Mesocrystals and nonclassical crystallization:
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Chichester
Wiley
2008
|
| Subjects: | |
| Online Access: | Publisher description Table of contents only Inhaltsverzeichnis |
| Physical Description: | XI, 276 S. Ill., graph. Darst. |
| ISBN: | 9780470029817 0470029811 |
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Record in the Search Index
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| adam_text | Contents
Preface
ix
1 Mesocrystals and Nonclassical
Crystallization
1
1.1
Introduction
1
References
6
2
Physico-Chemical Principles of Crystallization
7
2.1
Classical Crystallization
7
2.2
Definition of a Crystal and Crystal Growth
9
2.3
Nucleation Theories
15
2.3.1
Classical Nucleation Theory
15
2.3.2
Experimental Tests of Nucleation Theories
19
2.4
Some Points towards a More Realistic View of
Supersaturation
and Crystallization
19
2.4.1
Concentration Fluctuations and Spinodal Crystallization
19
2.4.2
Reduction of
Supersaturation
by the Formation of Clusters
and Amorphous Intermediates
21
2.5
Thermodynamic and Kinetic Crystallization Pathways
22
2.6
Polymorph Control
25
2.7
Crystal Morphology and the Role of Additives and
Selective Adsorption
28
2.7.1
Crystal Morphology
30
2.7.2
What Determines Adsorption of an Additive?
36
2.8
Properties of Single Crystals and Polycrystals
39
2.8.1
Electrical Polarization
39
2.8.2
Light Refraction and Birefringence
43
2.8.3
Mechanical Properties
44
References
47
3
Examples of Crystals Challenging the Classical Textbook Mechanism
51
3.1
Some
Biomineral
Examples
51
3.1.1
Elongated Magnetite Nanocrystals in Magnetotactic Bacteria
52
vi
Contents
3.1.2
Calcite
with Complex Form and Single Crystal Behavior
in Foraminifera
53
3.1.3
Calcite
with Complex Form and Single Crystal Behavior in
Sea Urchin Spines
56
3.1.4
Calcite
Single Crystals with Complex Form in Coccoliths
57
3.1.5
Morphological Complexity Develops with Time
58
3.2
From Biology to Biomimetics: In Vitro Mineralization Examples
59
3.3
Biomorphs
68
3.4
Other Synthetic Examples
69
References
71
4
Nonclassical Crystallization
73
4.1
Amorphous Precursors
75
4.2
Liquid Precursors
78
4.3
Oriented Attachment
83
4.4
Mesocrystals
96
References
98
5
Self-Assembly and Self-Organization
103
References
106
6
Colloidal Crystals with Spherical Units: Opals and Colloidal
Nanocrystals
107
References 111
7
Mesocrystal Systems
113
7.1
Mesocrystals and Their Properties
113
7.2
Early Reports on Mesocrystals
114
7.3
One-Dimensional Mesocrystals
117
7.4
Two-Dimensional Mesocrystals
118
7.5
Mesocrystals in Biomineralization
122
7.6
Mesocrystals in Gels
129
7.7
Mesocrystals Formed without Additives
135
7.8
Mesocrystals Formed with Simple Ion Additives
138
7.9
Mesocrystals Formed with Polymer Additives
142
7.10
Mesocrystals in Nonaqueous Systems
152
7.11
Mesocrystals Formed via Solid-State Reactions
157
7.11.1
Solid Matrices for Mesocrystal Formation
157
7.11.2
Topotactic Reactions
159
7.12
Liquid Crystals, Tactoids, Somatoids, and Schiller Layers
163
References
173
8
Mechanisms of Mesocrystal Formation
179
8.1
Principal Mechanisms Leading to Mesocrystals
179
8.2
Conditions for Mesocrystal Formation
186
Contents
vii
8.3
Alignment by Colloidal Forces, Capillarity and Other Short-Ranged
Physical Fields
190
8.3.1
Alignment by Capillary Forces
190
8.3.2
Alignment by
Hydrophobie
Forces and Interface Energies
192
8.3.3
Alignment by Minimization of the
Interfacial
Energy
192
8.3.4
Alignment by Additive Coding of Nanoparticles
194
8.3.5
Alignment by a Mechanical Stress Field
196
8.4
The Role of Magnetic Fields
198
8.5
The Role of
Dipole
and Polarization Forces
204
8.5.1
Polarization Forces
204
8.6
The Role of External Electric Fields
219
8.7
Self-Similar Assembly and Shape Constraints
222
8.8
Shaping of Mesocrystals
226
8.9
Mesocrystals as Intermediates in Single Crystal Formation
228
References
233
9
Analysis of Mesocrystals
237
9.1
Nucleation and Growth of Primary Nanoparticles
238
9.2
Rapid Aggregation and Formation of Randomly
Oriented Aggregates
239
9.3
Mesocrystal Formation
