Experimental neutron scattering:
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Oxford
Oxford University Press
2009
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Hier auch später erschienene, unveränderte Nachdrucke |
| Physical Description: | xii, 325 Seiten Illustrationen, Diagramme |
| ISBN: | 9780198519706 9780199673773 |
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MARC
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| 084 | |a PHY 480f |2 stub | ||
| 100 | 1 | |a Willis, B. T. M. |e Verfasser |0 (DE-588)142644234 |4 aut | |
| 245 | 1 | 0 | |a Experimental neutron scattering |c B. T. M. Willis (University of Oxford, U.K.) ; C. J. Carlile (Lund University, Sweden) |
| 264 | 1 | |a Oxford |b Oxford University Press |c 2009 | |
| 300 | |a xii, 325 Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Hier auch später erschienene, unveränderte Nachdrucke | ||
| 650 | 4 | |a Neutrons / Scattering | |
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| 689 | 1 | 0 | |a Neutronenstreuung |0 (DE-588)4041980-0 |D s |
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| 700 | 1 | |a Carlile, Colin J. |d 1946- |e Verfasser |0 (DE-588)172780659 |4 aut | |
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Record in the Search Index
| _version_ | 1818043366990938112 |
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| adam_text |
Contents
Preface
I Generell
considerations
1
1
Over
70
years of neutron scattering
3
1.1
The discovery of the neutron
3
1.2
Early history of neutron scattering
5
1.3
Future prospects
11
References
12
2
Neutron properties
15
2.1
Wave-particle duality
15
2.1.1
Interconversion
of units
16
2.2
Properties of thermal neutrons
18
2.2.1
Lifetime
18
2.2.2
Mass
19
2.2.3
Wavelength
19
2.2.4
Energy
21
2.2.5
Magnetic properties
21
2.2.6
Polarization properties
22
2.3
Definition of cross-sections
22
2.3.1
Total cross-section
23
2.3.2
Differential cross-section
25
2.3.3
Double differential cross-section
25
2.4
Coherent and incoherent nuclear scattering
26
2.5
Inelastic scattering: Van Hove formalism
30
2.6
Kinematics of inelastic scattering
32
2.7
Magnetic scattering
33
References
34
3
The production of neutrons
35
3.1
Introduction
35
3.2
Radioactive sources
35
3.3
Neutrons from nuclear reactors
36
3.3.1
The ILL reactor
40
3.3.2
Pulsed reactors
41
viii Contents
3.4 Neutrons
from pulsed accelerators
3.4.1
Photofission
sources using electron
accelerators
3.4.2
Spallation sources using proton
accelerators
3.5
Neutron moderation: hot and cold sources
3.6
The relative merits of continuous and
pulsed sources
52
References
57
4
Neutron detection
59
4.1
Introduction
59
4.2
Beam monitors
60
4.3
Gas detectors
60
4.3.1
Banks of individual detectors
64
4.3.2
Resistive-wire gas proportional counters
64
4.3.3
Multi-wire proportional counter
(MWPC)
64
4.3.4
Micropattern gas counters (MPGC)
65
4.4
Scintillation detectors
65
4.4.1
Discrete element scintillators
67
4.4.2
The Anger camera
67
4.5
Plate detectors
68
4.5.1
Photographic plates
68
4.5.2
Image plates
69
References
69
5
Instrument components
71
5.1
Neutron guide tubes
71
5.1.1
Supermirrors
75
5.1.2
Guides on reactors and pulsed sources
77
5.2
Collimators
78
5.2.1 Soller
slit collimators
78
5.2.2
Radial collimators
80
5.3
Beam filters and resonance foils
81
5.4
Selection and measurement of neutron energies
84
5.4.1
Choppers
85
5.4.2
Crystal monochromators
89
References
94
6
Sample preparation, sample environment
and radiological safety
95
6.1
General considerations
95
6.2
Containment of sample and ideal sample sizes
96
6.3
Cryostats
99
6.4
Pressure cells
101
6.4.1
Materials
102
6.4.2
Windows
102
Contents ix
6.4.3 Environment
and safety
103
6.4.4
Pressure cells used for neutron scattering
103
6.5
Radiological safety
104
6.5.1
Definitions
104
6.5.2
Limitation of effective dose
105
6.5.3
Activation of samples by neutron irradiation
105
6.5.4
Shielding from neutron radiation
106
References
107
II Neutron diffraction
109
7
Single crystal diffraction 111
7.1
General 111
