Synthesis of solid catalysts:
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| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH-Verl.
2009
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| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Item Description: | Literaturangaben |
| Physical Description: | XX, 401 S. Ill., graph. Darst. 24 cm |
| ISBN: | 9783527320400 |
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Record in the Search Index
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CONTENTS PREFACE XIII LIST OF CONTRIBUTORS XV ABBREVIATIONS XIX PART I
BASIC PRINCIPLES AND TOOLS 1 GENERAL ASPECTS 3 KRIJN P. DEJONG 1.1
IMPORTANCE OF SOLID CATALYSTS 3 1.2 DEVELOPMENT OF SOLID CATALYSTS 4 1.3
DEVELOPMENT OF SOLID CATALYST SYNTHESIS 5 1.4 ABOUT THIS BOOK 10
REFERENCES 10 2 INTERFACIAL CHEMISTRY 13 ALEXIS LYCOURGHIOTIS 2.1
INTRODUCTION 13 2.2 INTERFACIAL AND BULK DEPOSITION 14 2.3 THE SURFACE
OF THE OXIDIC SUPPORTS: SURFACE IONIZATION MODELS 15 2.3.1 THE CHARGED
SURFACE OF THE OXIDIC SUPPORTS 15 2.3.2 HOMOGENEOUS SURFACE IONIZATION
MODELS 16 2.3.3 THE MUSIC MODEL 17 2.4 THE SIZE AND THE STRUCTURE OF THE
INTERFACE 18 2.5 THE ARRANGEMENT OF THE IONS INSIDE THE INTERFACE AND
THE DEPOSITION MODES 20 2.5.1 INDIFFERENT IONS 20 2.5.2 TRANSITION-METAL
IONIC SPECIES 22 2.6 DETERMINING THE MODE OF INTERFACIAL DEPOSITION AND
THE SURFACE SPECIATION/STRUCTURE OF THE DEPOSITED PRECURSOR SPECIES 23
BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/991676483 DIGITALISIERT
DURCH VI CONTENTS 2.6.2 METHODOLOGIES BASED ON MACROSCOPIC ADSORPTION
DATA AND POTENTIOMETRIC TITRATIONS AS WELL AS ON MICROELECTROPHORETIC
MOBILITY OR STREAMING POTENTIAL MEASUREMENTS 23 2.6.3 SPECTROSCOPIC
INVESTIGATIONS 25 2.6.4 QUANTUM-MECHANICAL CAKULATIONS 26 2.6.5
ELECTROCHEMICAL (EQUILIBRIUM) MODELING 26 2.7 A CASE STUDY: THE
DEPOSITION OF CO(H 2 O) 62+ AQUA COMPLEX ON THE TITANIA SURFACE 27 2.7.1
EXPERIMENTAL INVESTIGATION 27 2.7.2 QUANTUM-MECHANICAL CALCULATIONS 28
2.7.3 ELECTROCHEMICAL (EQUILIBRIUM) MODELING 29 REFERENCES 30 3
ELECTROSTATIC ADSORPTION 33 JOHN R. REGALBUTO 3.1 INTRODUCTION 33 3.2
PURELY ELECTROSTATIC ADSORPTION 37 3.3 ELECTROSTATIC ADSORPTION WITH
METAL RESPECIATION 38 3.4 ELECTROSTATIC ADSORPTION AND ION EXCHANGE 41
3.5 ELECTROSTATIC ADSORPTION AND DEPOSITION-PRECIPITATION 45 3.6
ELECTROSTATIC ADSORPTION AND SURFACE REACTION 46 3.7 ELECTROSTATICS AND
DISSOLUTION, REACTION, AND REDEPOSITION 47 CONTENTS VII 4.5.2 DEGREES
OFFREEDOM: DRYING PARAMETERS AND LIGANDS IN SOLUTION 76 4.6 CONCLUSIONS
77 REFERENCES 78 5 SOL-CEL PROCESSING 83 MIRON V. LANDAU 5.1
INTRODUCTION 83 5.2 PHYSICOCHEMICAL BASIS AND PRINCIPLES OF SOL-GEL
PROCESSING 85 5.2.1 ACTIVATION 86 5.2.2 POLYCONDENSATION 87 5.2.3
GELATION/AGING/WASHING 89 5.2.4 GEL DRYING/DESOLVATION 90 5.2.5
STABILIZATION OF XERO- AND AEROGELS 90 5.3 APPLICATION OF SOL-GEL
PROCESSING FOR THE PREPARATION OF SOLID CATALYSTS 91 5.3.1 BULK
CATALYTIC PHASE MATERIALS: XERO-AND AEROGELS 91 5.3.1.1 MONOMETALLIC
CATALYTIC MATERIALS 91 5.3.1.2 MULTIMETALLIC COMPOSITE CATALYTIC PHASES
