Analysis, synthesis, and design of chemical processes:
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| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Upper Saddle River, NJ ; Munich [u.a.]
Prentice Hall
2009
|
| Edition: | 3. ed. |
| Series: | Prentice Hall international series in the physical and chemical engineering sciences
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Klappentext |
| Physical Description: | XXXIII, 1068 S. Ill., graph. Darst. 1 CD-ROM (12 cm) |
| ISBN: | 0135129664 9780135129661 |
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| 245 | 1 | 0 | |a Analysis, synthesis, and design of chemical processes |c Richard Turton ... |
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Chemical Engineering
The Leading Integrated
Chemical
Process
Design Guide:
Now with New Problems, New Projects, and More
More
than ever, effective design is the focal point of sound chemical engineering. Analysis, Synthesis, and
Design of Chemical Processes, Third Edition, presents design as a creative process that integrates both the big
picture and the small details
—
and knows which to stress when, and why. Realistic from start to finish, this book
moves readers beyond classroom exercises into open-ended, real-world process problem solving. The authors
introduce integrated techniques for every facet of the discipline, from finance to operations, new plant design to
existing process optimization.
This fully updated Third Edition presents entirely new problems at the end of every chapter. It also adds extensive
coverage of batch process design, including realistic examples of equipment sizing for batch sequencing; batch
scheduling for multi-product plants; improving production via intermediate storage and parallel equipment; and
new optimization techniques specifically for batch processes.
Coverage includes
•
Conceptualizing and analyzing chemical processes:
·
Analyzing process performance via I/O models,
flow diagrams, tracing, process conditions, and more performance curves, and other tools
•
Chemical process economics: analyzing capital and
·
Process troubleshooting and "debottlenecking"
manufacturing costs, and predicting or assessing
.
Chemical engineering design and society: ethics,
profitability professionalism, health, safety, and new "green
•
Synthesizing and optimizing chemical processing: engineering" techniques
experience-based principles, BFD/PFD, simulations,
.
Participating successfully in chemical engineering
and more design teams
Analysis, Synthesis, and Design of Chemical Processes, Third Edition, draws on nearly
35
years of innovative
chemical engineering instruction at West Virginia University. It includes suggested curricula for both single-
semester and year-long design courses; case studies and design projects with practical applications; and
appendixes with current equipment cost data and preliminary design information for eleven chemical processes-
including seven brand new to this edition.
About the CD-ROM
The CD-ROM contains the latest version of CAPCOST, a powerful tool for evaluating fixed capital investment, full
process economics, and profitability—now expanded with cost data for conveyors, crystallizers, dryers, dust
collectors, filters, mixers, reactors, and screens. It also contains the HENSAD tool for constructing temperature
interval, cascade, and temperature enthalpy diagrams; estimating optimal approach temperatures; and designing
heat exchanger networks. Also provided: additional chapters on outcomes assessment, written and oral
communications, and a written report case study, as well as six complete student design projects.
Richard Turton,
P.E.,
has taught the senior design course at West Virginia University for the past
22
years.
Previously, he spent five years in the design and construction industry. Richard
С
Bailie, professor emeritus at
WVU, taught chemical engineering design for more than
20
years, and has ten years of additional experience in
process evaluation, pilot plant operation, plant start-up, and industrial consulting. Wallace B. Whiting,
P.E.,
professor emeritus at the University of Nevada, Reno, has practiced and taught chemical process design for more
than
24
years. Joseph A. Shaeiwitz has been involved in WVU's senior design sequence and unique sophomore-
and junior-level integrated design projects for
20
years.
