Miniaturization of analytical systems: principles, designs and applications
"Modern analytical techniques aim to improve selectivity and sensitivity, achieve faster analysis time and increase throughput. These very ambitious goals are exacerbated by the need to reduce the overall size of the device and the instrumentation. The interest for portable analytical instrumen...
Gespeichert in:
| Hauptverfasser: | , , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester
Wiley
2009
|
| Ausgabe: | 1. publ. |
| Schlagworte: | |
| Online-Zugang: | Publisher description Table of contents only Inhaltsverzeichnis |
| Zusammenfassung: | "Modern analytical techniques aim to improve selectivity and sensitivity, achieve faster analysis time and increase throughput. These very ambitious goals are exacerbated by the need to reduce the overall size of the device and the instrumentation. The interest for portable analytical instruments, which allow field tests to be carried out easily, has increased the practical usefulness of miniaturized analytical systems. Miniaturization of Analytical Systems: Principles, Designs and Applications provides a highly needed general vision of the miniaturization of analytical systems, including their principles, design and applications."--BOOK JACKET. |
| Beschreibung: | Includes bibliographical references and index |
| Beschreibung: | XII, 371 S. Ill., graph. Darst. |
| ISBN: | 9780470061107 |
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Datensatz im Suchindex
| _version_ | 1804140938367336448 |
|---|---|
| adam_text | Titel: Miniaturization of analytical systems
Autor: Rios Castro, Angel
Jahr: 2009
Contents
Preface xi
1 Miniaturization in Analytical Chemistry 1
1.1 Introduction 1
1.2 Miniaturization as One of the Critical Trends in Modern
Analytical Chemistry 2
1.3 Evolution in the Field of Analytical Miniaturization 8
1.4 Classification of Miniaturized Analytical Systems
and Definition of Terms 10
1.5 Theory of Miniaturization 15
1.6 Features of Miniaturized Analytical Systems 17
1.7 Incidences of Miniaturization in the Analytical Process 19
1.7.1 Miniaturization of the Steps of the Analytical Process 20
1.7.2 Integrated (Micro)systems for the Performance
of the Entire Analytical Process 30
1.8 Outlook 33
References 36
2 Tools for the Design of Miniaturized Analytical Systems 39
2.1 Introduction 39
2.2 Miniaturized Analytical Processes: The Downsizing
and Integrating Phenomena 40
2.2.1 Transport within Microfluidic Systems 42
2.2.2 Microsystem Design from Transport Parameter Information 45
2.3 Microfluidic Devices 45
2.3.1 Microvalves 45
2.3.2 Moving Liquids in Miniaturized Systems 51
2.3.3 Mixers 59
2.3.4 Volume-dispensing and Sample-introduction Devices 63
2.3.5 Detection Systems for Analytical Microsystems 64
2.4 Microtechnology 66
2.4.1 Computer Simulations in Microfluidics 66
2.4.2 Micromachining 68
2.4.3 Packaging of Microsystems 74
vi Contents
2.5 MEMS and NEMS 74
2.5.1 Fabrication and Characterization 75
2.5.2 Functionalization 76
2.5.3 Detection Methods 81
2.6 Outlook 84
References 88
3 Automation and Miniaturization of Sample Treatment 93
3.1 Introduction 93
3.2 Simplification of Sample Treatment: Microextraction
Techniques 94
3.2.1 Calibration in Microextraction Processes 94
3.2.2 Solid Phase Microextraction (SPME) Techniques 95
3.2.3 Liquid Phase Microextraction (LPME) Techniques 114
3.2.4 Comparison of Solid and Liquid Phase Microextraction
Techniques 117
3.3 Simplification of Sample Treatment: Continuous Flow Systems 119
3.3.1 Coupling to Gas Chromatography 120
3.3.2 Coupling to Liquid Chromatography 123
3.3.3 Coupling to Capillary Electrophoresis (CE) 127
References 135
4 Miniaturized Systems for Analytical Separations I: Systems