94 5.3.2 CATALYTIC MATERIALS AND MODIFIERS ENTRAPPED IN POROUS MATRICES
97 5.3.2.1 ATOMS OR MOLECULAR SUBSTANCES ENTRAPPED BY COCONDENSATION AT
THE COLLOIDIZATION STEP 98 5.3.2.2 MOLECULAR SUBSTANCES ADSORBED OR
ENTRAPPED AT THE GELATION STEP 103 VIII CONTENTS 7.2 BASIC PRINCIPLES OF
PRECIPITATION AND NUCLEATION 136 7.3 RAW MATERIALS 139 7.4 PRECIPITATION
CONDITIONS 141 7.5 PROCESS OPERATION 141 7.6 EXAMPLES 145 7.6.1 HIGH
METAL NICKEL/ALUMINA CATALYSTS 145 7.6.2 SINGLE-STEP SULFUR-PROMOTED
NICKEL/ALUMINA CATALYST 146 7.6.3 COPPER/ZINC METHANOL CATALYSTS 147
7.6.4 IRON-BASED FISCHER-TROPSCH CATALYSTS 148 7.6.5 UNSUPPORTED METAL
SULFIDE CATALYSTS FOR HYDROTREATING 148 7.7 NEW DEVELOPMENTS IN PROCESS
MONITORING 148 ACKNOWLEDGMENTS 149 REFERENCES 149 8 CLUSTERS AND
IMMOBILIZATION 153 SOPHIE HERMAM 8.1 INTRODUCTION 153 8.2 THE SURFACE OF
COMMON SUPPORTS 154 8.3 CLUSTERS IN CATALYSIS 157 8.4 REACTION WITH
UNMODIFIED SURFACE 160 8.5 "SHIP-IN-A-BOTTLE" SYNTHESIS 163 8.6
TETHERING 167 8.7 CONDUDING REMARKS 168 REFERENCES 169 9 SHAPING OF
SOLID CATALYSTS 173 CONTENTS IX 10 SPACE AND TIME-RESOLVED SPECTROSCOPY
OF CATALYST BODIES 201 BERT M. WECKHUYSEN 10.1 INTRODUCTION 201 10.2
SPACE- AND TIME-RESOLVED METHODS APPLIED TO CATALYST BODIES 201 10.2.1
INVASIVE METHODS 202 10.2.2 NONINVASIVE METHODS 205 10.3 CASE STUDIES
209 10.3.1 KEGGIN-TYPE CO-MO COMPLEXES IN CATALYST BODIES 209 10.3.2
SPECIATION OF CO COMPLEXES IN CATALYST BODIES 212 10.4 FURURE PROSPECTS
215 ACKNOWLEDGMENTS 215 REFERENCES 216 11 HIGH-THROUGHPUT
EXPERIMENTATION 217 UWE RODEMERCK AND DAVID LINKE 11.1 INTRODUCTION 217
11.2 SYNTHESIS STRATEGIES 219 11.2.1 COMBINATORIAL STRATEGIES 220 11.2.2
METHODS TO REDUCE EXPERIMENTS 220 11.3 CATALYST LIBRARIES FOR PRIMARY
SCREENING 223 11.3.1 WAFER-BASED PREPARATION 223 11.3.2 SINGLE PELLETS
224 11.3.3 SINGLE BEADS 225 X CONTENTS 12.2.5 CONCENTRATION EFFECTS BY
SPECIFIC ADSORPTION 253 12.2.6 SITE ISOLATION OR THE ROLE OF ZEOLITES AS
SOLID SOLVENTS 254 12.3 ZEOLITIZARION 254 12.3.1 OVERALL STEPS IN
ZEOLITE CRYSTALLIZATION 255 12.3.2 CLASSIC MODEL FOR ZEOLITE GROWTH 257
12.3.3 THE AGGREGATION MODEL 259 12.3.4 ZEOLITIZATION PARAMETERS 260
12.3.5 NANOCRYSTALLINE ZEOLITES 264 12.3.6 ZEOLITE SYNTHESIS VIA THE DRY
GEL ROUTE 265 12.3.7 ALPO 4 -N-BASED MOLECULAR SIEVE ZEOLITES 266 12.3.8
IONOTHERMAL SYNTHESIS METHOD 267 12.3.9 ZEOLITES WITH PORES BEYOND THE
12-MR 267 12.3.10 UPSCALINGOF ZEOLITE SYNTHESIS 268 REFERENCES 268
FURTHER READING 276 13 ORDERED MESOPOROUS MATERIALS 277 YING WAN AND
DONGYUAN ZHAO 13.1 INTRODUCTION 277 13.2 MESOPOROUS SILICA 277 13.2.1
MCM-41 279 13.2.2 SBA-15 280 13.2.3 MCM-48 281 13.2.4 PORE-SIZE CONTROL
282 13.3 ORGANIC GROUP FUNCTIONALIZED MESOPOROUS SILICATES 284 CONTENTS
XI 14.2 TYPICAL HYDROTREATING CATALYST 302 14.2.1 TYPICAL CATALYST
COMPOSITION 302 14.2.2 LITERATURE DESCRIBING THE PREPARATION OF
HYDROTREATING CATALYSTS 302 14.3 SUPPORT PREPARATION 303 14.3.1
PRECIPITATION OFY-ALUMINA 303 14.3.2 ADDITION OFSIO 2 305 14.3.3
ADDITION OFOTHER COMPONENTS (E.G. ZEOLITES) AND EXTRUSION 305 14.3.4
DRYING AND CALCINATION OF A1 2 O 3 AND SIO 2 -AL 2 O 3 SUPPORTS 307 14.4