Contents
Material on the CD-ROM
xix
Preface
xxiii
About the Authors
xxvii
List of Nomenclature
xxix
SECTION
1
CONCEPTUALIZAnON AND ANALYSIS OF CHEMICAL PROCESSES
1
Chapter
1
Diagrams for Understanding Chemical Processes
5
1.1
Block Flow Diagrams (BFDs)
7
1.1.1
Block Flow Process Diagram
7
1.1.2
Block Flow Plant Diagram
9
1.2
Process Flow Diagram (PFD)
9
1.2.1
Process Topology
12
1.2.2
Stream Information
15
1.2.3
Equipment Information
19
1.2.4
Combining Topology, Stream Data, and Control Strategy
to Give a PFD
19
1.3
Piping and Instrumentation Diagram (P&ID)
26
1.4
Additional Diagrams
32
1.5
Three-Dimensional Representation of a Process
33
1.6
The
3-D
Plant Model
42
1.7
Summary
44
References
45
Short Answer Questions
45
Problems
46
Chapter
2
The Structure and Synthesis of Process Flow Diagrams
51
2.1
Hierarchy of Process Design
51
2.2
Step
1—
Batch versus Continuous Process
52
2.3
Step
2—
The Input/Output Structure of the Process
57
vi
Contents
Chapter
4
2.3.2
Process Concept Diagram
57
2.3.2
The Input/Output Structure of the Process Flow Diagram
58
2.3.3
The Input/Output Structure and Other Features of the Generic
Block Flow Process Diagram
60
2.3.4
Other Considerations for the Input/Output Structure
of the Process Flowsheet
63
2.3.5
What Information Can Be Determined Using the Input/
Output Diagram for a Process
? 66
2.4
Step
3—
The Recycle Structure of the Process
68
2.4.1
Efficiency of Raw Material Usage
69
2.4.2
Identification and Definition of the Recycle Structure
of the Process
70
2.4.3
Other Issues Affecting the Recycle Structure That Lead
to Process Alternatives
75
2.5
Step
4—
General Structure of the Separation System
84
2.6
Step
5—
Heat-Exchanger Network or Process Energy Recovery
System
84
2.7
Information Required and Sources
84
2.8
Summary
84
References
86
Short Answer Questions
88
Problems
88
Chapter
3
Batch Processing
93
93
3.1
Design Calculations for Batch Processes
3.2
Gantt Charts and Scheduling
100
3.3
Nonoverlapping,
Overlapping Operations, and Cycle Times
3.4
Flowshop and
Jobshop
Plants
104
3.4.1
Flowshop Plants
104
3.4.2 Jobshop
Plants
107
3.5
Product and Intermediate Storage and Parallel Process Units
3.5.1
Product Storage
f
or Single Product Campaigns
110
3.5.2
Intermediate Storage
113
3.5.3
Parallel Process Units
115
3.6
Design of Equipment for Multiproduct Batch Processes
116
3.7
Summary
119
References
119
Short Answer Questions
119
Problems
120
Chemical Product Design
123
4.1
Strategies for Chemical Product Design
124
4.2
Needs
126
101
110
Contents
vii
4.3
Ideas
128
4.4
Selection
129
4.5
Manufacture
131
4.6
Batch Processing
132
4.7
Economic Considerations
132
4.8
Summary
133
References
133
Chapter
5
Tracing Chemicals through the Process Flow Diagram
135
5.1
Guidelines and Tactics for Tracing Chemicals
135
5.2
Tracing Primary Paths Taken by Chemicals in a Chemical
Process
136
5.3
Recycle and Bypass Streams
142
5.4
Tracing Nonreacting Chemicals
146
5.5
Limitations
147
5.6
Written Process Description
147
5.7
Summary
149
Problems
149
Chapter
б
Understanding Process Conditions
151
6.1
Conditions of Special Concern for the Operation of Separation
and Reactor Systems
152
6.1.1
Pressure
152
6.1.2
Temperature
153
6.2
Reasons for Operating at Conditions of Special Concern
154
6.3
Conditions of Special Concern for the Operation of Other
Equipment
159
6.4
Analysis of Important Process Conditions
163
6A.1 Evaluation of Reactor R-101
163
6.4.2
Evaluation of High-Pressure Phase Separator V-102
170
6.4.3
Evaluation of Large Temperature Driving Force in Exchanger
E-101
171
6.4.4
Evaluation of Exchanger E-102
171
6.4.5
Pressure Control Valve on Stream
8 171
6.4.6
Pressure Control Valve on Stream from V-102 to V-103
