Applications of neutron powder diffraction:
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Oxford [u.a.]
Oxford University Press
2008
|
| Edition: | 1. publ. |
| Series: | Oxford series on neutron scattering in condensed matter
15 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Includes bibliographical references and index |
| Physical Description: | XVII, 486 S. zahlr. Ill. und graph. Darst. |
| ISBN: | 9780198515944 |
Staff View
MARC
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| 100 | 1 | |a Kisi, Erich |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Applications of neutron powder diffraction |c Erich H. Kisi, Christopher J. Howard |
| 250 | |a 1. publ. | ||
| 264 | 1 | |a Oxford [u.a.] |b Oxford University Press |c 2008 | |
| 300 | |a XVII, 486 S. |b zahlr. Ill. und graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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| 490 | 1 | |a Oxford series on neutron scattering in condensed matter |v 15 | |
| 500 | |a Includes bibliographical references and index | ||
| 650 | 4 | |a Neutrons |x Diffraction | |
| 650 | 4 | |a Powders |x Optical properties | |
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Record in the Search Index
| _version_ | 1804137937517936640 |
|---|---|
| adam_text | Contents
Preface
ix
Acknowledgements
xi
Image Acknowledgements
xii
Glossary of symbols
xiii
1
Introduction to neutron powder diffraction
1
1.1
What is neutron powder diffraction?
1
1.2
The role of neutron powder diffraction
2
1.3
Milestones in the development of neutron powder diffraction
3
2
Theory
-
the bare essentials
18
2.1
Neutrons for diffraction
18
2.2
Samples for diffraction
-
the structure of condensed matter
20
2.3
Neutron scattering by the sample
39
2.4
The powder diffraction pattern
49
3
Basic instrumentation and experimental techniques
65
3.1
Where to find neutron powder diffraction facilities
65
3.2
Constant wavelength neutron diffractometers
70
3.3
TOF
neutron diffractometers
77
3.4
Comparison of CW and
TOF
diffractometers
80
3.5
Experiment design
80
3.6
Sample preparation
100
4
Elements of data analysis
106
4.1
Preliminaries
106
4.2
Visual inspection
109
4.3
Phase identification
113
4.4
Unit cell parameters
118
vi
Contents
4.5
Peak shapes and widths
124
4.6
Whole pattern fitting
131
5
Crystal structures
134
5.1
Neutron powder diffraction and crystal structures
134
5.2
More crystallography
-
description of crystal structures
135
5.3
Reflection conditions and space group determination
146
5.4
Solving structures
150
5.5
Structure refinement
-
the
Rietveld
method
155
5.6
Le
Bail extraction
177
5.7
Practical considerations in structure refinement
178
5.8
Structure solution and refinement
-
examples
182
6
Ab
initia
structure solution
192
6.1
Introduction
192
6.2
Unit cell determination (powder pattern indexing)
193
6.3
Intensity extraction
205
6.4
Structure solution
212
6.5
Advanced refinement techniques
232
6.6
Looking ahead
249
7
Magnetic structures
251
7.1
Introduction
251
7.2
Crystallography and symmetry of magnetic structures
252
7.3
Magnetic scattering and diffraction
260
7.4
Solving magnetic structures
267
7.5
Recent examples
273
8
Quantitative phase analysis
284
8.1
Introduction
284
8.2
Theory
285
8.3
Individual peak methods
287
8.4
Whole pattern analysis
292
8.5
Evaluation of the techniques
293
8.6
Practical examples
294
9
Microstructural data
from powder patterns
308
9.1
Introduction
308
9.2
Particle size
309
9.3 Microstrains 330
9.4
Combined size and strain broadening
340
Contents
vii
9.5 Chemical
and physical gradients
346
9.6
Line defects
-
dislocation broadening
358
9.7
Plane defects and stacking disorder
368
9.8
Texture
374
10
Diffuse scattering
-
thermal, short-range order, gaseous,
liquid, and amorphous scattering
381
10.1
Introduction
381
10.2
Thermal diffuse scattering
382
10.3
Short-range order scattering
385
10.4
Scattering from gases, liquids, and amorphous solids
395
11
Stress and elastic constants
403
11.1
Stresses, strains, and elastic constants in
nature and industry
403
11.2
Influence of elastic strains on the powder diffraction pattern
414
11.3
Neutron diffraction residual stress analysis
420
11.4
Determination of single crystal elastic constants from
polycrystalline samples
438
12
New directions
443
12.1
Introduction
443
12.2
Neutron sources
443
12.3
Components
444
12.4
Diffractometers
446
12.5
Data analysis
449
12.6
New problems for study by neutron powder diffraction
453
12.7
Closing remarks
458
Appendix
1
459
Appendix
2
462
References
463
Index
481
|
| adam_txt |
Contents
Preface
ix
Acknowledgements
xi
Image Acknowledgements
xii
Glossary of symbols
xiii
1
Introduction to neutron powder diffraction
1
1.1
What is neutron powder diffraction?