7.1.1
The unit cell and the crystal lattice 111
7.1.2
The reciprocal lattice
112
7.1.3
The
Ewald
sphere
113
7.1.4
Nuclear Bragg scattering
114
7.2
Diffraction at constant wavelength
115
7.2.1
The four-circle diffractometer
115
7.2.2
Area detector instruments
118
7.3
Time-of-flight diffraction
119
7.4
Reduction of intensities to structure amplitudes
121
7.4.1
Correction for absorption
122
7.4.2
Correction for extinction
123
7.4.3
Avoidance of multiple diffraction
124
7.5
Some examples of studies by single crystal
neutron diffraction
125
References
127
8
The powder diffraction method
131
8.1
Principles of the powder diffraction method
132
8.1.1
Angle-dispersive procedure
132
8.1.2
Energy-dispersive procedure
134
8.2
Resolution of powder diffraction peaks
137
8.2.1
Effect of size of mosaic block
137
8.2.2
The focusing effect: fixed-wavelength
instruments
139
8.2.3
Time-of-flight instruments
141
8.3
Structure refinement from powder data
143
8.4
Neutron strain scanning
147
8.5
Some chemical applications of powder diffraction
150
8.6
Future prospects
151
References
152
9
Polarized neutrons and magnetic
neutron diffraction
155
9.1
Introduction
155
χ
Contents
9.2
Some fundamental concepts of magnetic scattering
155
9.3
Production of a polarized neutron beam
158
9.3.1
Polarizing single crystals
158
9.3.2
Polarizing mirrors
159
9.3.3
Polarizing filters
161
9.4
Neutron spin nippers and devices for
guiding the polarization
162
9.5
Experimental methods
165
9.5.1
Unpolarized neutrons
165
9.5.2
Polarized neutron scattering: measurement
of flipping ratios
167
9.5.3
Uniaxial
polarization analysis
170
9.5.4
Spherical neutron polarimetry
171
References
172
10
Small-angle neutron scattering
177
10.1
Theory of small-angle scattermg
178
10.1.1
The scattering contrast term
178
10.1.2
The form factor term P(Q)
180
10.1.3
The structure factor term S(Q)
182
10.2
The scattering 'laws'
182
10.2.1
The domain of very small
Q
182
10.2.2
The domain of large
Q
184
10.3
Experimental considerations
186
10.3.1
Design of SANS instruments
186
10.3.2
Sample size
188
10.3.3
Data analysis
189
10.4
Some applications of SANS
189
References
192
11
Neutron optics
195
11.1
Mirror reflection of neutrons
195
11.1.1
Gravity refractometer
198
11.2
Ultracold neutrons
200
11.3
Dynamical neutron diffraction
203
11.3.1
Basic equations of dynamical
diffraction theory
204
11.3.2
Neutron
interferometry
207
11.3.3
Pendellösung
effects
210
References
213
12
Neutron reflectometry
217
12.1
Theory of neutron reflectivity
218
12.1.1
Non-specular scattering
221
12.2
Spin-polarized neutron reflectometry
221
12.3
Experimental methods
223
12.4
Examples of reflectivity studies
224
12.4.1
Surfactant monolayers
225
Contents xi
12.4.2
Magnetic
films
225
12.4.3
Lipid bilayers
227
References
228
13
Liquids, glasses and amorphous materials
231
13.1
Diffraction theory
231
13.1.1
Van Hove correlation functions
235
13.2
Analysis of diffraction data
238
13.3
Diffractometers for liquid and amorphous samples
240
13.4
Atomic structure of liquids
241
13.4.1
Simple liquids
241
13.4.2
Binary liquids
244
13.4.3
Glasses
245
References
246
III Neutron spectroscopy
249
14
Coherent inelastic scattering from single crystals:
study of phonons and
magnons
251
14.1
The elements of lattice dynamics
251
14.2
One-phonon coherent scattering of neutrons
255
14.2.1
The one-phonon scattering surface
257
14.3
Instruments for inelastic scattering experiments
259
14.3.1
The triple-axis spectrometer
259
14.3.2
Time-of-flight spectrometers
263
14.4
Some examples of coherent inelastic scattering
studies of single crystals
266
14.4.1
Phonon dispersion curves
266
14.4.2
Phase transitions
267
14.4.3
Superconductivity
269
14.4.4
Magnon
dispersion curves
271
14.5
Comparison of
TAS
and
TOF
methods of
measuring phonon dispersion relations
273
References
275
15
Inelastic neutron scattering spectroscopy
279
15.1
Introduction
279
15.2
Inelastic molecular neutron spectroscopy
283
15.2.1
Simplified theory
285
15.3
Instrumentation for neutron spectroscopy