171
6.5
Summary
171
References
172
Short Answer Questions
172
Problems
172
viii
Contents
SECTION
2
ENGINEERING
ECONOMIC
ANALYSIS OF CHEMICAL PROCESSES
175
Chapter
7
Estimation of Capital Costs
177
7.1
Classifications of Capital Cost Estimates
177
7.2
Estimation of Purchased Equipment Costs
181
7.2.3
Effect of Capacity on Purchased Equipment Cost
182
7.2.2
Effect of Time on Purchased Equipment Cost
186
7.3
Estimating the Total Capital Cost of a Plant
187
7.3.1
Lang Factor Technique
191
7.3.2
Module Costing Technique
192
7.3.3
Bare Module Cost for Equipment at Base Conditions
193
7.3.4
Bare Module Cost for
Nonbase Case
Conditions
197
7.3.5
Combination of Pressure and
MOC
Information to Give
the Bare Module Factor, FBM, and Bare Module Cost, CBM
208
7.3.6
Algorithm for Calculating Bare Module Costs
209
7.3.7
Grass Roots and Total Module Costs
210
7.3.8
A Computer Program
(CAPCOST)for
Capital Cost Estimation
Using the Equipment Module Approach
212
7.4
Summary
215
References
215
Short Answer Questions
216
Problems
216
Chapter
8
Estimation of Manufacturing Costs
221
8.1
Factors Affecting the Cost of Manufacturing a Chemical
Product
221
8.2
Cost of Operating Labor
226
8.3
Utility Costs
228
8.3.3
Background Information on Utilities
228
8.3.2
Calculation of Utility Costs
230
8.4
Raw Material Costs
244
8.5
Yearly Costs and Stream Factors
246
8.6
Estimating Utility Costs from the PFD
247
8.7
Cost of Treating Liquid and Solid Waste Streams
250
8.8
Evaluation of Cost of Manufacture for the Production of Benzene
via the Hydrodealkylation of Toluene
250
8.9
Summary
251
References
252
Short Answer Questions
252
Problems
253
Chapter
9
Engineering Economic Analysis
257
9.1
Investments and the Time Value of Money
9.2
Different Types of Interest
262
258
Contents ix
9.2.2 Simple
Interest
262
9.2.2
Compound
Interest
262
9.2.3
Interest
Rates Changing with Time
264
9.3
Time Basis for Compound Interest Calculations
264
9.3.1
Effective Annual Interest Rate
265
9.3.2
Continuously Compounded Interest
265
9.4
Cash Flow Diagrams
266
9.4.1
Discrete Cash Flow Diagram
267
9.4.2
Cumulative Cash Flow Diagram
269
9.5
Calculations from Cash Flow Diagrams
270
9.5.3
Annuities
—
A Uniform Series of Cash Transactions
271
9.5.2
Discount Factors
272
9.6
Inflation
276
9.7
Depreciation of Capital Investment
279
9.7.1
Fixed Capital, Working Capital, and Land
280
9.7.2
Different Types of Depreciation
281
9.7.3
Current Depreciation Method: Modified Accelerated Cost
Recovery System (MACRS)
285
9.8
Taxation, Cash Flow, and Profit
286
9.9
Summary
288
References
290
Short Answer Questions
290
Problems
291
Chapter
10
Profitability Analysis
297
10.1
A Typical Cash Flow Diagram for a New Project
297
10.2
Profitability Criteria for Project Evaluation
299
10.2.1
Nondiscounted Profitability Criteria
300
10.2.2
Discounted Profitability Criteria
302
10.3
Comparing Several Large Projects: Incremental Economic
Analysis
308
10.4
Establishing Acceptable Returns from Investments: The Concept
of Risk
311
10.5
Evaluation of Equipment Alternatives
312
10.5.1
Equipment with the Same Expected Operating Lives
313
10.5.2
Equipment with Different Expected Operating Lives
314
10.6
Incremental Analysis for Retrofitting Facilities
319
10.6.1
Nondiscounted Methods for Incremental Analysis
320
10.6.2
Discounted Methods for Incremental Analysis
323
10.7
Evaluation of Risk in Evaluating Profitability
325
10.7.1
Forecasting Uncertainty in Chemical Processes
326
10.7.2
Quantifying Risk
331
10.8
Profit Margin Analysis
344
Contents
10.9
Summary
345
References
346
Short Answer Questions
346
Problems
347
SECTION
3
SYNTHESIS AND OPTIMIZATION OF CHEMICAL PROCESSES
