Magnetic nanoparticles:
Saved in:
| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Weinheim
WILEY-VCH
2009
|
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XIV, 466 S. Ill., graph. Darst. |
| ISBN: | 9783527407903 3527407901 |
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| adam_text |
Titel: Magnetic nanoparticles
Autor: Gubin, Sergej P.
Jahr: 2009
Contents
Preface XI
List of Contributors XIII
1 Introduction 1
Sergey P. Gubin
1.1 Some Words about Nanopartides 1
1.2 Scope 3
1.2.1 Magnetic Nanopartides Inside Us and Everywhere Around Us 4
1.3 The Most Extensively Studied Magnetic Nanopartides
and Their Preparation 5
1.3.1 Metals 6
1.3.2 Nanopartides of Rare Earth Metals 9
1.3.3 Oxidation ofMetallic Nanopartides 10
1.3.4 Magnetic Alloys 11
1.3.4.1 Fe-Co Alloys 11
1.3.5 Magnetic Oxides 13
1.3.6 Final Remarks 19
2 Synthesis of Nanoparticulate Magnetic Materials 25
Vladimir L. Kolesnichenko
2.1 What Makes Synthesis of Inorganic Nanopartides Different
from Bulk Materials? 25
2.2 Synthesis of Magnetic Metal Nanopartides 28
2.2.1 Reduction of Metal Salts in Solution 29
2.2.1.1 Electron Transfer Reduction 29
2.2.1.2 Reduction via Intermediate Complexes 32
2.2.2 Thermal Decomposition Reactions 36
2.2.2.1 Decomposition of Metal Carbonyls 36
2.2.2.2 Decomposition of Metal Alkene and Arene Complexes 38
2.2.3 Combination Methods Used for Synthesis of Alloy
Nanopartides 39
Magnetic Nanopartides. Sergey P. Gubin
© 20O9 WILEY-VCH Verlag GmbH Co. KGaA, Weinheim
ISBN: 978-3-527-40790-3
VI Contents
2.3 Synthesis ofMagnetic Metal Oxide Nanopartides 40
2.3.1 Reactions of Hydrolysis 40
2.3.1.1 Hydrolysis in Aqueous Solutions 40
2.3.1.2 Hydrolysis in Nonaqueous Solutions 42
2.3.2 Oxidation Reactions 46
2.3.3 Thermal Decomposition of Metal Complexes with O-Donor
Ligands 47
2.4 Technology ofthe Preparation ofMagnetic Nanopartides 49
2.4.1 Stabilizing Agents in Homogeneous Solution Techniques 50
2.4.2 Heterogeneous Solution Techniques 51
2.5 Conclusions 53
3 Magnetic Metallopolymer Nanocomposites: Preparation
and Properties 59
Gulzhian I. Dzhardimalieva, Anatolii D. Pomogailo,
Aleksander 5. Rozenberg and Marcin Leonowicz
3.1 Introduction 59
3.2 The General Methods of Synthesis and Characterization ofMagnetic
Nanopartides in a Polymer Matrix 60
3.2.1 Magnetic Nanopartides in Inorganic Matrices 60
3.2.2 Magnetic Nanopartides in Polymer Matrices 60
3.2.3 Preparation ofMagnetic Polymer Nanocomposites
in Magnetic Fields 63
3.2.4 Peculiarities ofMagnetic Behavior of Metallic Nanopartides
in Polymer Matrix 63
3.3 Magnetic Metal Nanopartides in Stabilizing the Polymer
Matrix In Situ via Thermal Transformations of Metal-Containing
Monomers 67
3.3.1 The Kinetics of Thermolysis of Metal-Containing Monomers 68
3.3.1.1 Dehydration 68
3.3.1.2 Polymerization 69
3.3.1.3 Kinetics of Decarboxylation 69
3.3.2 The Topography and Structure ofMagnetic Metallopolymer
Nanocomposites 75
3.3.3 The Magnetic Properties ofthe Metallopolymer
Nanocomposites 78
3.4 Conclusion 82
Acknowledgments 83
4 Magnetic Nanocomposites Based on the Metal-Containing