288
15.3.1
Direct-geometry spectroscopy
289
15.3.2
Indirect-geometry spectroscopy
290
15.4
Spectroscopie
studies using inelastic
neutron scattering
290
References
293
xii Contents
16
Quasi-elastic scattering and high-resolution
spectroscopy
295
16.1
Introduction
295
16.2
Energy resolution and time scales
296
16.3
Types of spectrometer
298
16.3.1
Direct geometry time-of-flight spectrometer
298
16.3.2
Inverted-geometry spectrometers
300
16.3.3
Neutron spin-echo spectrometer
303
16.4
Examples of studies by high-resolution spectroscopy
304
16.4.1
Diffusion
304
16.4.2
Tunnelling spectroscopy
306
16.4.3
Fast dynamical studies
307
References
308
Appendix A
311
A.I Glossary of special terms
311
Appendix
В
319
B.I Neutron scattering lengths and cross-sections
of the elements
319
References
321
Index
323 |
| adam_txt |
Contents
Preface
I Generell
considerations
1
1
Over
70
years of neutron scattering
3
1.1
The discovery of the neutron
3
1.2
Early history of neutron scattering
5
1.3
Future prospects
11
References
12
2
Neutron properties
15
2.1
Wave-particle duality
15
2.1.1
Interconversion
of units
16
2.2
Properties of thermal neutrons
18
2.2.1
Lifetime
18
2.2.2
Mass
19
2.2.3
Wavelength
19
2.2.4
Energy
21
2.2.5
Magnetic properties
21
2.2.6
Polarization properties
22
2.3
Definition of cross-sections
22
2.3.1
Total cross-section
23
2.3.2
Differential cross-section
25
2.3.3
Double differential cross-section
25
2.4
Coherent and incoherent nuclear scattering
26
2.5
Inelastic scattering: Van Hove formalism
30
2.6
Kinematics of inelastic scattering
32
2.7
Magnetic scattering
33
References
34
3
The production of neutrons
35
3.1
Introduction
35
3.2
Radioactive sources
35
3.3
Neutrons from nuclear reactors
36
3.3.1
The ILL reactor
40
3.3.2
Pulsed reactors
41
viii Contents
3.4 Neutrons
from pulsed accelerators
3.4.1
Photofission
sources using electron
accelerators
3.4.2
Spallation sources using proton
accelerators
3.5
Neutron moderation: hot and cold sources
3.6
The relative merits of continuous and
pulsed sources
52
References
57
4
Neutron detection
59
4.1
Introduction
59
4.2
Beam monitors
60
4.3
Gas detectors
60
4.3.1
Banks of individual detectors
64
4.3.2
Resistive-wire gas proportional counters
64
4.3.3
Multi-wire proportional counter
(MWPC)
64
4.3.4
Micropattern gas counters (MPGC)
65
4.4
Scintillation detectors
65
4.4.1
Discrete element scintillators
67
4.4.2
The Anger camera
67
4.5
Plate detectors
68
4.5.1
Photographic plates
68
4.5.2
Image plates
69
References
69
5
Instrument components
71
5.1
Neutron guide tubes
71
5.1.1
Supermirrors
75
5.1.2
Guides on reactors and pulsed sources
77
5.2
Collimators
78
5.2.1 Soller
slit collimators
78
5.2.2
Radial collimators
80
5.3
Beam filters and resonance foils
81
5.4
Selection and measurement of neutron energies
84
5.4.1
Choppers
85
5.4.2
Crystal monochromators
89
References
94
6
Sample preparation, sample environment
and radiological safety
95
6.1
General considerations
95
6.2
Containment of sample and ideal sample sizes
96
6.3
Cryostats
99
6.4
Pressure cells
101
6.4.1
Materials
102
6.4.2
Windows
102
Contents ix
6.4.3 Environment
and safety
103
6.4.4
Pressure cells used for neutron scattering
103
6.5
Radiological safety
104
6.5.1
Definitions
104
6.5.2
Limitation of effective dose
105
6.5.3
Activation of samples by neutron irradiation
105
6.5.4
Shielding from neutron radiation
106
References
107
II Neutron diffraction
109
7
Single crystal diffraction 111
7.1
General 111
7.1.1
The unit cell and the crystal lattice 111
7.1.2
The reciprocal lattice
112
7.1.3
The
Ewald
sphere
113
7.1.4
Nuclear Bragg scattering
114
7.2
Diffraction at constant wavelength
115
7.2.1
The four-circle diffractometer
115
7.2.2
Area detector instruments
118
7.3
Time-of-flight diffraction
119
7.4
Reduction of intensities to structure amplitudes
121
7.4.1
Correction for absorption
122
7.4.2
Correction for extinction
123
7.4.3
Avoidance of multiple diffraction
124
7.5
Some examples of studies by single crystal
neutron diffraction
125
References