361
Chapter
11
Utilizing Experience-Based Principles to Confirm the Suitability
of a Process Design
363
11.1
The Role of Experience in the Design Process
364
11.1.1
Introduction to Technical Heuristics and Short-Cut
Methods
365
11.1.2
Maximizing the Benefits Obtained from Experience
365
11.2
Presentation of Tables of Technical Heuristics and Guidelines
368
11.3
Summary
371
References
389
Problems
389
Chapter
12
Synthesis of the PFD from the Generic BFD
391
12.1
Information Needs and Sources
392
12.1.1
Interactions with Other Engineers and Scientists
392
12.1.2
Reaction Kinetics Data
392
12.1.3
Physical Property Data
393
12.2
Reactor Section
394
12.3
Separator Section
396
12.3.1
General Guidelines
f
or Choosing Separation
Operations
397
12.3.2
Sequencing of Distillation Columns for Simple
Distillation
400
12.3.3
Azeotropic Distillation
403
12.4
Reactor Feed Preparation and Separator Feed Preparation
Sections
415
12.5
Recycle Section
416
12.6
Environmental Control Section
416
12.7
Major Process Control Loops
416
12.8
Flow Summary Table
417
12.9
Major Equipment Summary Table
417
12.10
Summary
418
References
418
Problems
419
Contents xi
Chapter
13
Synthesis of a Process Using a Simulator and Simulator
Troubleshooting
423
13.1
The Structure of a Process Simulator
424
13.2
Information Required to Complete a Process Simulation:
Input Data
428
13.2.1
Selection of Chemical Components
428
13.2.2
Selection of Physical Property Models
428
13.2.3
Input the Topology of the Flowsheet
431
13.2.4
Select Feed Stream Properties
431
13.2.5
Select Equipment Parameters
432
13.2.6
Selection of Output Display Options
440
13.2.7
Selection of Convergence Criteria and Running
a Simulation
440
13.3
Handling Recycle Streams
441
13.4
Choosing Thermodynamic Models
443
13.4.1
Pure-Component Properties
444
13.4.2
Enthalpy
445
13.4.3
Phase Equilibria
445
13.4.4
Using Thermodynamic Models
454
13.5
Case Study: Toluene Hydrodealkylation Process
457
13.6
Summary
460
References
460
Problems
461
Chapter
14
Process Optimization
465
14.1
Background Information on Optimization
465
14.1.1
Common Misconceptions
467
14.1.2
Estimating Problem Difficulty
469
14.1.3
Тор
-Down
and Bottom-Up Strategies
470
14.1.4
Communication of Optimization Results
471
14.2
Strategies
471
14.2.1
Base Case
471
14.2.2
Objective Functions
473
14.2.3
Analysis of the Base Costs
474
14.2.4
Identifying and Prioritizing Key Decision Variables
475
14.3
Topological Optimization
476
24.3.1
Introduction
476
14.3.2
Elimination of Unwanted Nonhazardous By-Products
or Hazardous Waste Streams
477
14.3.3
Elimination and Rearrangement of Equipment
479
14.3.4
Alternative Separation Schemes and Reactor
Configurations
482
xii
Contents
14.4
Parametric
Optimization
484
14.4.1
Single-Variable Optimization: A Case Study on T-201,
the
DME
Separation Column
485
14.4.2
Two-Variable Optimization: The Effect of Pressure and
Reflux Ratio on T-201, the
DME
Separation Column
486
14.4.3
Flowsheet Optimization Using Key Decision Variables
491
14.5
Lattice Search Techniques versus Response Surface
Techniques
496
14.6
Process Flexibility and the Sensitivity of the Optimum
497
14.7
Optimization in Batch Systems
497
14.7.2
Problem of Scheduling Equipment
498
14.7.2
Problem of Optimum Cycle Time
503
14.8
Summary
506
References
507
Short Answer Questions
507
Problems
507
Chapter
15
Pinch Technology
521
15.1
Introduction
521
15.2
Heat Integration and Network Design
522
15.3
Composite Temperature-Enthalpy Diagram
539
15.4
Composite Enthalpy Curves for Systems without a Pinch
540
15.5
Using the Composite Enthalpy Curve to Estimate Heat-Exchanger
Surface Area
541
15.6
Effectiveness Factor (F) and the Number of Shells