METAL COMIXING/COEXTRUSION AND COPRECIPITATION ROUTES 307 14.4.1
ADDITION OF METALS TO THE A1 2 O 3 DOUGH 307 14.4.2 BULK CATALYSTS 308
14.4.3 DRYING AND CALCINATION OF CATALYSTS PREPARED BY
COMIXING/COEXTRUSION AND COPRECIPITATION ROUTES 308 14.5 IMPREGNATION OF
METALS 309 14.5.1 TYPICAL ADDITIVES AND SOLUTION STABILIZERS 309 14.5.2
PORE-VOLUME IMPREGNATION VERSUS DIPPING/EQUILIBRIUM IMPREGNATION OF
COMPACTED SUPPORT PARTICLES 310 XII CONTENTS ACKNOWLEDGMENT 348
REFERENCES 349 16 CASE STUDIES OF NOBEL-METAL CATALYSTS 353 STUART SOLED
16.1 INTRODUCTION 353 16.2 OPTIMIZATION OF CATALYST PREPARATION 354
16.2.1 ELECTROSTATIC INTERACTIONS AND THE USE OF ZETA POTENTIAL
MEASUREMENTS 355 16.2.2 NOBLE-METAL IMPREGNATION EXAMPLE ONTO A MODIFIED
SILICA-ALUMINA SUPPORT 356 16.2.3 A NOVEL APPROACH FOR THE PREPARATION
OF DISPERSED RU ON SILICA 358 16.2.4 OTHER METALS THAT FORM SIMILAR
SUPPORTED COMPLEXES AS RU 363 16.2.5 CONCLUSIONS 365 ACKNOWLEDGMENTS 366
REFERENCES 366 17 GOLD CATALYSTS 369 CATHERINE LOUIS 17.1 INTRODUCTION
369 17.2 PREPARATIONS INVOLVING AQUEOUS SOLUTIONS 370 17.,2.1
IMPREGNATION TO INCIPIENT WERNESS 370 17.2.2 ANION ADSORPTION 371
17.2.3 SMALL PARTIDES FROM HAUCL,-3H 2 O 371 17.2 A
DEPOSITION-PREDPITATION WITH NAOH 373 17.2.5 GOLD COMPLEX INTERACTION
WITH OXIDE SUPPORTS 375 |
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| spelling | Synthesis of solid catalysts ed. by Krijn P. de Jong Weinheim Wiley-VCH-Verl. 2009 XX, 401 S. Ill., graph. Darst. 24 cm txt rdacontent n rdamedia nc rdacarrier Literaturangaben Catalysts Synthesis Heterogeneous catalysis Herstellung (DE-588)4159653-5 gnd rswk-swf Heterogene Katalyse (DE-588)4123377-3 gnd rswk-swf Katalysator (DE-588)4029919-3 gnd rswk-swf Katalysator (DE-588)4029919-3 s Heterogene Katalyse (DE-588)4123377-3 s Herstellung (DE-588)4159653-5 s DE-604 Jong, Krijn P. de (DE-588)138239967 edt text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3192078&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017685726&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Synthesis of solid catalysts Catalysts Synthesis Heterogeneous catalysis Herstellung (DE-588)4159653-5 gnd Heterogene Katalyse (DE-588)4123377-3 gnd Katalysator (DE-588)4029919-3 gnd |
| subject_GND | (DE-588)4159653-5 (DE-588)4123377-3 (DE-588)4029919-3 |
| title | Synthesis of solid catalysts |
| title_auth | Synthesis of solid catalysts |
| title_exact_search | Synthesis of solid catalysts |
| title_full | Synthesis of solid catalysts ed. by Krijn P. de Jong |
| title_fullStr | Synthesis of solid catalysts ed. by Krijn P. de Jong |
| title_full_unstemmed | Synthesis of solid catalysts ed. by Krijn P. de Jong |
| title_short | Synthesis of solid catalysts |
| title_sort | synthesis of solid catalysts |
| topic | Catalysts Synthesis Heterogeneous catalysis Herstellung (DE-588)4159653-5 gnd Heterogene Katalyse (DE-588)4123377-3 gnd Katalysator (DE-588)4029919-3 gnd |
| topic_facet | Catalysts Synthesis Heterogeneous catalysis Herstellung Heterogene Katalyse Katalysator |
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