Nanochromatography and nanocapillary electrophoresis: pharmaceutical and environmental analyses
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| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Hoboken, NJ
Wiley
2009
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Literaturangaben |
| Physical Description: | XVI, 270 S. Ill., graph. Darst. |
| ISBN: | 9780470178515 |
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Record in the Search Index
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| adam_text | Titel: Nanochromatography and nanocapillary electrophoresis
Autor: Ali, Imran
Jahr: 2009
CONTENTS
PREFACE xüi
ACKNOWLEDGMENTS xv
1 Introduction 1
1.1. Nanoanalyses / 1
1.2. Definition of Nanochromatography and Nanocapillary
Electrophoresis / 2
1.3. Nanochromatography and Nanocapillary Electrophoresis / 3
1.4. Fabrication of Microdevices / 4
1.5. Developments in Nanoanalyses / 6
1.6. Data Integration / 7
1.7. Protocol of Nanoanalyses / 10
1.8. Scope of the Book / 12
1.9. Conclusion / 12
References / 12
2 Fabrication of Microchips 17
2.1. Introduction / 17
2.2. Substrates / 18
VII
Viii CONTENTS
2.3. Techniques of Fabrication / 20
2.3.1. Glass Chips / 22
2.3.2. Quartz Chips / 28
2.3.3. Silica Chips / 31
2.3.4. Polymer Chips / 34
2.3.5. Plastic Chips / 36
2.3.6. Chips and the Polymerase Chain Reaction / 37
2.4. Surface Modification / 39
2.4.1. Modification by Polymers / 40
2.4.2. Modification by Silica Gel / 42
2.4.3. Modification by Monolithics / 44
2.4.4. Modification by Sulfonation / 44
2.5. Designs of Chips / 45
2.6. Bindings in Chips / 49
2.7. Conclusion / 50
References / 51
3 Instrumentation of Nanochromatography and
Nanocapillary Electrophoresis 59
3.1. Introduction / 59
3.2. Nanoliquid Chromatography (NLC) / 60
3.2.1. Mobile Phase Reservoirs / 62
3.2.2. Mobile Phases and Flow Calibration / 62
3.2.3. Mobile Phase Tubings / 63
3.2.4. Solvent Delivery Pump / 64
3.2.5. Sample Injector / 66
3.2.6. Separation Chips / 68
3.2.7. Detectors / 70
3.2.8. Recorder / 71
3.2.9. Sample Preparation Units / 72
3.3. Nanocapillary Electrophoresis / 74
3.3.1. Separation Chip / 76
3.3.2. Background Electrolyte and
Its Reservoirs / 79
3.3.3. Sample Injection Port / 79
3.3.4. Detectors / 82
CONTENTS IX
3.3.5. Recorder / 83
3.3.6. Sample Preparation Units / 83
3.4. Conclusion / 85
References / 86
4 Detection in Nanochromatography and
Nanocapillary Electrophoresis 91
4.1. Introduction / 91
4.2. Mass Spectrometer Detectors / 92
4.3. Fluorescence Detectors / 97
4.4. Electrochemical Detectors / 99
4.5. Element Specific Detectors / 101
4.6. Miscellaneous Detectors / 103
4.7. Conclusion / 105
References / 105
5 Sample Preparation in Nanochromatography
and Nanocapillary Electrophoresis 109
5.1. Introduction / 109
5.2. Sample Preparation / 111
5.3. Sampling /111
5.3.1. Biological Samples /111
5.3.1.1. Blood / 112
5.3.1.2. Urine / 112
5.3.1.3. Tissues / 112
5.3.1.4. Plants / 113
5.3.1.5. FoodStuffs / 113
5.3.2. Environmental Samples / 113
5.3.2.1. Air / 113
5.3.2.2. Water / 114
5.3.2.3. Sediment and Soils / 115
5.4. Preservation / 115
5.5. Filtration / 116
5.6. Digestion/Homogenization / 118
5.7. Extractions / 119
5.8. CleanUp / 119
5.9. Preconcentration / 121
CONTENTS
5.10. Off-Line Nanosample Preparation Methods / 121
5.10.1. Nano Solid Phase Extractions / 121
5.10.2. Nano Membrane Extractions / 123
5.10.3. Nano Miscellaneous Extractions / 124
5.11. Online Nanosample Preparation Methods / 125
5.12. Conclusion / 138
References / 138
6 Nano-High Performance Liquid Chromatography 145
6.1. Introduction / 145
6.2. Nano-HPLC / 146
6.3. Applications / 146
6.3.1. Nano-HPLC of Biological Matrices / 146
6.3.1.1. Proteomics / 147
6.3.1.2. Drugs Development and Design / 151
6.3.1.3. Environmental Analysis / 155
6.4. Optimization of Separations in Nano-HPLC / 161
6.5. Troubleshooting in Nano-HPLC / 161
6.6. Conclusion / 161
References / 162
7 Nanocapillary Electrochromatography and
Nanomicellar Electrokinetic Chromatography 167
7.1. Introduction / 167
7.2. Nanocapillary Electrochromatography / 167
7.2.1. Biological Samples / 168
7.2.2. Environmental Samples / 177
7.2.3. Mechanism of Separation / 181
7.3. Nanomicellar Electrokinetic
Chromatography / 181
7.3.1. Biological Samples / 182
7.3.2. Environmental Samples / 184
7.3.3. Mechanisms of Separation / 187
7.4. Conclusion / 188
References / 188
CONTENTS Xi
8 Nanocapillary Electrophoresis 191
8.1. Introduction / 191
8.2. Optimization / 192