(Fe, Co, Ni) Nanopartides Insidethe Polyethylene Matrix 87
Cleb Yu Yurkov, Sergey P. Gubin, and Evgeny A. Ovchenkov
4.1 Introduction 87
4.2 Experimental Details 88
4.2.1 Synthesis 88
Contents I VII
4.2.2 Composition and Structure of Magnetic Nanometallopolymers 92
4.3 Magnetic Properties of Metal-Containing Nanoparticles 93
4.3.1 Iron Containing Nanoparticles 93
4.3.2 Iron Oxide Nanoparticles 101
4.3.3 Cobalt Nanoparticles 104
4.3.4 Co@Fe2O3 Particles 106
4.4 FMR Investigations of Nanocomposites 108
4.5 Conclusions 112
Acknowledgments 114
5 Organized Ensembles of Magnetic Nanoparticles:
Preparation, Structure, and Properties 117
Cennady B. Khomutov and Yury A. Koksharov
5.1 Introduction 117
5.2 Two-Dimensional Systems: Layers and Nanofilms 119
5.2.1 Self-AssembledNanostructures 121
5.2.2 Langmuir-BlodgettTechnique 124
5.2.3 Layer-by-Layer Assembly 130
5.2.3.1 Supported Films 131
5.2.3.2 Nanofdm Capsules 134
5.2.3.3 Free-Standing and Free-Floating Films 135
5.2.4 Bulk Phase Self-Assembled Sheetlike Nanofilms 137
5.3 Anisotropie and Quasilinear (1D) Systems 145
5.3.1 Synthesis under Applied Magnetic Field 146
5.3.2 Ligand Effects and Synthesis in Nanostructured Media 148
5.3.3 Quasilinear Nanoparticulate Structures 153
5.3.4 Templated Structures 156
5.3.5 Nanorubes 160
5.4 Pattemed, Seif-Organized, Composite, and Other Complex
Magnetic Nanoparticulate Nanostructures 163
5.5 Bioinorganic Magnetic Nanostructures 170
5.6 Magnetic Properties of Organized Ensembles of Magnetic
Nanoparticles 174
5.7 Conclusions and Perspectives 182
Acknowledgments 183
6 Magnetism of Nanoparticles: Effects of Size, Shape,
and Interactions 197
Yury A. Koksharov
6.1 Introduction 197
6.2 Magnetism of Nanoparticles in the View of Atomic
and Solid State Physics 198
6.3 Magnetic Finite-Size Effects and Characteristic Magnetic Lengths.
Single-Domain Particles 199
6.4 Shape Effects 208
VIII Contents
6.5 Superparamagnetism 210
6.6 Surface Effects 214
6.7 Matrix EfFects 220
6.8 Interparticle Interaction EfFects 223
6.9 Nanoparticles of Typical Magnetic Materials: Illustrative
Examples 227
6.10 Antiferromagnetic Nanoparticles 232
6.11 Semiconductor Magnetic Nanoparticles 233
6.11.1 Magnetism of Intrinsic and Diluted Magnetic
Semiconductors 233
6.11.2 Unusual Magnetism of Magnetic Semiconductors
and Role ofNanosize Effects 235
6.12 Some Applications of Magnetic Nanoparticles 238
6.12.1 High-Density Information Magnetic Storage 238
6.12.2 Traditional and New Applications of Ferrofluids 240
6.12.3 Magnetic Nanoparticles and Spintronics 244
6.13 Final Remarks 246
7 Electron Magnetic Resonance of Nanoparticles:
Superparamagnetic Resonance 255
Jörns Kliava
7.1 Introduction 255
7.2 Superparamagnetic Resonance Spectrum in a Disordered
System 257
7.3 Resonance Magnetic Field 259
7.4 Resonance Lineshapes 263
74.1 Damped Gyromagnetic Precession 263
7.4.1.1 Defmitions 263
7.4.1.2 The Bloch-Bloembergen Equation 265
7.4.1.3 The Modified Bloch Equation 268
7.4.1.4 The Gilbert Equation 269
7.4.1.5 The Landau- Lifshitz Equation 269
7.4.1.6 The Callen Equation 271
7.4.2 Linewidths and Apparent Shift ofthe Resonance Field 272