239
9.4
Fusion of the Mesocrystal to a Single Crystal/Ripening and
Ion-Mediated Recrystallization Towards an Outer Single
Crystalline Shell
240
9.5
Analytical Techniques for Mesocrystals
241
References
244
10
Tuning of Properties
247
References
249
11
A Unifying Crystallization Mechanism
251
References
255
12
Analogy between Oriented Attachment or Hierarchically Structured
Crystals and Polymers
257
12.1
Analogy between Oriented Attachment and Polymerization
259
12.2
Structural Levels in Hierarchically Structured Crystals and
Biopolymers 263
References
264
13
Summary and Outlook
265
13.1
Summary
265
13.2
Outlook
267
References
270
Index
271
|
| adam_txt |
Contents
Preface
ix
1 Mesocrystals and Nonclassical
Crystallization
1
1.1
Introduction
1
References
6
2
Physico-Chemical Principles of Crystallization
7
2.1
Classical Crystallization
7
2.2
Definition of a Crystal and Crystal Growth
9
2.3
Nucleation Theories
15
2.3.1
Classical Nucleation Theory
15
2.3.2
Experimental Tests of Nucleation Theories
19
2.4
Some Points towards a More Realistic View of
Supersaturation
and Crystallization
19
2.4.1
Concentration Fluctuations and 'Spinodal Crystallization'
19
2.4.2
Reduction of
Supersaturation
by the Formation of Clusters
and Amorphous Intermediates
21
2.5
Thermodynamic and Kinetic Crystallization Pathways
22
2.6
Polymorph Control
25
2.7
Crystal Morphology and the Role of Additives and
Selective Adsorption
28
2.7.1
Crystal Morphology
30
2.7.2
What Determines Adsorption of an Additive?
36
2.8
Properties of Single Crystals and Polycrystals
39
2.8.1
Electrical Polarization
39
2.8.2
Light Refraction and Birefringence
43
2.8.3
Mechanical Properties
44
References
47
3
Examples of Crystals Challenging the Classical Textbook Mechanism
51
3.1
Some
Biomineral
Examples
51
3.1.1
Elongated Magnetite Nanocrystals in Magnetotactic Bacteria
52
vi
Contents
3.1.2
Calcite
with Complex Form and Single Crystal Behavior
in Foraminifera
53
3.1.3
Calcite
with Complex Form and Single Crystal Behavior in
Sea Urchin Spines
56
3.1.4
Calcite
Single Crystals with Complex Form in Coccoliths
57
3.1.5
Morphological Complexity Develops with Time
58
3.2
From Biology to Biomimetics: In Vitro Mineralization Examples
59
3.3
Biomorphs
68
3.4
Other Synthetic Examples
69
References
71
4
Nonclassical Crystallization
73
4.1
Amorphous Precursors
75
4.2
Liquid Precursors
78
4.3
Oriented Attachment
83
4.4
Mesocrystals
96
References
98
5
Self-Assembly and Self-Organization
103
References
106
6
Colloidal Crystals with Spherical Units: Opals and Colloidal
Nanocrystals
107
References 111
7
Mesocrystal Systems
113
7.1
Mesocrystals and Their Properties
113
7.2
Early Reports on Mesocrystals
114
7.3
One-Dimensional Mesocrystals
117
7.4
Two-Dimensional Mesocrystals
118
7.5
Mesocrystals in Biomineralization
122
7.6
Mesocrystals in Gels
129
7.7
Mesocrystals Formed without Additives
135
7.8
Mesocrystals Formed with Simple Ion Additives
138
7.9
Mesocrystals Formed with Polymer Additives
142
7.10
Mesocrystals in Nonaqueous Systems
152
7.11
Mesocrystals Formed via Solid-State Reactions
157
7.11.1
Solid Matrices for Mesocrystal Formation
157
7.11.2
Topotactic Reactions
159
7.12
Liquid Crystals, Tactoids, Somatoids, and Schiller Layers
163
References
173
8
Mechanisms of Mesocrystal Formation
179
8.1
Principal Mechanisms Leading to Mesocrystals
179
8.2
Conditions for Mesocrystal Formation
186
Contents
vii
8.3
Alignment by Colloidal Forces, Capillarity and Other Short-Ranged
Physical Fields
190
8.3.1
Alignment by Capillary Forces
190
8.3.2
Alignment by
Hydrophobie
Forces and Interface Energies
192
8.3.3
Alignment by Minimization of the
Interfacial
Energy
192
8.3.4
Alignment by Additive Coding of Nanoparticles
194
8.3.5
Alignment by a Mechanical Stress Field
196
8.4
The Role of Magnetic Fields
198
8.5
The Role of
Dipole
and Polarization Forces
204
8.5.1
Polarization Forces
204
8.6
The Role of External Electric Fields
219
8.7
Self-Similar Assembly and Shape Constraints
222
8.8
Shaping of Mesocrystals
226
8.9
Mesocrystals as Intermediates in Single Crystal Formation