545
15.7
Combining Costs to Give the EAOC for the Network
552
15.8
Other Considerations
554
15.8.1
Materials of Construction and Operating Pressure
Issues
554
15.8.2
Problems with Multiple Utilities
558
15.8.3
Handling Streams with Phase Changes
558
15.9
Heat-Exchanger Network Synthesis Analysis and Design
(HENSAD) Program
559
15.10
Mass-Exchange Networks
560
15.11
Summary
570
References
570
Short Answer Questions
571
Problems
572
SEOI0N4 ANALYSIS OF PROCESS PERFORMANCE
579
Chapter
16
Process Input/Output Models
583
16.1
Representation of Process Inputs and Outputs
584
16.2
Analysis of the Effect of Process Inputs on Process Outputs
587
Contents xiii
16.3
A Process Example
588
16.4
Summary
590
Problems
591
Chapter
17
Tools for Evaluating Process Performance
593
17.1
Key Relationships
593
17.2
Thinking with Equations
595
37.2.1
GENI
595
17.2.2
Predicting Trends
595
17.3
Base-Case Ratios
597
17.4
Analysis of Systems Using Controlling Resistances
599
17.5
Graphical Representations
601
17.5.2
The Moody Diagram for Friction Factors
601
17.5.2
The System Curve for Frictional Losses
602
17.5.3
The T-Q Diagram for Heat Exchangers
604
17.6
Summary
606
Reference
607
Problems
607
Chapter
18
Performance Curves for Individual Unit Operations
609
18.1
Applications to Heat Transfer
611
18.2
Application to Fluid Flow
617
18.2.1
Pump and System Curves
617
18.2.2
Regulating Flowrates
623
18.2.3
Reciprocating or Positive Displacement Pumps
627
18.2.4
Net Positive Suction Head
627
18.2.5
Compressors
631
18.3
Application to Separation Problems
633
18.3.1
Separations with Mass Separating Agents
633
18.3.2
Distillation
639
18.4
Summary
647
Reference
648
Short Answer Questions
648
Problems
650
Chapter
19
Performance of Multiple Unit Operations
659
19.1
Analysis of a Reactor with Heat Transfer
659
19.2
Performance of a Distillation Column
664
19.3
Performance of a Heating Loop
671
19.4
Performance of the Feed Section to a Process
677
19.5
Summary
681
References
682
Short Answer Questions
682
Problems
682
XIV
Contents
Chapter
20
Reactor Performance
699
20.1
Production of Desired Product
701
20.2
Reaction Kinetics and Thermodynamics
703
20.2.1
Reaction Kinetics
703
20.2.2
Thermodynamic Limitations
705
20.3
The Chemical Reactor
706
20.4
Heat Transfer in the Chemical Reactor
712
20.5
Reactor System Case Studies
715
20.5.1
Replacement of Catalytic Reactor in Benzene Process
716
20.5.2
Replacement of Cumene Catalyst
721
20.5.3
Increasing Acetone Production
726
20.6
Summary
730
References
731
Short Answer Questions
731
Problems
732
Chapter
21
Regulating Process Conditions
737
21.1
A Simple Regulation Problem
738
21.2
The Characteristics of Regulating Valves
740
21.3
Regulating Flowrates and Pressures
742
21.4
The Measurement of Process Variables
746
21.5
Common Control·Strategies Used in Chemical Processes
746
21.5.1
Feedback Control and Regulation
747
21.5.2
Feed-Forward Control and Regulation
749
21.5.3
Combination Feedback and Feed-Forward Control
751
21.5
A Cascade Regulation
752
21.6
Exchanging Heat and Work between Process and Utility
Streams
753
21.6.1
Increasing the Pressure of a Process Stream
and Regulating Its Flowrate
754
21.6.2
Exchanging Heat between Process Streams
and Utilities
756
21.6.3
Exchanging Heat between Process Streams
761
21.7
Case Studies
761
21.7.2
The Cumene Reactor, R-801
761
21.7.2
A Basic Control System for a Binary Distillation
Column
763
21.7.3
A More Sophisticated Control System for a Binary
Distillation Column
766
21.8
Summary
767
References
768
Problems
768
Contents
XV
Chapter
22
Process Troubleshooting and Debottlenecking
773
22.1
Recommended Methodology
775
22.1.2
