Principles and applications of emulsion polymerization:
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Hoboken, N.J.
Wiley
2008
|
| Subjects: | |
| Online Access: | Publisher description Table of contents only Inhaltsverzeichnis |
| Item Description: | Includes bibliographical references and index |
| Physical Description: | XIII, 252 S. graph. Darst. |
| ISBN: | 9780470124314 0470124318 |
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MARC
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| 100 | 1 | |a Chern, Chorng-Shyan |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Principles and applications of emulsion polymerization |c Chorng-Shyan Chern |
| 264 | 1 | |a Hoboken, N.J. |b Wiley |c 2008 | |
| 300 | |a XIII, 252 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Includes bibliographical references and index | ||
| 650 | 4 | |a Emulsion polymerization | |
| 650 | 0 | 7 | |a Emulsionspolymerisation |0 (DE-588)4121186-8 |2 gnd |9 rswk-swf |
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Record in the Search Index
| _version_ | 1804138320836427776 |
|---|---|
| adam_text | CONTENTS
Preface
xi
1
Introduction
1
1.1
Free
Radical
Polymerization
/ 1
1.1.1
Free Radical Polymerization Mechanisms
/ 1
1.1.2
Free Radical Polymerization Kinetics
/ 3
1.2
Emulsion Polymerization
/ 5
1.2.1
Conventional Emulsion Polymerization
/ 5
1.2.2
Emulsion Polymerization Processes
/ 6
1.2.3
Miniemulsion
Polymerization
/ 8
1.2.4 Microemulsion
Polymerization
/ 9
1.2.5
Inverse Emulsion Polymerization
/ 10
1.3
Colloidal Stability
/ 11
1.3.1
A Critical but Often Ignored Issue
/ 11
1.3.2
Electrostatic Interactions
/ 12
1.3.3
Steric Interactions
/ 13
1.3.4
Mechanical Stability
/ 14
1.4
Some Performance Properties for Industrial Applications
/15
1.4.1
Rheology
/ 15
1.4.2
Film Formation
/ 16
References
/ 19
2
Interfacial
Phenomena
23
2.1
Thermodynamic Consideration
/ 23
2.1.1
Emulsification of Oil in Water
/ 23
2.1.2
Interfaces
/ 25
2.1.3
Surfactant Molecules Adsorbed at an Interface
/ 26
VÍ
CONTENTS
2.2
Surfactants
/ 26
2.2.1
Critical Micelle Concentration (CMC)
/ 27
2.2.2
Hydrophile-Lipophile Balance (HLB)
/ 27
2.2.3
Solubility Parameter
/ 29
2.3
Colloidal Stability
/ 32
2.3.1
Van
der Waals
Forces
/ 32
2.3.2
Electrostatic Interactions
/ 36
2.3.3
Steric Interactions
/ 44
2.3.4
Kinetics of Flocculation
/ 48
References
/ 50
3
Particle Nucleation Mechanisms
53
3.1
Micellar Nucleation
/ 54
3.1.1
Harkins-Smith-Ewart Theory
/ 54
3.1.2
Competitive Absorption of Free Radicals by Micelles and
Particle Nuclei
/ 57
3.2
Homogeneous Nucleation
/ 60
3.2.1
Formation of Particle Nuclei in the Continuous Aqueous
Phase
/ 60
3.2.2 Hansen-Ugelstad-Fitch-Tsai (HUFT)
Model
/ 63
3.3
Coagulative
Nucleation
/ 65
3.3.1
General Features of
Coagulative
Nucleation
/ 65
3.3.2
Coagulative
Nucleation Model Development
/ 66
3.4
Mixed Mode of Particle Nucleation Mechanisms
/ 68
3.5
Surfactant-Free Emulsion Polymerization
/ 71
3.6
Experimental Work on Particle Nucleation
/ 76
3.6.1
A Dilemma about Particle Nucleation Mechanisms
/ 76
3.6.2
Some Representative Experimental Data of Particle
Nucleation
/ 77
3.6.3
Some Potential Techniques for Studying Particle
Nucleation
/ 82
3.6.4
Effects of Surfactant Concentration on Particle
Nucleation
/ 86
3.7
Nonionic and Mixed Surfactant Systems
/ 87
3.7.1
Nonionic Surfactant Systems
/ 88
3.7.2
Mixed
Anionie
and Nonionic Surfactant Systems
/ 89
References
/ 91
CONTENTS
VU
Emulsion
Polymerization Kinetics
95
4.1
Emulsion Polymerization Kinetics