127
8
The powder diffraction method
131
8.1
Principles of the powder diffraction method
132
8.1.1
Angle-dispersive procedure
132
8.1.2
Energy-dispersive procedure
134
8.2
Resolution of powder diffraction peaks
137
8.2.1
Effect of size of mosaic block
137
8.2.2
The focusing effect: fixed-wavelength
instruments
139
8.2.3
Time-of-flight instruments
141
8.3
Structure refinement from powder data
143
8.4
Neutron strain scanning
147
8.5
Some chemical applications of powder diffraction
150
8.6
Future prospects
151
References
152
9
Polarized neutrons and magnetic
neutron diffraction
155
9.1
Introduction
155
χ
Contents
9.2
Some fundamental concepts of magnetic scattering
155
9.3
Production of a polarized neutron beam
158
9.3.1
Polarizing single crystals
158
9.3.2
Polarizing mirrors
159
9.3.3
Polarizing filters
161
9.4
Neutron spin nippers and devices for
guiding the polarization
162
9.5
Experimental methods
165
9.5.1
Unpolarized neutrons
165
9.5.2
Polarized neutron scattering: measurement
of flipping ratios
167
9.5.3
Uniaxial
polarization analysis
170
9.5.4
Spherical neutron polarimetry
171
References
172
10
Small-angle neutron scattering
177
10.1
Theory of small-angle scattermg
178
10.1.1
The scattering contrast term
178
10.1.2
The form factor term P(Q)
180
10.1.3
The structure factor term S(Q)
182
10.2
The scattering 'laws'
182
10.2.1
The domain of very small
Q
182
10.2.2
The domain of large
Q
184
10.3
Experimental considerations
186
10.3.1
Design of SANS instruments
186
10.3.2
Sample size
188
10.3.3
Data analysis
189
10.4
Some applications of SANS
189
References
192
11
Neutron optics
195
11.1
Mirror reflection of neutrons
195
11.1.1
Gravity refractometer
198
11.2
Ultracold neutrons
200
11.3
Dynamical neutron diffraction
203
11.3.1
Basic equations of dynamical
diffraction theory
204
11.3.2
Neutron
interferometry
207
11.3.3
Pendellösung
effects
210
References
213
12
Neutron reflectometry
217
12.1
Theory of neutron reflectivity
218
12.1.1
Non-specular scattering
221
12.2
Spin-polarized neutron reflectometry
221
12.3
Experimental methods
223
12.4
Examples of reflectivity studies
224
12.4.1
Surfactant monolayers
225
Contents xi
12.4.2
Magnetic
films
225
12.4.3
Lipid bilayers
227
References
228
13
Liquids, glasses and amorphous materials
231
13.1
Diffraction theory
231
13.1.1
Van Hove correlation functions
235
13.2
Analysis of diffraction data
238
13.3
Diffractometers for liquid and amorphous samples
240
13.4
Atomic structure of liquids
241
13.4.1
Simple liquids
241
13.4.2
Binary liquids
244
13.4.3
Glasses
245
References
246
III Neutron spectroscopy
249
14
Coherent inelastic scattering from single crystals:
study of phonons and
magnons
251
14.1
The elements of lattice dynamics
251
14.2
One-phonon coherent scattering of neutrons
255
14.2.1
The one-phonon scattering surface
257
14.3
Instruments for inelastic scattering experiments
259
14.3.1
The triple-axis spectrometer
259
14.3.2
Time-of-flight spectrometers
263
14.4
Some examples of coherent inelastic scattering
studies of single crystals
266
14.4.1
Phonon dispersion curves
266
14.4.2
Phase transitions
267
14.4.3
Superconductivity
269
14.4.4
Magnon
dispersion curves
271
14.5
Comparison of
TAS
and
TOF
methods of
measuring phonon dispersion relations
273
References
275
15
Inelastic neutron scattering spectroscopy
279
15.1
Introduction
279
15.2
Inelastic molecular neutron spectroscopy
283
15.2.1
Simplified theory
285
15.3
Instrumentation for neutron spectroscopy
288
15.3.1
Direct-geometry spectroscopy
289
15.3.2
Indirect-geometry spectroscopy
290
15.4
Spectroscopie
studies using inelastic
neutron scattering
290
References
293
xii Contents
16
Quasi-elastic scattering and high-resolution
spectroscopy
295
16.1
Introduction
295
16.2
Energy resolution and time scales
296
16.3
Types of spectrometer
298
16.3.1
Direct geometry time-of-flight spectrometer
298
16.3.2
Inverted-geometry spectrometers
300
16.3.3
Neutron spin-echo spectrometer
303
16.4
Examples of studies by high-resolution spectroscopy
304
16.4.1