Elements of Problem-Solving Strategies
775
22.1.2
Application to Troubleshooting Problems
778
22.2
Troubleshooting Individual Units
780
22.2.1
Troubleshooting a Packed-Bed Absorber
780
22.2.2
Troubleshooting the Cumene Process Feed Section
784
22.3
Troubleshooting Multiple Units
787
22.3.1
Troubleshooting Off-Specification Acrylic Acid Product
787
22.3.2
Troubleshooting Steam Release in Cumene Reactor
789
22.4
A Process Troubleshooting Problem
792
22.5
Debottlenecking Problems
798
22.6
Summary
799
References
799
Problems
799
SECTION
5
THE IMPACT OF CHEMICAL ENGINEERING DESIGN ON SOCIETY
809
Chapter
23
Ethics and Professionalism
811
23.1
Ethics
812
23.1.1
Moral Autonomy
813
23.1.2
Rehearsal
814
23.1.3
Reflection in Action
815
23.1.4
Mobile Truth
816
23.1.5
Nonprofessional
Responsibilities
818
23.1.6
Duties and Obligations
819
23.1.7
Codes of Ethics
820
23.1.8
Whistle-Blowing
823
23.1.9
Ethical Dilemmas
828
23.1.10
Additional Ethics Heuristics
829
23.1.11
Other Resources
829
23.2
Professional Registration
833
23.2.1
Engineer-in-Training
834
23.2.2
Registered Professional Engineer
838
23.3
Legal Liability
839
23.4
Business Codes of Conduct
841
23.5
Summary
842
References
842
Problems
844
XVI
Contents
Chapter
24
Health, Safety, and the Environment
847
24.1
Risk Assessment
848
24.1.1
Accident Statistics
848
24.1.2
Worst-Case Scenarios
849
24.1.3
The Role of the Chemical Engineer
850
24.2
Regulations and Agencies
851
24.2.1 OSHA
and NIOSH
852
24.2.2
Environmental Protection Agency (EPA)
858
24.2.3
Nongovernmental Organizations
862
24.3
Fires and Explosions
863
24.3.1
Terminology
863
24.3.2
Pressure-Relief Systems
865
24.4
Process Hazard Analysis
865
24.4.1
HAZOP
867
24.4.2
Dow Fire
&
Explosion Index and Chemical Exposure
Index
868
24.5
Chemical Safety and Hazard Investigation Board
875
24.6
Inherently Safe Design
875
24.7
Summary
876
24.8
Glossary
876
References
878
Problems
879
Chapter
25
Green Engineering
881
25.1
Environmental Regulations
881
25.2
Environmental Fate of Chemicals
883
25.3
Green Chemistry
886
25.4
Pollution Prevention during Process Design
887
25.5
Analysis of a PFD for Pollution Performance and Environmental
Performance
890
25.6
An Example of the Economics of Pollution Prevention
891
25.7
Life Cycle Analysis
892
25.8
Summary
893
References
894
Problems
895
SECTION
б
INTERPERSONAL AND COMMUNICATION SKILLS
897
Chapter
26
Teamwork
899
26.1
Groups
899
26.1.1
Characteristics of Effective Groups
900
26.1.2
Assessing and Improving the Effectiveness of a Group
26.1.3
Organizational Behaviors and Strategies
905
903
Contents
XVII
26.2 Group Evolution 910
26.2.1
Forming
910
26.2.2
Storming
911
26.2.3 Norming 912
26.2.4
Performing
913
26.3 Teams and Teamwork 913
26.3.1
When Groups become Teams
914
26.3.2
Unique Characteristics of Teams
915
26.4
Misconceptions
916
26.4.1
Team Exams
917
26.4.2
Overreliance on Team Members
917
26.5
Learning in Teams
917
26.6
Other Reading
918
26.7
Summary
920
References
920
Problems
921
Appendix A Cost Equations and Curves for the CAPCOST Program
923
A.1
A.2
923
941
A.3
Appendix
В
Purchased Equipment Costs
Pressure Factors
941
A.2.1 Pressure Factors for Process Vessels
941
A.2.2 Pressure Factors for Other Process Equipment
Material Factors and Bare Module Factors
945
A.3.1 Bare Module
ană
Material Factors for Heat Exchangers,
Process Vessels, and Pumps
945
A.3.2 Bare Module and Material Factors for the Remaining Process
Equipment
949
References
954
Information for the Preliminary Design of Eleven Chemical
Processes
955
B.I
DME
Production, Unit
200 956
B.I.I Process Description
956
B.1.2 Reaction Kinetics
960
B.1.3 Simulation (CHEMCAD) Hints
961
B.1.4 References
961
B.2 Ethyl Benzene Production, Unit