7A3 Angular Dependence ofthe Linewidth 274
7.5 Superparamagnetic Narrowing ofthe Resonance Spectra 275
7.5.1 De Biasi and Devezas model 275
7.5.2 Raikher and Stepanov Model 278
7.6 Nanopartide Size and Shape Distribution 279
7.6.1 Distribution of Diameters 279
7.6.2 Nonsphericity of Nanoparticles: Distribution of Demagnetizing
Factors 280
7.6.3 Joint Distribution of Diameters and Demagnetizing Factors 285
7.7 Superparamagnetic Resonance in Oxide Glasses:
Some Experimental Results 287
Contents IX
7.7.1 Lithium Borate Glass 287
7.7.2 Sol-Gel Silica Glass 292
7.7.3 Potassium-Alumino-Borate Glass 295
7.7.4 Gadolinium-Containing Multicomponent Oxide Glass 297
7.8 Conclusions and Prospective 297
8 Micromagnetics of Small Ferromagnetic Particles 303
Nickolai A. Usov and Yury B. Grebenshchikov
8.1 Introduction 303
8.2 Particle Morphology and Single-Domain Radius 306
8.2.1 Quasiuniform States 306
8.2.1.1 Particles of Perfect Geometrical Shape 306
8.2.1.2 Particle of Quasiellipsoidal Shape 310
8.2.2 Nonuniform States 313
8.2.2.1 Spherical Particle 314
8.2.2.2 Ellipsoidal Partide 317
8.2.2.3 Cylindrical Particle 319
8.2.2.4 Cubic Particle 321
8.2.3 Effective Single-Domain Radius 322
8.3 Surface and Interface Effects 322
8.3.1 Brown's Surface Anisotropy 324
8.3.2 Surface Spin Disorder 327
8.3.3 Interface Boundary Condition 330
8.4 Thermally Activated Switching 332
8.4.1 Analytical Estimates ofthe Relaxation Time 333
8.4.2 Stochastic Langevin Equation 334
8.4.3 Simple Examples 335
8.4.3.1 Uniaxial Anisotropy 335
8.4.3.2 Nonsymmetrical Case 336
8.4.3.3 Cubic Anisotropy 339
8.4.4 Nonuniform Modes 341
8.5 Conclusions 343
9 High-Spin Polynuclear Carboxylate Complexes
and Molecular Magnets with VII and VIII Group 3d-Metals 349
Igor L Eremenko, Aleksey A. Sidorov, and Mikhail A Kiskin
9.1 Introduction 349
9.2 High-Spin 3d-Metal Pivalate Polymers as a Good Starting
Spin Materials 351
9.3 Chemical Design of High-Spin Polynuclear Structures
with Different Magnetic Properties 365
9.4 Pivalate-Bridged Heteronuclear Magnetic Species 374
9.5 Pivalate-Based Single Molecular Magnets 385
9.6 Conclusions 388
X Contents
10 Biomedical Applications ofMagnetic Nanoparticles 393
Vladimir N. Nikiforov and Elena Yu. Filinova
10.1 Introduction 393
10.2 Biocompatibility ofMagnetic Nanoparticles 397
10.3 Magnetic Separation for Purification and Immunoassay 401
10.3.1 Cell Labeling for Separation 402
10.3.2 Magnetic Separator Design 404
10.3.3 The Biomedicine Applications 405
10.3.4 The Immunomagnetic Separation 405
10.3.5 Basic Principles ofMagnetic Separation of Proteins
and Peptides 408
10.3.6 Examples ofMagnetic Separations of Proteins and Peptides 410
10.3.6.1 Perspectives 412
10.4 Magnetic Nanoparticles in Cancer Therapy 414
10.4.1 Is a Heat Suitable for Health? 415
10.4.2 Basics of Hyperthermia 419
10.4.3 Magnetic Hyperthermia in Cancer Treatment 422
10.4.4 Prospective of Clinical Applications 425
10.4.5 Conclusions 428
10.5 Targeted Drug and Gene Delivery 429
10.5.1 Magnetic Targeting Local Hyperthermia 431
10.5.2 M agnetic Targeting Applications 431