/ 96
4.1.1
Smith-Ewart Theory
/ 96
4.1.2
Pioneering Kinetic Models for Predicting Average Number
of Free Radicals per Particle
/ 100
4.2
Absorption of Free Radicals by Latex Particles
/ 103
4.2.1
Collision- and Diffusion-Controlled Models
/ 104
4.2.2
Propagation-Controlled Model
/ 106
4.2.3
Some Controversial Issues
/ 108
4.3
Desorption of Free Radicals Out of Latex Particles
/ 109
4.3.1
Desorption of Free Radicals in Emulsion
Homopolymerization Systems
/110
4.3.2
Desorption of Free Radicals in Emulsion Copolymerization
Systems
/112
4.3.3
Effect of
Interfacial
Properties on Desorption of Free
Radicals
/ 113
4.4
Growth of Latex Particles
/114
4.4.1
Thermodynamic Consideration
/114
4.4.2
Concentrations of Comonomers in Emulsion
Copolymerization Systems
/ 116
4.4.3
Competitive Growth of Latex Particles
/119
4.5
Polymer Molecular Weight
/ 120
References
/ 123
Miniemulsion
Polymerization
128
5.1
Polymerization in Monomer Droplets
/129
5.2
Stability of Monomer Emulsions
/ 130
5.2.1
Ostwald Ripening Effect
/ 130
5.2.2
Role of Costabilizer in Stabilizing Monomer Emulsions
/ 132
5.3
Type of Costabilizers in
Miniemulsion
Polymerization
/ 133
5.4
Miniemulsion
Polymerization Mechanisms and Kinetics
/ 135
5.4.1
Initial Conditions for
Miniemulsion
Polymerization
Systems
/ 135
5.4.2
Particle Nucleation Mechanisms
/ 136
5.4.3
Effect of Functional Monomers and Initiators on Particle
Nucleation
/140
5.4.4
Polymerization Kinetics
/ 142
VIU
CONTENTS
5.5
Versatility of
Miniemulsion
Polymerization
/ 145
5.5.1
Catalytic Chain Transfer Reaction
/ 147
5.5.2
Living Free Radical Polymerization
/ 147
5.5.3
Step Polymerization
/ 148
References
/ 150
6 Microemulsion
Polymerization
154
6.1
Introduction
/ 154
6.2
Formation and Microstructure of Microemulsions
/ 155
6.2.1
Formation of Microemulsions
/ 155
6.2.2
Factors that Govern
Microemulsion
Structures
/ 157
6.3 O/W Microemulsion
Polymerization
/ 158
6.3.1
General Features
/ 158
6.3.2
Polymerization Mechanisms and Kinetics
/ 159
6.4 W/O Microemulsion
Polymerization
/ 167
6.5
Polymerization in Continuous or Bicontinuous Phases of
Microemulsions
/ 169
References
/170
7
Semibatch
and Continuous Emulsion Polymerizations
175
7.1
Semibatch
Emulsion Polymerization
/ 175
7.1.1
Pseudo-Steady-State Polymerization Behavior
/ 175
7.1.2
Polymerization Mechanisms and Kinetics
/ 177
7.1.3
Mathematical Modeling Studies
/ 186
7.2
Continuous Emulsion Polymerization
/ 187
7.2.1
General Features of Continuous Emulsion Polymerization
Processes
/ 187
7.2.2
Particle Nucleation and Growth Mechanisms
/ 191
7.3
Development of Commercial Continuous Emulsion Polymerization
Processes
/ 194
References
/ 196
8
Emulsion Polymerizations in
Nonuniform
Latex Particles
200
8.1
Origin of
Nonuniform
Latex Particles
/ 200
8.2
Seeded Emulsion Polymerizations
/ 201
CONTENTS
ІХ
8.3
Factors
Affecting Particle Morphology
/ 202
8.3.1
Effect of Initiators
/ 202
8.3.2
Effect of Monomer Addition Methods
/ 203
8.3.3
Effect of Polymer Molecular Weight
/ 204
8.3.4
Effect of Volume Fractions of Polymer Pairs
/ 205
8.3.5
Effect of Polymerization Temperature
/ 205
8.4
Morphology Development in Latex Particles
/ 205
8.4.1
Thermodynamic Considerations
/ 205
8.4.2
Nonequilibrium Morphology Development
/ 206
8.4.3
Techniques for Characterization of Particle
Morphology
/ 210
8.5
Polymerization Kinetics in
Nonuniform
Latex Particles
/ 211
8.5.1
Pioneering Studies
/ 212
8.5.2
Effect of Distribution of Free Radicals in
Nonuniform
Latex
Particles
/ 213
References
/ 220
9
