Integrated design and control of continuous suspension crystallization:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Düsseldorf
VDI-Verl.
2008
|
| Edition: | Als Ms. gedr. |
| Series: | Fortschrittberichte VDI
Reihe 3, Verfahrenstechnik ; 895 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XIV, 163 S. graph. Darst. 21 cm |
| ISBN: | 9783183895038 |
Staff View
MARC
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| 100 | 1 | |a Grosch, Robert |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Integrated design and control of continuous suspension crystallization |c Robert Grosch |
| 250 | |a Als Ms. gedr. | ||
| 264 | 1 | |a Düsseldorf |b VDI-Verl. |c 2008 | |
| 300 | |a XIV, 163 S. |b graph. Darst. |c 21 cm | ||
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| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Fortschrittberichte VDI : Reihe 3, Verfahrenstechnik |v 895 | |
| 490 | 0 | |a Berichte aus dem Lehrstuhl für Prozesstechnik RWTH Aachen | |
| 502 | |a Zugl.: Aachen, Techn. Hochsch., Diss., 2008 | ||
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Record in the Search Index
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|---|---|
| adam_text | Contents
1 Introduction 1
2 Modeling and dynamics of Suspension crystallization 4
2.1 Basics of Suspension crystallization 4
2.1.1 Physical fundamentals 5
2.1.2 Rate processes 7
2.1.3 Design and Operation of continuous crystallizers in practice . . . 9
2.2 Population balance modeling for crystallization 11
2.2.1 Rate processes in the PBE 13
2.2.2 Coupling of the PBE with the mass balance 14
2.3 Example process modeis 15
2.3.1 A simple MSMPR crystallizer model 15
2.3.2 A batch fines dissolution process 16
2.3.3 A DTB pilot plant crystallizer model 17
2.3.4 A detailed DTB pilot plant crystallizer model 17
2.4 Analysis of crystallizer modeis 18
2.4.1 Dynamics of the simple MSMPR crystallizer model 18
2.4.1.1 Numerical results 18
2.4.1.2 Mechanistic interpretation 20
2.4.2 The status of dynamic analysis in crystallization 21
2.4.3 Conclusions 24
3 Discretization of the process modeis 25
3.1 Existing methods 26
3.1.1 Solution methods for füll CSD 26
3.1.1.1 Analytical transformation to ODE 26
3.1.1.2 Stochastic approaches 27
3.1.1.3 Finite differences (FD) discretization of the PBE ... 28
3.1.1.4 Control volume reformulation 28
3.1.1.5 Method of Weighted Residual (MWR) 30
3.1.1.6 Discussion 32
V
Contents
3.1.2 Solution methods for CSD moments 33
3.1.2.1 Analytical transformation to moment equations .... 33
3.1.2.2 Approximate moment methods 33
3.1.3 QMOM solution of a DTB pilot plant crystallizer model .... 36
3.2 A generalized franiework for QMOM 38
3.2.1 Transformation of the size coordinate 38
3.2.2 Weighting function 39
3.2.3 Quadrature closure 40
3.2.4 Moment equations 42
3.2.5 Overall structure of the system of equations 46
3.2.6 Derivation of the existing approaches to QMOM 48
3.2.7 A QMOM method with Laguerre polynomials 49
3.3 Numerical investigation of QMOM 51
3.3.1 A fines dissolution process 51
3.3.1.1 Transformations 51
3.3.1.2 Forrrmlations 55
3.3.2 A DTB pilot plant crystallizer model 59
3.3.2.1 Scaling 59
3.3.2.2 Transformations 60
3.3.2.3 Choice of weighting function 61
3.3.2.4 Formulation 62
3.3.2.5 Simulation results 62
3.3.2.6 Continuation results M
3.3.3 A detailed DTB pilot plant crystallizer model 66
3.3.3.1 Nurnerical results 67
3.4 Summary and Discussion 69
4 Integration of design and control 74
4.1 Existing approacbes a
4.1.1 The status of design and control Integration ^
4.1.2 Control and design integration in crystallization 8
4.2 Stabüity and Performance constraints in steady-state process