228
References
233
9
Analysis of Mesocrystals
237
9.1
Nucleation and Growth of Primary Nanoparticles
238
9.2
Rapid Aggregation and Formation of Randomly
Oriented Aggregates
239
9.3
Mesocrystal Formation
239
9.4
Fusion of the Mesocrystal to a Single Crystal/Ripening and
Ion-Mediated Recrystallization Towards an Outer Single
Crystalline Shell
240
9.5
Analytical Techniques for Mesocrystals
241
References
244
10
Tuning of Properties
247
References
249
11
A Unifying Crystallization Mechanism
251
References
255
12
Analogy between Oriented Attachment or Hierarchically Structured
Crystals and Polymers
257
12.1
Analogy between Oriented Attachment and Polymerization
259
12.2
Structural Levels in Hierarchically Structured Crystals and
Biopolymers 263
References
264
13
Summary and Outlook
265
13.1
Summary
265
13.2
Outlook
267
References
270
Index
271 |
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| id | DE-604.BV035072867 |
| illustrated | Illustrated |
| index_date | 2024-07-02T22:04:43Z |
| indexdate | 2024-07-09T21:21:34Z |
| institution | BVB |
| isbn | 9780470029817 0470029811 |
| language | English |
| lccn | 2008004950 |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016741232 |
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| open_access_boolean | |
| owner | DE-703 DE-29T DE-19 DE-BY-UBM DE-11 |
| owner_facet | DE-703 DE-29T DE-19 DE-BY-UBM DE-11 |
| physical | XI, 276 S. Ill., graph. Darst. |
| publishDate | 2008 |
| publishDateSearch | 2008 |
| publishDateSort | 2008 |
| publisher | Wiley |
| record_format | marc |
| spelling | Cölfen, Helmut 1965-2023 Verfasser (DE-588)123271894 aut Mesocrystals and nonclassical crystallization Helmut Cölfen ; Markus Antonietti Chichester Wiley 2008 XI, 276 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Colloidal crystals Crystal growth Nanostructured materials Kristallisation (DE-588)4033215-9 gnd rswk-swf Nanostrukturiertes Material (DE-588)4342626-8 gnd rswk-swf Kristallisation (DE-588)4033215-9 s Nanostrukturiertes Material (DE-588)4342626-8 s DE-604 Antonietti, Markus 1960- Verfasser (DE-588)142882585 aut http://www.loc.gov/catdir/enhancements/fy0810/2008004950-d.html Publisher description http://www.loc.gov/catdir/enhancements/fy0810/2008004950-t.html Table of contents only Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016741232&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Cölfen, Helmut 1965-2023 Antonietti, Markus 1960- Mesocrystals and nonclassical crystallization Colloidal crystals Crystal growth Nanostructured materials Kristallisation (DE-588)4033215-9 gnd Nanostrukturiertes Material (DE-588)4342626-8 gnd |
| subject_GND | (DE-588)4033215-9 (DE-588)4342626-8 |
| title | Mesocrystals and nonclassical crystallization |
| title_auth | Mesocrystals and nonclassical crystallization |
| title_exact_search | Mesocrystals and nonclassical crystallization |
| title_exact_search_txtP | Mesocrystals and nonclassical crystallization |
| title_full | Mesocrystals and nonclassical crystallization Helmut Cölfen ; Markus Antonietti |
| title_fullStr | Mesocrystals and nonclassical crystallization Helmut Cölfen ; Markus Antonietti |
| title_full_unstemmed | Mesocrystals and nonclassical crystallization Helmut Cölfen ; Markus Antonietti |
| title_short | Mesocrystals and nonclassical crystallization |
| title_sort | mesocrystals and nonclassical crystallization |
| topic | Colloidal crystals Crystal growth Nanostructured materials Kristallisation (DE-588)4033215-9 gnd Nanostrukturiertes Material (DE-588)4342626-8 gnd |
| topic_facet | Colloidal crystals Crystal growth Nanostructured materials Kristallisation Nanostrukturiertes Material |
| url | http://www.loc.gov/catdir/enhancements/fy0810/2008004950-d.html http://www.loc.gov/catdir/enhancements/fy0810/2008004950-t.html http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016741232&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT colfenhelmut mesocrystalsandnonclassicalcrystallization AT antoniettimarkus mesocrystalsandnonclassicalcrystallization |