Applications of Emulsion Polymers
223
9.1
Physical Properties of Emulsion Polymers
/ 224
9.1.1
Effect of Polymer Molecular Weight
/ 224
9.1.2
Effect of Polymer Morphology
/ 225
9.1.3
Effect of Crosslinking Reactions
/ 229
9.2
Rheological Properties of Emulsion Polymers
/ 230
9.3
Film Formation of Emulsion Polymers
/ 233
9.4
Foaming and Antifoaming Agents
/ 236
9.5
Wetting
/ 238
9.6
Surface Modifications
/ 241
9.7
Stability of Latex Products
/ 242
References
/ 245
Index
248
|
| adam_txt |
CONTENTS
Preface
xi
1
Introduction
1
1.1
Free
Radical
Polymerization
/ 1
1.1.1
Free Radical Polymerization Mechanisms
/ 1
1.1.2
Free Radical Polymerization Kinetics
/ 3
1.2
Emulsion Polymerization
/ 5
1.2.1
Conventional Emulsion Polymerization
/ 5
1.2.2
Emulsion Polymerization Processes
/ 6
1.2.3
Miniemulsion
Polymerization
/ 8
1.2.4 Microemulsion
Polymerization
/ 9
1.2.5
Inverse Emulsion Polymerization
/ 10
1.3
Colloidal Stability
/ 11
1.3.1
A Critical but Often Ignored Issue
/ 11
1.3.2
Electrostatic Interactions
/ 12
1.3.3
Steric Interactions
/ 13
1.3.4
Mechanical Stability
/ 14
1.4
Some Performance Properties for Industrial Applications
/15
1.4.1
Rheology
/ 15
1.4.2
Film Formation
/ 16
References
/ 19
2
Interfacial
Phenomena
23
2.1
Thermodynamic Consideration
/ 23
2.1.1
Emulsification of Oil in Water
/ 23
2.1.2
Interfaces
/ 25
2.1.3
Surfactant Molecules Adsorbed at an Interface
/ 26
VÍ
CONTENTS
2.2
Surfactants
/ 26
2.2.1
Critical Micelle Concentration (CMC)
/ 27
2.2.2
Hydrophile-Lipophile Balance (HLB)
/ 27
2.2.3
Solubility Parameter
/ 29
2.3
Colloidal Stability
/ 32
2.3.1
Van
der Waals
Forces
/ 32
2.3.2
Electrostatic Interactions
/ 36
2.3.3
Steric Interactions
/ 44
2.3.4
Kinetics of Flocculation
/ 48
References
/ 50
3
Particle Nucleation Mechanisms
53
3.1
Micellar Nucleation
/ 54
3.1.1
Harkins-Smith-Ewart Theory
/ 54
3.1.2
Competitive Absorption of Free Radicals by Micelles and
Particle Nuclei
/ 57
3.2
Homogeneous Nucleation
/ 60
3.2.1
Formation of Particle Nuclei in the Continuous Aqueous
Phase
/ 60
3.2.2 Hansen-Ugelstad-Fitch-Tsai (HUFT)
Model
/ 63
3.3
Coagulative
Nucleation
/ 65
3.3.1
General Features of
Coagulative
Nucleation
/ 65
3.3.2
Coagulative
Nucleation Model Development
/ 66
3.4
Mixed Mode of Particle Nucleation Mechanisms
/ 68
3.5
Surfactant-Free Emulsion Polymerization
/ 71
3.6
Experimental Work on Particle Nucleation
/ 76
3.6.1
A Dilemma about Particle Nucleation Mechanisms
/ 76
3.6.2
Some Representative Experimental Data of Particle
Nucleation
/ 77
3.6.3
Some Potential Techniques for Studying Particle
Nucleation
/ 82
3.6.4
Effects of Surfactant Concentration on Particle
Nucleation
/ 86
3.7
Nonionic and Mixed Surfactant Systems
/ 87
3.7.1
Nonionic Surfactant Systems
/ 88
3.7.2
Mixed
Anionie
and Nonionic Surfactant Systems
/ 89
References
/ 91
CONTENTS
VU
Emulsion
Polymerization Kinetics
95
4.1
Emulsion Polymerization Kinetics
/ 96
4.1.1
Smith-Ewart Theory
/ 96
4.1.2
Pioneering Kinetic Models for Predicting Average Number
of Free Radicals per Particle
/ 100
4.2
Absorption of Free Radicals by Latex Particles
/ 103
4.2.1
Collision- and Diffusion-Controlled Models
/ 104
4.2.2
Propagation-Controlled Model
/ 106
4.2.3
Some Controversial Issues
/ 108
4.3
Desorption of Free Radicals Out of Latex Particles
/ 109
4.3.1
Desorption of Free Radicals in Emulsion
Homopolymerization Systems
/110
4.3.2
Desorption of Free Radicals in Emulsion Copolymerization
Systems
/112
4.3.3
Effect of
Interfacial
Properties on Desorption of Free
Radicals
/ 113
4.4