optimization 78
4.2.1 Eigenvalues and process stability 9
4.2.2 Stability boundaries 82
4.2.3 Extension to Performance 85
4.2.4 Bounding of dominant eigenvalues for large parameter variations 86
4.2.5 Feasibility constraints 8*
4.2.6 The overall design and control problem 8^
4.3 Performance constraints in the design and control problem 88
4.3.1 Optimization of the open-loop process 88
4.3.2 Guaranteed stability of the closed-loop crystallization process • 9
VI
Contents
4.3.3 Guaranteed Performance and fast disturbances 93
4.3.3.1 Dynamic Performance bounds 93
4.3.3.2 Optimal economic Performance 94
4.3.3.3 Maximum Performance 96
4.3.4 Uncertainty in kinetic parameters 97
4.4 Discussion of results 101
4.4.1 Comparison of results 101
4.4.1.1 Economic versus dynamic Performance 101
4.4.1.2 Economic Performance versus model uncertainty . . . 104
4.4.2 Analysis of the Performance constraints 104
4.4.2.1 Physical interpretation of the stability boundary . . .104
4.4.2.2 Relation between stability boundaries of the
open-loop and closed-loop processes 105
4.4.2.3 Failure of the Standard tuning rule 105
4.4.3 Integrated design and control 106
4.4.4 Conclusions 106
4.5 Robust nonlinear tuning for a pilot plant crystallizer 107
4.5.1 Crystallizer control 107
4.5.2 DTB pilot plant crystallizer and control loops 109
4.5.3 The nonlinear robust tuning problem 110
4.5.4 Results 111
4.5.5 Behavior for other cases 114
4.5.5.1 Startup 114
4.5.5.2 Product quality change 116
4.5.6 Discussion of results 118
5 Concluding remarks 119
5.1 Summary and Conclusion 119
5.2 Areas for development 120
Appendix 123
A Example processes 123
A.l A simple MSMPR crystallizer model 123
A.l.l Model assumptions 123
A.1.2 Kinetics 124
A.1.3 Parameters 124
A.l.4 Moment model 125
A.1.5 Control of Suspension density 125
A.2 A batch ftnes dissolution process model 126
A.2.1 Model assumptions 126
A.2.2 Fines dissolution 126
VII
Contents
A.2.3 Parameters 126
A.3 A DTB pilot plant crystallizer model 127
A.3.1 Model assumptions 127
A.3.2 Kinetics 128
A.3.3 Fines dissolution 128
A.3.4 Parameters 129
A.3.5 CSD and level control 130
A.4 A detailed DTB pilot plant crystallizer model 131
A.4.1 Model assumptions 131
A.4.2 Kinetics 131
A.4.3 Fines dissolution 133
A.4.4 Parameters 133
B Transformations of the PBE 135
B.l Coordinate transformation of the PBE 135
B.2 Moment transformation of the agglomeration source and sink 137
C The long quotient difference algorithm 141
C.l Introduction .... 141
C.2 The algorithm 142
D Properties of parameter-dependent Laguerre polynomials l45
E Details of QMOM-DODE formulation 147
F Time-domain constraints for the simple MSMPR crystallizer I48
Bibliography 150
|
| any_adam_object | 1 |
| author | Grosch, Robert |
| author_facet | Grosch, Robert |
| author_role | aut |
| author_sort | Grosch, Robert |
| author_variant | r g rg |
| building | Verbundindex |
| bvnumber | BV035203766 |
| classification_rvk | VN 7267 |
| ctrlnum | (OCoLC)316190526 (DE-599)HBZHT015762508 |
| dewey-full | 660.284298 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660.284298 |
| dewey-search | 660.284298 |
| dewey-sort | 3660.284298 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| edition | Als Ms. gedr. |
| format | Thesis Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV035203766 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T21:28:30Z |
| institution | BVB |
| isbn | 9783183895038 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017010185 |
| oclc_num | 316190526 |
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| owner | DE-91G DE-BY-TUM DE-210 DE-634 DE-83 |
