Basic gas chromatography:
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Hoboken, NJ
Wiley,
2009
|
| Edition: | 2. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Klappentext |
| Physical Description: | XIII, 239 S. Ill., graph. Darst. |
| ISBN: | 9780470439548 |
Staff View
MARC
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| 100 | 1 | |a McNair, Harold M. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Basic gas chromatography |c Harold M. McNair ; James M. Miller |
| 250 | |a 2. ed. | ||
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Record in the Search Index
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|---|---|
| adam_text | CONTENTS
PREFACE TO THE SECOND EDITION
ix
PREFACE
xi
ACKNOWLEDGMENTS
xiii
1
INTRODUCTION
1
A Brief History
/ 1
Definitions
/ 3
Overview: Advantages and Disadvantages
/ 9
Instrumentation
/11
References
/ 13
2
INSTRUMENT OVERVIEW
14
Carrier Gas
/15
Flow Control and Measurement
/ 16
Sample Inlets and Sampling Devices
/ 20
Columns
/ 23
Temperature Zones
/ 24
Detectors
/ 27
Data Systems
/ 27
References
/ 28
V¡
CONTENTS
3
BASIC CONCEPTS
AND TERMS
29
Definitions, Terms, and Symbols
/ 29
The Rate Theory
/ 40
A Redefinition of
H
I
50
The Achievement of Separation
/ 51
References
/ 52
4
STATIONARY PHASES
53
Selecting a Column
/ 53
Classification of Stationary Phases for GLC
/ 54
Liquid Stationary Phases (GLC)
/ 65
Solid Stationary Phases (GSC)
/ 69
References
/ 69
5
PACKED COLUMNS AND INLETS
71
Solid Supports
/ 71
Liquid Stationary Phases
/ 73
Solid Stationary Phases (GSC)
/ 74
Gas Analysis
/ 76
Analysis of Other Inorganics
/ 80
Inlets for Liquid Samples and Solutions
/ 80
Special Columns
/ 81
Upgrading for Capillary Columns
/ 82
References
/ 83
6
CAPILLARY COLUMNS AND INLETS
84
Types of
ОТ
Columns
/ 84
ОТ
Column Tubing
/ 86
Advantages of
ОТ
Columns
/ 89
Column Selection
/ 91
Capillary Inlet Systems
/ 97
Miscellaneous Topics
/ 100
References
/ 102
7
DETECTORS
104
Classification of Detectors
/ 105
Detector Characteristics
/ 108
Flame Ionization Detector (FID)
/ 115
Thermal Conductivity Detector (TCD)
/ 119
CONTENTS
VII
Electron
Capture
Detector (ECD)
/ 122
Other Detectors
/ 125
References
/ 127
8
QUALITATIVE AND QUANTITATIVE ANALYSIS
129
Qualitative Analysis
/ 129
Quantitative Analysis
/ 135
References
/ 144
9
PROGRAMMED TEMPERATURE
145
Temperature Effects
/ 145
Advantages and Disadvantages of PTGC
/ 147
Requirements of PTGC
/ 149
Theory of PTGC
/ 151
Special Topics
/153
References
/155
10
GAS CHROMATOGRAPHY-MASS SPECTROMETRY
(GC-MS)
156
Instrumentation
/ 157
History
/ 165
Limitations of GC-MS Systems
/ 166
Data Analysis
/ 167
References
/ 169
11
MULTIDIMENSIONAL GAS CHROMATOGRAPHY
170
Overview
/ 170
Fundamental Principles of Multidimensional
Chromatography
/ 171
GCxGC with Heart Cutting
/ 174
Comprehensive GCxGC
/ 175
LCxGC with Heart Cutting
/ 178
Comprehensive LCxGC
/ 179
Summary
/180
References
/ 181
12
SAMPLING METHODS
183
Overview
/183
Liquid-Liquid Extraction (LLE)
/ 185
viii
CONTENTS
Solid-Liquid Extraction: Soxhlet Extraction and
Accelerated Solvent Extraction
(ASE)
/ 188
Liquid-Solid Extraction: Solid-Phase Extraction
(SPE)
/ 189
Liquid- or Solid-Vapor Extraction: Headspace
Extraction
/191
Solid-Phase Micro-extraction (SPME)
/ 193
Additional Techniques and Summary
/ 195
References
/ 197
13
SPECIAL TOPICS
Fast GC
/ 198
Chiral Analysis by GC
/ 201
GC Analysis of Nonvolatile Compounds
/ 202
References
/ 205
14
TROUBLESHOOTING GC SYSTEMS
APPENDIX I SYMBOLS AND ACRONYMS
APPENDIX II GUIDELINES FOR SELECTING
CAPILLARY COLUMNS
APPENDIX III GC: HOW TO AVOID PROBLEMS
APPENDIX IV CALCULATION OF SPLIT RATIO FOR
SPLIT INJECTION ON
ОТ
COLUMNS
APPENDIX V OPERATING CONDITIONS FOR