Growth of Latex Particles
/114
4.4.1
Thermodynamic Consideration
/114
4.4.2
Concentrations of Comonomers in Emulsion
Copolymerization Systems
/ 116
4.4.3
Competitive Growth of Latex Particles
/119
4.5
Polymer Molecular Weight
/ 120
References
/ 123
Miniemulsion
Polymerization
128
5.1
Polymerization in Monomer Droplets
/129
5.2
Stability of Monomer Emulsions
/ 130
5.2.1
Ostwald Ripening Effect
/ 130
5.2.2
Role of Costabilizer in Stabilizing Monomer Emulsions
/ 132
5.3
Type of Costabilizers in
Miniemulsion
Polymerization
/ 133
5.4
Miniemulsion
Polymerization Mechanisms and Kinetics
/ 135
5.4.1
Initial Conditions for
Miniemulsion
Polymerization
Systems
/ 135
5.4.2
Particle Nucleation Mechanisms
/ 136
5.4.3
Effect of Functional Monomers and Initiators on Particle
Nucleation
/140
5.4.4
Polymerization Kinetics
/ 142
VIU
CONTENTS
5.5
Versatility of
Miniemulsion
Polymerization
/ 145
5.5.1
Catalytic Chain Transfer Reaction
/ 147
5.5.2
Living Free Radical Polymerization
/ 147
5.5.3
Step Polymerization
/ 148
References
/ 150
6 Microemulsion
Polymerization
154
6.1
Introduction
/ 154
6.2
Formation and Microstructure of Microemulsions
/ 155
6.2.1
Formation of Microemulsions
/ 155
6.2.2
Factors that Govern
Microemulsion
Structures
/ 157
6.3 O/W Microemulsion
Polymerization
/ 158
6.3.1
General Features
/ 158
6.3.2
Polymerization Mechanisms and Kinetics
/ 159
6.4 W/O Microemulsion
Polymerization
/ 167
6.5
Polymerization in Continuous or Bicontinuous Phases of
Microemulsions
/ 169
References
/170
7
Semibatch
and Continuous Emulsion Polymerizations
175
7.1
Semibatch
Emulsion Polymerization
/ 175
7.1.1
Pseudo-Steady-State Polymerization Behavior
/ 175
7.1.2
Polymerization Mechanisms and Kinetics
/ 177
7.1.3
Mathematical Modeling Studies
/ 186
7.2
Continuous Emulsion Polymerization
/ 187
7.2.1
General Features of Continuous Emulsion Polymerization
Processes
/ 187
7.2.2
Particle Nucleation and Growth Mechanisms
/ 191
7.3
Development of Commercial Continuous Emulsion Polymerization
Processes
/ 194
References
/ 196
8
Emulsion Polymerizations in
Nonuniform
Latex Particles
200
8.1
Origin of
Nonuniform
Latex Particles
/ 200
8.2
Seeded Emulsion Polymerizations
/ 201
CONTENTS
ІХ
8.3
Factors
Affecting Particle Morphology
/ 202
8.3.1
Effect of Initiators
/ 202
8.3.2
Effect of Monomer Addition Methods
/ 203
8.3.3
Effect of Polymer Molecular Weight
/ 204
8.3.4
Effect of Volume Fractions of Polymer Pairs
/ 205
8.3.5
Effect of Polymerization Temperature
/ 205
8.4
Morphology Development in Latex Particles
/ 205
8.4.1
Thermodynamic Considerations
/ 205
8.4.2
Nonequilibrium Morphology Development
/ 206
8.4.3
Techniques for Characterization of Particle
Morphology
/ 210
8.5
Polymerization Kinetics in
Nonuniform
Latex Particles
/ 211
8.5.1
Pioneering Studies
/ 212
8.5.2
Effect of Distribution of Free Radicals in
Nonuniform
Latex
Particles
/ 213
References
/ 220
9
Applications of Emulsion Polymers
223
9.1
Physical Properties of Emulsion Polymers
/ 224
9.1.1
Effect of Polymer Molecular Weight
/ 224
9.1.2
Effect of Polymer Morphology
/ 225
9.1.3
Effect of Crosslinking Reactions
/ 229
9.2
Rheological Properties of Emulsion Polymers
/ 230
9.3
Film Formation of Emulsion Polymers
/ 233
9.4
Foaming and Antifoaming Agents
/ 236
9.5
Wetting
/ 238
9.6
Surface Modifications
/ 241
9.7
Stability of Latex Products
/ 242
References
/ 245
Index
248 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Chern, Chorng-Shyan |
| author_facet | Chern, Chorng-Shyan |
| author_role | aut |
| author_sort | Chern, Chorng-Shyan |