| owner_facet | DE-91G DE-BY-TUM DE-210 DE-634 DE-83 |
| physical | XIV, 163 S. graph. Darst. 21 cm |
| publishDate | 2008 |
| publishDateSearch | 2008 |
| publishDateSort | 2008 |
| publisher | VDI-Verl. |
| record_format | marc |
| series | Fortschrittberichte VDI |
| series2 | Fortschrittberichte VDI : Reihe 3, Verfahrenstechnik Berichte aus dem Lehrstuhl für Prozesstechnik RWTH Aachen |
| spelling | Grosch, Robert Verfasser aut Integrated design and control of continuous suspension crystallization Robert Grosch Als Ms. gedr. Düsseldorf VDI-Verl. 2008 XIV, 163 S. graph. Darst. 21 cm txt rdacontent n rdamedia nc rdacarrier Fortschrittberichte VDI : Reihe 3, Verfahrenstechnik 895 Berichte aus dem Lehrstuhl für Prozesstechnik RWTH Aachen Zugl.: Aachen, Techn. Hochsch., Diss., 2008 Kristallisation (DE-588)4033215-9 gnd rswk-swf Prozessmodell (DE-588)4237203-3 gnd rswk-swf Prozessregelung (DE-588)4222919-4 gnd rswk-swf Korngrößenverteilung (DE-588)4032495-3 gnd rswk-swf Suspension (DE-588)4058671-6 gnd rswk-swf Diskretisierung (DE-588)4012469-1 gnd rswk-swf Kontinuierlicher Betrieb (DE-588)4325761-6 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Suspension (DE-588)4058671-6 s Kristallisation (DE-588)4033215-9 s Kontinuierlicher Betrieb (DE-588)4325761-6 s Korngrößenverteilung (DE-588)4032495-3 s Prozessmodell (DE-588)4237203-3 s Diskretisierung (DE-588)4012469-1 s DE-604 Prozessregelung (DE-588)4222919-4 s Aachen (DE-588)2027976-0 gnd uvp Fortschrittberichte VDI Reihe 3, Verfahrenstechnik ; 895 (DE-604)BV001897067 895 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017010185&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Grosch, Robert Integrated design and control of continuous suspension crystallization Fortschrittberichte VDI Kristallisation (DE-588)4033215-9 gnd Prozessmodell (DE-588)4237203-3 gnd Prozessregelung (DE-588)4222919-4 gnd Korngrößenverteilung (DE-588)4032495-3 gnd Suspension (DE-588)4058671-6 gnd Diskretisierung (DE-588)4012469-1 gnd Kontinuierlicher Betrieb (DE-588)4325761-6 gnd |
| subject_GND | (DE-588)4033215-9 (DE-588)4237203-3 (DE-588)4222919-4 (DE-588)4032495-3 (DE-588)4058671-6 (DE-588)4012469-1 (DE-588)4325761-6 (DE-588)4113937-9 |
| title | Integrated design and control of continuous suspension crystallization |
| title_auth | Integrated design and control of continuous suspension crystallization |
| title_exact_search | Integrated design and control of continuous suspension crystallization |
| title_full | Integrated design and control of continuous suspension crystallization Robert Grosch |
| title_fullStr | Integrated design and control of continuous suspension crystallization Robert Grosch |
| title_full_unstemmed | Integrated design and control of continuous suspension crystallization Robert Grosch |
| title_short | Integrated design and control of continuous suspension crystallization |
| title_sort | integrated design and control of continuous suspension crystallization |
| topic | Kristallisation (DE-588)4033215-9 gnd Prozessmodell (DE-588)4237203-3 gnd Prozessregelung (DE-588)4222919-4 gnd Korngrößenverteilung (DE-588)4032495-3 gnd Suspension (DE-588)4058671-6 gnd Diskretisierung (DE-588)4012469-1 gnd Kontinuierlicher Betrieb (DE-588)4325761-6 gnd |
| topic_facet | Kristallisation Prozessmodell Prozessregelung Korngrößenverteilung Suspension Diskretisierung Kontinuierlicher Betrieb Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017010185&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV001897067 |
| work_keys_str_mv | AT groschrobert integrateddesignandcontrolofcontinuoussuspensioncrystallization |