CAPILLARY COLUMNS
APPENDIX VI OV LIQUID PHASES PHYSICAL
PROPERTY DATA
APPENDIX
VII SOME
COMPRESSIBILITY CORRECTION
FACTORS (J)
APPENDIX
VIII
SOME INTERNET WEBSITES FOR GAS
CHROMATOGRAPHERS
198
APPENDIX IX
OTHER BOOKS ON GAS
CHROMATOGRAPHY
INDEX OF APPLICATIONS
INDEX
207
215
218
220
222
224
225
227
228
230
231
233
THE NEW EDITION OF THE
WELL-REGARDED HANDBOOK
ON GAS CHROMATOGRAPHY
ince
the publication of the highly successful first edition of
1
Basic Gas Chromatography, the practice of chromatography
has undergone several notable developments. Basic Gas Chromatography,
Second Edition covers the latest in the field, giving readers the most
up-to-date guide available, while maintaining the first edition s practi¬
cal, applied approach to the subject and its accessibility to a wide range
of readers.
The text provides comprehensive coverage of basic topics in the field, such
as stationary phases, packed columns and inlets, capillary columns and inlets,
detectors, and qualitative and quantitative analysis. At the same time, the
coverage also features key additions and updated topics including:
•
Gas chromatography-mass spectrometry (GC-MS)
•
Sampling methods
•
Multidimensional gas chromatography
•
Fast gas chromatography
•
Gas chromatography analysis of nonvolatile compounds
•
Inverse gas chromatography and pyrolysis gas chromatography
Along with these new and updated topics, the references, resources, and
Web sites in Bask Gas Chromatography have been revised to reflect the
state of the field. Concise and fundamental in its coverage, Basic Gas
Chromatograpliv, Second Edition remains the standard handbook for every¬
one from undergraduates studying analytical chemistry to working industrial
chemists.
HAROLD M. Me NAffi, PhD, known internationally as a leading researcher
and educator in the Held of chromatography, is currently Professor Emeritus
of Chemistry at Virginia Tech.
JAMES M. MILLER, PhD, is Professor Emeritus of Chemistry at Drew
University, where he taught for thirty-six years. He is also the author of
Chromatography: Concepts and Contrasts (Wiley).
|
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| indexdate | 2024-07-09T21:42:43Z |
| institution | BVB |
| isbn | 9780470439548 |
| language | English |
| lccn | 2009013332 |
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| physical | XIII, 239 S. Ill., graph. Darst. |
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| spelling | McNair, Harold M. Verfasser aut Basic gas chromatography Harold M. McNair ; James M. Miller 2. ed. Hoboken, NJ Wiley, 2009 XIII, 239 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Gaschromatographie (DE-588)4019330-5 s DE-604 Miller, James M. Verfasser aut Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017715657&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017715657&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Klappentext |
| spellingShingle | McNair, Harold M. Miller, James M. Basic gas chromatography Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| subject_GND | (DE-588)4019330-5 |
| title | Basic gas chromatography |
| title_auth | Basic gas chromatography |
| title_exact_search | Basic gas chromatography |
| title_full | Basic gas chromatography Harold M. McNair ; James M. Miller |
| title_fullStr | Basic gas chromatography Harold M. McNair ; James M. Miller |
| title_full_unstemmed | Basic gas chromatography Harold M. McNair ; James M. Miller |
| title_short | Basic gas chromatography |
| title_sort | basic gas chromatography |
| topic | Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| topic_facet | Gas chromatography Gaschromatographie |
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