300 962
B.2.1 Process Description
962
B.2.2 Reaction Kinetics
963
B.2.3 Simulation (CHEMCAD) Hints
969
B.2.4 References
970
B.3
Styrene
Production, Unit
400 970
B.3.1 Process Description
970
B.3.2 Reaction Kinetics
971
xviii Contents
8.3.3
Simulation
(CHEMCAD) Hints
978
8.3.4
References
978
B.4 Drying Oil Production, Unit
500 978
B.4.1 Process Description
978
BA.2 Reaction Kinetics
980
B.4.3 Simulation (CHEMCAD) Hints
980
BAA Reference
984
B.5 Production of Maleic Anhydride from Benzene, Unit
600 984
B.5.1 Process Description
984
B.5.2 Reaction Kinetics
985
B.5.3 Simulation (CHEMCAD) Hints
990
B.5A References
990
B.6
Ethylene
Oxide Production, Unit
700 991
B.6.1 Process Description
991
B.6.2 Reaction Kinetics
991
B.6.3 Simulation (CHEMCAD) Hints
1000
B.6A References
1000
B.7 Formalin Production, Unit
800 1000
B.7.1 Process Description
1000
B.7.
2
Reaction Kinetics
1001
B.7.3 Simulation (CHEMCAD) Hints
1001
B.7.4 References
1007
B.8 Batch Production of L-Phenylalanine and L-Aspartic Acid,
Unit
900 1007
B.8.1 Process Description
1007
B.8.2 Reaction Kinetics
1008
B.8.3 References
1015
B.9 Acrylic Acid Production via the Catalytic Partial Oxidation
of Propylene
1015
B.9.1 Process Description
1016
B.9.2 Reaction Kinetics and Reactor Configuration
1018
B.9.3 Simulation (CHEMCAD) Hints
1018
B.9.4 References
1026
B.10 Production of Acetone via the Dehydrogenation of Isopropyl
Alcohol
(IPA),
Unit
1100 1026
B.10.1 Process Description
1027
B.10.2 Reaction Kinetics
1034
B.10.3 Simulation (CHEMCAD) Hints
1034
B.10.4 References
1034
B.ll Production of Heptenes from Propylene and
Butènes,
Unit
1200 1035
B.U.l Process Description
1035
B.11.2 Reaction Kinetics
1036
B.11.3 Simulation (CHEMCAD) Hints
1044
B.11.4 Reference
1044
Index
1045
Material
on the CD-ROM
Chapter
0
Outcomes Assessment
Chapter
27
O.I
Student
t
Self-Assessment
0.2
Assessment by Faculty
0.3
Summary
Written and
Oral Communication
27.1
Audience Analysis
27.2
Written Communication
27.2.1
Design Reports
27.2.2
Transmittal Letters or
Memos
27.2.3
Executive Summaries and Abstracts
27.2.4
Other Types of Written Communication
27.2.5
Exhibits (Figures and Tables)
27.2.6
References
27.2.7
Strategies for Writing
27.2.8
WVU Guidelines for Written Design Report
27.3
Oral Communication
27.3.1
Formal Oral Presentations
27.3.2
Briefings
27.3.3
Visual Aids
27.3.4
WVU Oral Presentation Guidelines
27.4
Software and Author Responsibility
27.4.1
Spell Checkers
27.4.2
Thesaurus
27.4.3
Grammar Checkers
27.4.4
Graphs
27.4.5
Tables
XIX
xx
Material
on the CD-ROM
27.4.6
Colors and Exotic Features
27.4.7
Raw Output from Process Simulators
27.5
Summary
References
Problems
Chapter
28
A Report Writing Case Study
28.1
The Assignment Memorandum
28.2
Response Memorandum
28.3
Visual Aids
28.4
Example Reports
28.4.2
An Example of a Portion of a Student Report
28.4.2
An Example of an Improved Student Report
28.5
Checklist of Common Mistakes and Errors
28.5.1
Common Mistakes for Visual Aids
28.5.2
Common Mistakes for Written Text
Appendix
С
Design Projects
Project
1
Increasing the Production of
З-СМого-і-Ргорепе
(Allyl
Chloride) in Unit
600
C.I.I Background
C.1.2 Process Description of the Beaumont Allyl Chloride Facility
C.1.3 Specific Objectives of Assignment
CIA Additional Background Information
C.1.5 Process Design Calculations
Fluidized
Bed Reactor, R-601
C.1.6 Reference
Project
2
Design and Optimization of a New 20,000-Metric-Tons-
per-Year Facility to Produce Allyl Chloride at
La Nueva
Cantina,
Mexico
C.2.1 Background
C.2.2 Assignment
C.2.3 Problem-Solving Methodology
Process Information
Project
3
Scale-Down of Phthalic Anhydride Production at TBWS
Unit
700
C.3.1 Background