Based on a Hydrodynamic Flow 139
4.1 Introduction 139
4.2 The Earliest Example of Miniaturization of a Gas
Chromatograph and Some Other Developments 141
4.3 Capillary Liquid Chromatography (CLC) 144
4.4 Liquid Chromatography on Microchips 150
4.4.1 The Agilent HPLC Chip 150
4.4.2 Other Approaches to Microchip HPLC 155
4.4.3 Some Selected Applications 157
References 163
5 Miniaturized Systems for Analytical Separations II: Systems
Based on Electroosmotic Flow (EOF) 165
5.1 Introduction 165
5.2 CE on the Microchip Format 168
5.3 Modes and Theories of CE Microchips 170
5.4 Microfabrication Techniques 175
5.4.1 Microfabrication of Glass CE Microchips 177
5.4.2 Microfabrication of Polymer CE Microchips 178
Contents v/7
5.5 Basic Fluidic Manipulation/Motivation: Electrokinetic
Injection and Separation Protocols 181
5.6 Electrochromatography in Microchip Format: Designs
and Applications 184
5.7 Comparison of Hydrodynamic and Electroosmotic
Flow-driven Miniaturized Systems 187
5.8 Analytical Applications 189
5.8.1 DNA Analysis 190
5.8.2 Protein Analysis 196
5.8.3 Small-molecule Analysis 200
5.9 Outlook 206
References 208
6 Detection in Miniaturized Analytical Systems 213
6.1 Introduction 213
6.2 Laser-induced Fluorescence (LIF) Detection 214
6.2.1 Lamp-based Fluorescence Detection 218
6.2.2 Fluorescence Excited by Light-emitting
Diodes 218
6.2.3 (Electro)chemiluminescence Detection 219
6.3 Electrochemical Detection (ED) 220
6.3.1 End-channel Detection 221
6.3.2 In-channel Detection 224
6.3.3 Off-channel Detection 225
6.3.4 Electrode Materials 228
6.3.5 Modes of Detection 230
6.4 Microfluidics-MS Interfacing 234
6.4.1 Microfluidics-based Electrospray Ionization
(ESI) Sources 234
6.4.2 Microfluidics-MALDI-MS Interfacing 243
6.5 Unconventional Detection Methods 248
6.5.1 Absorbance Detection 248
6.5.2 Surface Plasmon Resonance (SPR) Detection 249
6.5.3 Thermal Lens Detection 251
6.5.4 Other Detection Methods 253
6.6 Outlook 254
References 254
7 Miniaturization of the Entire Analytical Process I:
Micro(nano)sensors 263
7.1 Introduction 263
7.2 Evolution of Sensors with Nanotechnology 264
viii Contents
7.3 Micro(nano)sensors 266
7.3.1 Optical Sensors 266
7.3.2 Electrochemical Sensors 270
7.3.3 Magnetic Sensors 272
7.3.4 Mass Sensors 273
7.4 Nanoprobes for In Vivo Bioanalysis 275
References 278
8 Miniaturization of the Entire Analytical Process II:
Micro Total Analysis Systems (u,TAS) 281
8.1 (ATAS, Microfluidics and Lab-on-a-Chip: Concepts
and Terminology 281
8.2 Basic Concepts of Microfluidics: The Design
of Analytical Microsystems 283
8.2.1 Types of Transport 284
8.2.2 Laminar and Turbulent Flows 285
8.2.3 The Design of Microfluidic Systems 286
8.3 The Basics of Downscaling in Microsystems 290
8.4 Microfluidic Platforms: Types, Principles and Classification 293
8.4.1 Capillary-driven Test Strips 294
8.4.2 Microfluidic Large-scale Integration (LSI) 296
8.4.3 Centrifugal Microfluidics 297
8.4.4 Electrokinetic Platforms 299
8.4.5 Droplet-based Microfluidic Platforms 300
8.5 Microfluidic Devices for Analytical Lab-on-a-Chip
Applications 302
8.5.1 DNA Analysis Integrated on Microfluidic Devices 305
8.5.2 Real Clinical Sample Analysis on Microfluidic
Devices 310
8.5.3 Real Environmental and Related Sample Analysis
on Microfluidic Devices 323
8.5.4 Real Food Sample Analysis on Microfluidic Devices 328
8.6 Outlook 338
References 339
9 Portability of Miniaturized Analytical Systems 345
9.1 Introduction 345
9.2 Portable Gas Analysers 346
9.3 Portable Electrochemical Analysers 351
9.4 Portable Optical Analysers 351
9.5 Portable Lab-on-a-Chip Analysers 352
References 354
Contents ix
10 Analytical Performance of Miniaturized Analytical Systems 357
10.1 Introduction 357