| author_variant | c s c csc |
| building | Verbundindex |
| bvnumber | BV035158752 |
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| callnumber-search | QD281.P6 |
| callnumber-sort | QD 3281 P6 |
| callnumber-subject | QD - Chemistry |
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| ctrlnum | (OCoLC)191697433 (DE-599)BVBBV035158752 |
| dewey-full | 668.9/2 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 668 - Technology of other organic products |
| dewey-raw | 668.9/2 |
| dewey-search | 668.9/2 |
| dewey-sort | 3668.9 12 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie Physik Werkstoffwissenschaften Chemie Chemie-Ingenieurwesen |
| discipline_str_mv | Chemie / Pharmazie Physik Werkstoffwissenschaften Chemie Chemie-Ingenieurwesen |
| format | Book |
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| id | DE-604.BV035158752 |
| illustrated | Illustrated |
| index_date | 2024-07-02T22:49:49Z |
| indexdate | 2024-07-09T21:26:19Z |
| institution | BVB |
| isbn | 9780470124314 0470124318 |
| language | English |
| lccn | 2008003740 |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016965903 |
| oclc_num | 191697433 |
| open_access_boolean | |
| owner | DE-703 DE-91G DE-BY-TUM DE-634 |
| owner_facet | DE-703 DE-91G DE-BY-TUM DE-634 |
| physical | XIII, 252 S. graph. Darst. |
| publishDate | 2008 |
| publishDateSearch | 2008 |
| publishDateSort | 2008 |
| publisher | Wiley |
| record_format | marc |
| spelling | Chern, Chorng-Shyan Verfasser aut Principles and applications of emulsion polymerization Chorng-Shyan Chern Hoboken, N.J. Wiley 2008 XIII, 252 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references and index Emulsion polymerization Emulsionspolymerisation (DE-588)4121186-8 gnd rswk-swf Emulsionspolymerisation (DE-588)4121186-8 s DE-604 http://www.loc.gov/catdir/enhancements/fy0827/2008003740-d.html Publisher description http://www.loc.gov/catdir/enhancements/fy0827/2008003740-t.html Table of contents only Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016965903&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Chern, Chorng-Shyan Principles and applications of emulsion polymerization Emulsion polymerization Emulsionspolymerisation (DE-588)4121186-8 gnd |
| subject_GND | (DE-588)4121186-8 |
| title | Principles and applications of emulsion polymerization |
| title_auth | Principles and applications of emulsion polymerization |
| title_exact_search | Principles and applications of emulsion polymerization |
| title_exact_search_txtP | Principles and applications of emulsion polymerization |
| title_full | Principles and applications of emulsion polymerization Chorng-Shyan Chern |
| title_fullStr | Principles and applications of emulsion polymerization Chorng-Shyan Chern |
| title_full_unstemmed | Principles and applications of emulsion polymerization Chorng-Shyan Chern |
| title_short | Principles and applications of emulsion polymerization |
| title_sort | principles and applications of emulsion polymerization |
| topic | Emulsion polymerization Emulsionspolymerisation (DE-588)4121186-8 gnd |
| topic_facet | Emulsion polymerization Emulsionspolymerisation |
| url | http://www.loc.gov/catdir/enhancements/fy0827/2008003740-d.html http://www.loc.gov/catdir/enhancements/fy0827/2008003740-t.html http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016965903&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT chernchorngshyan principlesandapplicationsofemulsionpolymerization |