NMR studies of translational motion: [principles and applications]
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Cambridge [u.a.]
Cambridge Univ. Press
2009
|
| Edition: | 1. publ. |
| Series: | Cambridge molecular science
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXII, 393 S. Ill., graph. Darst. |
| ISBN: | 9780521806961 0521806968 |
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Record in the Search Index
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| adam_text | NMR STUDIES OF TRANSLATIONAL MOTION WILLIAM S. PRICE NANOSCALE
ORGANISATION AND DYNAMICS GROUP UNIVERSITY OF WESTERN SYDNEY, AUSTRALIA
IKI CAMBRIDGE UNIVERSITY PRESS CONTENTS PREFACE IX ACKNOWLEDGEMENTS XIV
ABBREVIATIONS XV DIFFUSION AND ITS MEASUREMENT L 1.1 INTRODUCTION 1 1.2
TYPES OF TRANSLATIONAL MOTION - PHYSICAL INTERPRETATION AND SIGNIFICANCE
1 1.3 MATHEMATICAL MODELLING OF SELF-DIFFUSION 6 1.4 PROPAGATION 14 1.5
SOLVING THE DIFFUSION EQUATION 20 1.6 MEAN SQUARE DISPLACEMENT,
TIME-DEPENDENT DIFFUSION COEFFICIENTS AND THE DIFFUSION ELLIPSOID 31 1.7
MEASUREMENT TIMESCALES AND RESTRICTED DIFFUSION 36 1.8 DIFFUSION IN
HETEROGENEOUS, POROUS AND POLYMER SYSTEMS 39 1.9 FLOW IN POROUS MEDIA 54
1.10 TECHNIQUES FOR MEASURING DIFFUSION 55 REFERENCES 57 THEORY OF NMR
DIFFUSION AND FLOW MEASUREMENTS 69 2.1 INTRODUCTION 69 2.2 NUCLEAR
SPINS, MAGNETIC GRADIENTS AND MOTION 70 2.3 CORRELATING THE PGSE SIGNAL
ATTENUATION WITH DIFFUSION 90 2.4 OSCILLATING GRADIENTS, HIGHER-ORDER
GRADIENT PULSE TRAINS AND PROBING DJFI)) 98 2.5 PGSE OF FREELY DIFFUSING
MULTICOMPONENT SYSTEMS 101 2.6 THE LONG-RANGE DIPOLAR FIELD AND MULTIPLE
ECHOES 111 REFERENCES 112 PGSE MEASUREMENTS IN SIMPLE POROUS SYSTEMS 120
3.1 INTRODUCTION 120 3.2 EXPERIMENTAL DETERMINATION OF P(R, A) 122 V VI
CONTENTS 3.3 EXPERIMENTAL DETERMINATION OF THE MOMENTS OF P(R, *) 3.4
THE SPECTRAL FUNCTION AND THE RETURN TO ORIGIN PROBABILITY 3.5 DIFFUSIVE
DIFFRACTION 3.6 AN EXAMPLE - DIFFUSION BETWEEN PLANES 3.7 DIFFUSION IN
REFLECTING SPHERES 3.8 SIZE DISTRIBUTIONS OF THE RESTRICTING GEOMETRY
3.9 FINITE GRADIENT PULSES AND THE VALIDITY OF THE SGP AND GPD
APPROXIMATIONS 3.10 OTHER METHODS FOR DETERMINING E(Q, A) REFERENCES 4
PGSE MEASUREMENTS IN COMPLEX AND EXCHANGING SYSTEMS 4.1 INTRODUCTION 4.2
SIMPLE BINDING AND EXCHANGE: THE KAERGER EQUATIONS 4.3 EXCHANGE BETWEEN
FREE AND RESTRICTED SITES 4.4 ANISOTROPIC AND LOW DIMENSIONAL DIFFUSION
4.5 GENERAL POROUS MEDIA 4.6 POLYMER DIFFUSION 4.7 FLOW AND VELOCITY
DISTRIBUTIONS 4.8 INTERNAL MAGNETIC FIELD GRADIENTS REFERENCES 5 PGSE
HARDWARE 5.1 INTRODUCTION 5.2 GRADIENT COILS AND FRINGE FIELDS 5.3
CURRENT AMPLIFIERS 5.4 CONNECTING TO THE SPECTROMETER 5.5
FIELD-FREQUENCY LOCKING 5.6 TEMPERATURE CONTROL AND CALIBRATION
REFERENCES 6 SETUP AND ANALYSIS OF PGSE EXPERIMENTS 6.1 INTRODUCTION 6.2
SELECTION OF PGSE PARAMETERS 6.3 SAMPLE PREPARATION 6.4 GRADIENT
CALIBRATION 6.5 ANALYSIS REFERENCES 7 PGSE HARDWARE AND SAMPLE PROBLEMS
7.1 INTRODUCTION 7.2 RF PROBLEMS 7.3 RADIATION DAMPING AND LONG-RANGE
DIPOLAR FIELD EFFECTS 7.4 CONVECTION AND FLOW COMPENSATION 7.5 GRADIENT