10.2 Quality Control in Miniaturized Systems 358
10.3 Validation of Microsystems 360
10.4 Qualification of Microsystems 361
10.5 Robustness of Microsystems 362
Further Reading 363
Index 365
|
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| spelling | Rios Castro, Angel Verfasser aut Miniaturization of analytical systems principles, designs and applications Angel Rios ; Alberto Escarpa ; Bartolomé Simonet 1. publ. Chichester Wiley 2009 XII, 371 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references and index "Modern analytical techniques aim to improve selectivity and sensitivity, achieve faster analysis time and increase throughput. These very ambitious goals are exacerbated by the need to reduce the overall size of the device and the instrumentation. The interest for portable analytical instruments, which allow field tests to be carried out easily, has increased the practical usefulness of miniaturized analytical systems. Miniaturization of Analytical Systems: Principles, Designs and Applications provides a highly needed general vision of the miniaturization of analytical systems, including their principles, design and applications."--BOOK JACKET. Chemistry, Analytic Miniature electronic equipment Mikrosystemtechnik (DE-588)4221617-5 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Instrumentelle Analytik (DE-588)4222592-9 gnd rswk-swf Miniaturisierung (DE-588)4406753-7 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s Miniaturisierung (DE-588)4406753-7 s DE-604 Instrumentelle Analytik (DE-588)4222592-9 s Mikrosystemtechnik (DE-588)4221617-5 s Escarpa, Alberto Verfasser aut Simonet, Bartolomé Verfasser aut http://www.loc.gov/catdir/enhancements/fy0909/2009016260-d.html Publisher description http://www.loc.gov/catdir/enhancements/fy0909/2009016260-t.html Table of contents only HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018804711&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Rios Castro, Angel Escarpa, Alberto Simonet, Bartolomé Miniaturization of analytical systems principles, designs and applications Chemistry, Analytic Miniature electronic equipment Mikrosystemtechnik (DE-588)4221617-5 gnd Analytische Chemie (DE-588)4129906-1 gnd Instrumentelle Analytik (DE-588)4222592-9 gnd Miniaturisierung (DE-588)4406753-7 gnd |
| subject_GND | (DE-588)4221617-5 (DE-588)4129906-1 (DE-588)4222592-9 (DE-588)4406753-7 |
| title | Miniaturization of analytical systems principles, designs and applications |
| title_auth | Miniaturization of analytical systems principles, designs and applications |
| title_exact_search | Miniaturization of analytical systems principles, designs and applications |
| title_full | Miniaturization of analytical systems principles, designs and applications Angel Rios ; Alberto Escarpa ; Bartolomé Simonet |
| title_fullStr | Miniaturization of analytical systems principles, designs and applications Angel Rios ; Alberto Escarpa ; Bartolomé Simonet |
| title_full_unstemmed | Miniaturization of analytical systems principles, designs and applications Angel Rios ; Alberto Escarpa ; Bartolomé Simonet |
| title_short | Miniaturization of analytical systems |
| title_sort | miniaturization of analytical systems principles designs and applications |
| title_sub | principles, designs and applications |
| topic | Chemistry, Analytic Miniature electronic equipment Mikrosystemtechnik (DE-588)4221617-5 gnd Analytische Chemie (DE-588)4129906-1 gnd Instrumentelle Analytik (DE-588)4222592-9 gnd Miniaturisierung (DE-588)4406753-7 gnd |
| topic_facet | Chemistry, Analytic Miniature electronic equipment Mikrosystemtechnik Analytische Chemie Instrumentelle Analytik Miniaturisierung |
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