10.5.3 Targeted Liposomal Drug and Gene Delivery 432
10.5.4 Magnetic Targeting of Radioactivity 436
10.5.5 Other Magnetic Targeting Applications 436
10.5.6 MRI Contrast Enhancement 437
10.6 Prospective of MRI 443
10.7 Problems and Perspectives 444
Index 457 |
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| owner_facet | DE-29T DE-91G DE-BY-TUM DE-703 DE-634 DE-19 DE-BY-UBM DE-83 DE-526 DE-11 |
| physical | XIV, 466 S. Ill., graph. Darst. |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | WILEY-VCH |
| record_format | marc |
| spelling | Magnetic nanoparticles ed. by Sergey P. Gubin Weinheim WILEY-VCH 2009 XIV, 466 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Nanomatériaux - Propriétés magnétiques Nanoparticules Nanoparticles Magnetic properties Nanostructures Magnetic properties Nanostrukturiertes Material (DE-588)4342626-8 gnd rswk-swf Nanopartikel (DE-588)4333369-2 gnd rswk-swf Magnetwerkstoff (DE-588)4136920-8 gnd rswk-swf Magnetteilchen (DE-588)4406122-5 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Magnetteilchen (DE-588)4406122-5 s Nanopartikel (DE-588)4333369-2 s DE-604 Magnetwerkstoff (DE-588)4136920-8 s Nanostrukturiertes Material (DE-588)4342626-8 s 1\p DE-604 Gubin, Sergej P. Sonstige (DE-588)137982704 oth text/html http://deposit.dnb.de/cgi-bin/dokserv?id=3059960&prov=M&dok_var=1&dok_ext=htm Inhaltstext HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017368208&sequence=000004&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Magnetic nanoparticles Nanomatériaux - Propriétés magnétiques Nanoparticules Nanoparticles Magnetic properties Nanostructures Magnetic properties Nanostrukturiertes Material (DE-588)4342626-8 gnd Nanopartikel (DE-588)4333369-2 gnd Magnetwerkstoff (DE-588)4136920-8 gnd Magnetteilchen (DE-588)4406122-5 gnd |
| subject_GND | (DE-588)4342626-8 (DE-588)4333369-2 (DE-588)4136920-8 (DE-588)4406122-5 (DE-588)4143413-4 |
| title | Magnetic nanoparticles |
| title_auth | Magnetic nanoparticles |
| title_exact_search | Magnetic nanoparticles |
| title_full | Magnetic nanoparticles ed. by Sergey P. Gubin |
| title_fullStr | Magnetic nanoparticles ed. by Sergey P. Gubin |
| title_full_unstemmed | Magnetic nanoparticles ed. by Sergey P. Gubin |
| title_short | Magnetic nanoparticles |
| title_sort | magnetic nanoparticles |
| topic | Nanomatériaux - Propriétés magnétiques Nanoparticules Nanoparticles Magnetic properties Nanostructures Magnetic properties Nanostrukturiertes Material (DE-588)4342626-8 gnd Nanopartikel (DE-588)4333369-2 gnd Magnetwerkstoff (DE-588)4136920-8 gnd Magnetteilchen (DE-588)4406122-5 gnd |
| topic_facet | Nanomatériaux - Propriétés magnétiques Nanoparticules Nanoparticles Magnetic properties Nanostructures Magnetic properties Nanostrukturiertes Material Nanopartikel Magnetwerkstoff Magnetteilchen Aufsatzsammlung |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=3059960&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017368208&sequence=000004&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT gubinsergejp magneticnanoparticles |