)4138351-5 gnd Elektronenmikroskopie (DE-588)4014327-2 gnd |
| topic_facet | Electron microscopy Hyperspace Space and time Three-dimensional imaging Vierdimensionaler Raum Elektronenmikroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018867246&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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