8.3. Applications / 200
8.3.1. Proteomics / 200
8.3.2. Genomics / 205
8.3.3. Amino Acids / 210
8.3.4. Drug Development and Design / 211
8.3.5. Enzymes and Hormones / 214
8.3.6. Biological Fluids / 218
8.3.7. Foods and Beverages / 221
8.3.8. Viruses and Bacteria / 224
8.3.9. Explosives / 226
8.3.10. Environmental Analyses / 228
8.3.11. Miscellaneous Applications / 232
8.4. Mechanism of Separation / 234
8.5. Conclusion / 234
References / 235
9 Chiral Separations by Nanoliquid Chromatography
and Nanocapillary Electrophoresis 245
9.1. Introduction / 245
9.2. Nanoliquid Chromatography / 246
9.3. Nanocapillary Electrophoresis / 249
9.4. Mechanisms of Chiral Separation / 260
9.5. Conclusion / 261
References / 261
10 Perspectives on Nanoanalyses 263
10.1. Introduction / 263
10.2. Future of Microfluidic Devices / 264
10.3. Future Challenges / 265
10.4. Conclusion / 266
References / 267
Subject Index 269
|
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| spelling | Khan, Imran Ali 1931- Verfasser (DE-588)105652059 aut Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses Imran Ali ; Hassan Y. Aboul-Enein ; Vinod K. Gupta Hoboken, NJ Wiley 2009 XVI, 270 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Literaturangaben Chromatographic analysis Capillary electrophoresis Drugs / Analysis Pollutants / Analysis Environmental pollutants / Analysis Nanoparticles / Analysis Drugs Analysis Electrophoresis, Capillary methods Environmental Pollutants analysis Nanoparticles Analysis Nanotechnology methods Pharmaceutical Preparations analysis Pollutants Analysis Nanotechnologie (DE-588)4327470-5 gnd rswk-swf Chromatographie (DE-588)4010153-8 gnd rswk-swf Elektrophorese (DE-588)4014373-9 gnd rswk-swf Nanotechnologie (DE-588)4327470-5 s Chromatographie (DE-588)4010153-8 s Elektrophorese (DE-588)4014373-9 s DE-604 Aboul-Enein, Hassan Y. Verfasser aut Gupta, Vinod Kumar Verfasser aut HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018679906&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Khan, Imran Ali 1931- Aboul-Enein, Hassan Y. Gupta, Vinod Kumar Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses Chromatographic analysis Capillary electrophoresis Drugs / Analysis Pollutants / Analysis Environmental pollutants / Analysis Nanoparticles / Analysis Drugs Analysis Electrophoresis, Capillary methods Environmental Pollutants analysis Nanoparticles Analysis Nanotechnology methods Pharmaceutical Preparations analysis Pollutants Analysis Nanotechnologie (DE-588)4327470-5 gnd Chromatographie (DE-588)4010153-8 gnd Elektrophorese (DE-588)4014373-9 gnd |
| subject_GND | (DE-588)4327470-5 (DE-588)4010153-8 (DE-588)4014373-9 |
| title | Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses |
| title_auth | Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses |
| title_exact_search | Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses |
| title_full | Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses Imran Ali ; Hassan Y. Aboul-Enein ; Vinod K. Gupta |
| title_fullStr | Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses Imran Ali ; Hassan Y. Aboul-Enein ; Vinod K. Gupta |
| title_full_unstemmed | Nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses Imran Ali ; Hassan Y. Aboul-Enein ; Vinod K. Gupta |
| title_short | Nanochromatography and nanocapillary electrophoresis |
| title_sort | nanochromatography and nanocapillary electrophoresis pharmaceutical and environmental analyses |
| title_sub | pharmaceutical and environmental analyses |
| topic | Chromatographic analysis Capillary electrophoresis Drugs / Analysis Pollutants / Analysis Environmental pollutants / Analysis Nanoparticles / Analysis Drugs Analysis Electrophoresis, Capillary methods Environmental Pollutants analysis Nanoparticles Analysis Nanotechnology methods Pharmaceutical Preparations analysis Pollutants Analysis Nanotechnologie (DE-588)4327470-5 gnd Chromatographie (DE-588)4010153-8 gnd Elektrophorese (DE-588)4014373-9 gnd |
| topic_facet | Chromatographic analysis Capillary electrophoresis Drugs / Analysis Pollutants / Analysis Environmental pollutants / Analysis Nanoparticles / Analysis Drugs Analysis Electrophoresis, Capillary methods Environmental Pollutants analysis Nanoparticles Analysis Nanotechnology methods Pharmaceutical Preparations analysis Pollutants Analysis Nanotechnologie Chromatographie Elektrophorese |
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