C.3.2 Phthalic Anhydride Production
C.3.3 Other Information
C.3.4 Assignment
C.3.5 Report Format
Material
on the CD-ROM
xxi
Project
4
The Design of a New lOO^OO-Metric-Tons-per-Year
Phthalic Anhydride Production Facility
C.4.1 Background
C.4.2 Other Information
C.4.3 Assignment
C.4.4 Report Format
Project
5
Problems at the Cumene Production Facility, Unit
800
C.5.1 Background
C.S.2 Cumene Production Reactions
C.5.3 Process Description
C.5.4 Recent Problems in Unit
800
C.5.5 Other Information
C.5.6 Assignment
C.5.7 Report Format
C.5.8 Process Calculations
Project
6
Design of a New lOO^OO-Metric-Tons-per Year, Cumene
Production Facility
C.6.1 Background
C.6.2 Assignment
C.6.3 Report Format |
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| id | DE-604.BV035460492 |
| illustrated | Illustrated |
| indexdate | 2025-03-20T19:11:00Z |
| institution | BVB |
| isbn | 0135129664 9780135129661 |
| language | English |
| lccn | 2008040404 |
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| owner | DE-703 DE-83 |
| owner_facet | DE-703 DE-83 |
| physical | XXXIII, 1068 S. Ill., graph. Darst. 1 CD-ROM (12 cm) |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | Prentice Hall |
| record_format | marc |
| series2 | Prentice Hall international series in the physical and chemical engineering sciences |
| spelling | Analysis, synthesis, and design of chemical processes Richard Turton ... 3. ed. Upper Saddle River, NJ ; Munich [u.a.] Prentice Hall 2009 XXXIII, 1068 S. Ill., graph. Darst. 1 CD-ROM (12 cm) txt rdacontent n rdamedia nc rdacarrier Prentice Hall international series in the physical and chemical engineering sciences Chemical processes Prozessentwicklung Technik (DE-588)4278925-4 gnd rswk-swf Chemische Verfahrenstechnik (DE-588)4069941-9 gnd rswk-swf Chemischer Prozess (DE-588)4147636-0 gnd rswk-swf Chemischer Prozess (DE-588)4147636-0 s DE-604 Chemische Verfahrenstechnik (DE-588)4069941-9 s Prozessentwicklung Technik (DE-588)4278925-4 s Turton, Richard Sonstige oth Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017380345&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017380345&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Klappentext |
| spellingShingle | Analysis, synthesis, and design of chemical processes Chemical processes Prozessentwicklung Technik (DE-588)4278925-4 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd Chemischer Prozess (DE-588)4147636-0 gnd |
| subject_GND | (DE-588)4278925-4 (DE-588)4069941-9 (DE-588)4147636-0 |
| title | Analysis, synthesis, and design of chemical processes |
| title_auth | Analysis, synthesis, and design of chemical processes |
| title_exact_search | Analysis, synthesis, and design of chemical processes |
| title_full | Analysis, synthesis, and design of chemical processes Richard Turton ... |
| title_fullStr | Analysis, synthesis, and design of chemical processes Richard Turton ... |
| title_full_unstemmed | Analysis, synthesis, and design of chemical processes Richard Turton ... |
| title_short | Analysis, synthesis, and design of chemical processes |
| title_sort | analysis synthesis and design of chemical processes |
| topic | Chemical processes Prozessentwicklung Technik (DE-588)4278925-4 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd Chemischer Prozess (DE-588)4147636-0 gnd |
| topic_facet | Chemical processes Prozessentwicklung Technik Chemische Verfahrenstechnik Chemischer Prozess |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017380345&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017380345&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
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