Diffusion
304
16.4.2
Tunnelling spectroscopy
306
16.4.3
Fast dynamical studies
307
References
308
Appendix A
311
A.I Glossary of special terms
311
Appendix
В
319
B.I Neutron scattering lengths and cross-sections
of the elements
319
References
321
Index
323 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Willis, B. T. M. Carlile, Colin J. 1946- |
| author_GND | (DE-588)142644234 (DE-588)172780659 |
| author_facet | Willis, B. T. M. Carlile, Colin J. 1946- |
| author_role | aut aut |
| author_sort | Willis, B. T. M. |
| author_variant | b t m w btm btmw c j c cj cjc |
| building | Verbundindex |
| bvnumber | BV035014862 |
| callnumber-first | Q - Science |
| callnumber-label | QC793 |
| callnumber-raw | QC793.5.N4628 |
| callnumber-search | QC793.5.N4628 |
| callnumber-sort | QC 3793.5 N4628 |
| callnumber-subject | QC - Physics |
| classification_rvk | UP 2000 |
| classification_tum | PHY 607f PHY 480f |
| ctrlnum | (OCoLC)213301925 (DE-599)BSZ284345350 |
| dewey-full | 539.7213 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 539 - Modern physics |
| dewey-raw | 539.7213 |
| dewey-search | 539.7213 |
| dewey-sort | 3539.7213 |
| dewey-tens | 530 - Physics |
| discipline | Physik |
| discipline_str_mv | Physik |
| format | Book |
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| id | DE-604.BV035014862 |
| illustrated | Illustrated |
| index_date | 2024-07-02T21:45:05Z |
| indexdate | 2024-12-10T09:01:05Z |
| institution | BVB |
| isbn | 9780198519706 9780199673773 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016684047 |
| oclc_num | 213301925 |
| open_access_boolean | |
| owner | DE-703 DE-91G DE-BY-TUM DE-11 DE-19 DE-BY-UBM DE-20 DE-29T DE-83 DE-384 |
| owner_facet | DE-703 DE-91G DE-BY-TUM DE-11 DE-19 DE-BY-UBM DE-20 DE-29T DE-83 DE-384 |
| physical | xii, 325 Seiten Illustrationen, Diagramme |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | Oxford University Press |
| record_format | marc |
| spelling | Willis, B. T. M. Verfasser (DE-588)142644234 aut Experimental neutron scattering B. T. M. Willis (University of Oxford, U.K.) ; C. J. Carlile (Lund University, Sweden) Oxford Oxford University Press 2009 xii, 325 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Hier auch später erschienene, unveränderte Nachdrucke Neutrons / Scattering Neutronenbeugung (DE-588)4171630-9 gnd rswk-swf Neutronenstreuung (DE-588)4041980-0 gnd rswk-swf Neutronenbeugung (DE-588)4171630-9 s DE-604 Neutronenstreuung (DE-588)4041980-0 s Carlile, Colin J. 1946- Verfasser (DE-588)172780659 aut Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016684047&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Willis, B. T. M. Carlile, Colin J. 1946- Experimental neutron scattering Neutrons / Scattering Neutronenbeugung (DE-588)4171630-9 gnd Neutronenstreuung (DE-588)4041980-0 gnd |
| subject_GND | (DE-588)4171630-9 (DE-588)4041980-0 |
| title | Experimental neutron scattering |
| title_auth | Experimental neutron scattering |
| title_exact_search | Experimental neutron scattering |
| title_exact_search_txtP | Experimental neutron scattering |
| title_full | Experimental neutron scattering B. T. M. Willis (University of Oxford, U.K.) ; C. J. Carlile (Lund University, Sweden) |
| title_fullStr | Experimental neutron scattering B. T. M. Willis (University of Oxford, U.K.) ; C. J. Carlile (Lund University, Sweden) |
| title_full_unstemmed | Experimental neutron scattering B. T. M. Willis (University of Oxford, U.K.) ; C. J. Carlile (Lund University, Sweden) |
| title_short | Experimental neutron scattering |
| title_sort | experimental neutron scattering |
| topic | Neutrons / Scattering Neutronenbeugung (DE-588)4171630-9 gnd Neutronenstreuung (DE-588)4041980-0 gnd |
| topic_facet | Neutrons / Scattering Neutronenbeugung Neutronenstreuung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016684047&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT willisbtm experimentalneutronscattering AT carlilecolinj experimentalneutronscattering |