1
1.2
The role of neutron powder diffraction
2
1.3
Milestones in the development of neutron powder diffraction
3
2
Theory
-
the bare essentials
18
2.1
Neutrons for diffraction
18
2.2
Samples for diffraction
-
the structure of condensed matter
20
2.3
Neutron scattering by the sample
39
2.4
The powder diffraction pattern
49
3
Basic instrumentation and experimental techniques
65
3.1
Where to find neutron powder diffraction facilities
65
3.2
Constant wavelength neutron diffractometers
70
3.3
TOF
neutron diffractometers
77
3.4
Comparison of CW and
TOF
diffractometers
80
3.5
Experiment design
80
3.6
Sample preparation
100
4
Elements of data analysis
106
4.1
Preliminaries
106
4.2
Visual inspection
109
4.3
Phase identification
113
4.4
Unit cell parameters
118
vi
Contents
4.5
Peak shapes and widths
124
4.6
Whole pattern fitting
131
5
Crystal structures
134
5.1
Neutron powder diffraction and crystal structures
134
5.2
More crystallography
-
description of crystal structures
135
5.3
Reflection conditions and space group determination
146
5.4
Solving structures
150
5.5
Structure refinement
-
the
Rietveld
method
155
5.6
Le
Bail extraction
177
5.7
Practical considerations in structure refinement
178
5.8
Structure solution and refinement
-
examples
182
6
Ab
initia
structure solution
192
6.1
Introduction
192
6.2
Unit cell determination (powder pattern indexing)
193
6.3
Intensity extraction
205
6.4
Structure solution
212
6.5
Advanced refinement techniques
232
6.6
Looking ahead
249
7
Magnetic structures
251
7.1
Introduction
251
7.2
Crystallography and symmetry of magnetic structures
252
7.3
Magnetic scattering and diffraction
260
7.4
Solving magnetic structures
267
7.5
Recent examples
273
8
Quantitative phase analysis
284
8.1
Introduction
284
8.2
Theory
285
8.3
Individual peak methods
287
8.4
Whole pattern analysis
292
8.5
Evaluation of the techniques
293
8.6
Practical examples
294
9
Microstructural data
from powder patterns
308
9.1
Introduction
308
9.2
Particle size
309
9.3 Microstrains 330
9.4
Combined size and strain broadening
340
Contents
vii
9.5 Chemical
and physical gradients
346
9.6
Line defects
-
dislocation broadening
358
9.7
Plane defects and stacking disorder
368
9.8
Texture
374
10
Diffuse scattering
-
thermal, short-range order, gaseous,
liquid, and amorphous scattering
381
10.1
Introduction
381
10.2
Thermal diffuse scattering
382
10.3
Short-range order scattering
385
10.4
Scattering from gases, liquids, and amorphous solids
395
11
Stress and elastic constants
403
11.1
Stresses, strains, and elastic constants in
nature and industry
403
11.2
Influence of elastic strains on the powder diffraction pattern
414
11.3
Neutron diffraction residual stress analysis
420
11.4
Determination of single crystal elastic constants from
polycrystalline samples
438
12
New directions
443
12.1
Introduction
443
12.2
Neutron sources
443
12.3
Components
444
12.4
Diffractometers
446
12.5
Data analysis
449
12.6
New problems for study by neutron powder diffraction
453
12.7
Closing remarks
458
Appendix
1
459
Appendix
2
462
References
463
Index
481 |
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| id | DE-604.BV035014871 |
| illustrated | Illustrated |
| index_date | 2024-07-02T21:45:05Z |
| indexdate | 2024-07-09T21:20:14Z |
| institution | BVB |
| isbn | 9780198515944 |
| language | English |
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| series | Oxford series on neutron scattering in condensed matter |
| series2 | Oxford series on neutron scattering in condensed matter |
| spelling | Kisi, Erich Verfasser aut Applications of neutron powder diffraction Erich H. Kisi, Christopher J. Howard 1. publ. Oxford [u.a.] Oxford University Press 2008 XVII, 486 S. zahlr. Ill. und graph. Darst. txt rdacontent n rdamedia nc rdacarrier Oxford series on neutron scattering in condensed matter 15 Includes bibliographical references and index Neutrons Diffraction Powders Optical properties Neutronenbeugung (DE-588)4171630-9 gnd rswk-swf Pulvermethode (DE-588)4176353-1 gnd rswk-swf Neutronenbeugung (DE-588)4171630-9 s Pulvermethode (DE-588)4176353-1 s DE-604 Howard, Christopher J. Verfasser (DE-588)136955193 aut Oxford series on neutron scattering in condensed matter 15 (DE-604)BV000831267 15 Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016684057&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kisi, Erich Howard, Christopher J. Applications of neutron powder diffraction Oxford series on neutron scattering in condensed matter Neutrons Diffraction Powders Optical properties Neutronenbeugung (DE-588)4171630-9 gnd Pulvermethode (DE-588)4176353-1 gnd |
| subject_GND | (DE-588)4171630-9 (DE-588)4176353-1 |
| title | Applications of neutron powder diffraction |
| title_auth | Applications of neutron powder diffraction |
| title_exact_search | Applications of neutron powder diffraction |
| title_exact_search_txtP | Applications of neutron powder diffraction |
| title_full | Applications of neutron powder diffraction Erich H. Kisi, Christopher J. Howard |
| title_fullStr | Applications of neutron powder diffraction Erich H. Kisi, Christopher J. Howard |
| title_full_unstemmed | Applications of neutron powder diffraction Erich H. Kisi, Christopher J. Howard |
| title_short | Applications of neutron powder diffraction |
| title_sort | applications of neutron powder diffraction |
| topic | Neutrons Diffraction Powders Optical properties Neutronenbeugung (DE-588)4171630-9 gnd Pulvermethode (DE-588)4176353-1 gnd |
| topic_facet | Neutrons Diffraction Powders Optical properties Neutronenbeugung Pulvermethode |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016684057&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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