CONSTANCY CONTENTS VLL 7.6 BACKGROUND GRADIENTS 230 7.7 EDDY CURRENTS
AND PERTURBATION OF B 0 235 7.8 GRADIENT MISMATCH AND SAMPLE MOVEMENT
242 7.9 CROSS RELAXATION 246 7.10 HOMONUCLEAR SCALAR COUPLINGS 247
REFERENCES 248 8 SPECIALISED PGSE AND RELATED TECHNIQUES 256 8.1
INTRODUCTION 256 8.2 STEADY GRADIENT AND STRAY FIELD MEASUREMENTS 256
8.3 MULTIPLE QUANTUM AND HETERONUCLEAR 258 8.4 FAST SEQUENCES 262 8.5
DISTRIBUTIONS OF RELAXATION TIMES 269 8.6 MULTI-DIMENSIONAL MIXTURE
SEPARATION AND DIFFUSION EDITING 269 8.7 DOUBLE PGSE AND
MULTI-DIMENSIONAL CORRELATIONS 272 8.8 FLOW MEASUREMENTS 281 8.9
ELECTROPHORETIC NMR 282 8.10 MULTIPLE SPIN-ECHOES AND MISCELLANEOUS 286
REFERENCES 286 9 NMR IMAGING STUDIES OF TRANSLATIONAL MOTION 296 9.1
INTRODUCTION 296 9.2 IMAGING - BASIC CONCEPTS 297 9.3 COMBINING PGSE
MEASUREMENTS WITH IMAGING 297 9.4 IMAGING-BASED FLOW MEASUREMENTS 300
REFERENCES 303 10 B GRADIENT METHODS 308 10.1 INTRODUCTION 308 10.2 5J
GRADIENTS 308 10.3 *I GRADIENT DIFFUSION MEASUREMENTS 309 10.4
MISCELLANEOUS 310 REFERENCES 311 11 APPLICATIONS 313 11.1 INTRODUCTION
AND REVIEWS 313 11.2 APPLICATIONS TO HIGH-RESOLUTION NMR 314 11.3
BIOLOGICAL AND PHARMACEUTICAL STUDIES 316 11.4 CHEMICAL AND MATERIAL
STUDIES 326 11.5 SPIN-DIFFUSION 340 11.6 IMAGING-BASED STUDIES 340
REFERENCES 344 APPENDIX 369 INDEX *11
|
| any_adam_object | 1 |
| author | Price, William S. 1941- |
| author_GND | (DE-588)138975671 |
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| author_role | aut |
| author_sort | Price, William S. 1941- |
| author_variant | w s p ws wsp |
| building | Verbundindex |
| bvnumber | BV025603544 |
| classification_rvk | UM 3500 VE 5900 VG 9500 WC 2600 |
| ctrlnum | (OCoLC)600909471 (DE-599)BVBBV025603544 |
| dewey-full | 541.39 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541.39 |
| dewey-search | 541.39 |
| dewey-sort | 3541.39 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Biologie |
| edition | 1. publ. |
| format | Book |
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| indexdate | 2024-07-09T22:37:20Z |
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| isbn | 9780521806961 0521806968 |
| language | English |
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| spelling | Price, William S. 1941- Verfasser (DE-588)138975671 aut NMR studies of translational motion [principles and applications] William S. Price 1. publ. Cambridge [u.a.] Cambridge Univ. Press 2009 XXII, 393 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Cambridge molecular science Diffusionsmessung (DE-588)4199712-8 gnd rswk-swf Kernspintomografie (DE-588)4120806-7 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Translationsbewegung (DE-588)4268491-2 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 s Translationsbewegung (DE-588)4268491-2 s Diffusionsmessung (DE-588)4199712-8 s DE-604 Kernspintomografie (DE-588)4120806-7 s GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020198736&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Price, William S. 1941- NMR studies of translational motion [principles and applications] Diffusionsmessung (DE-588)4199712-8 gnd Kernspintomografie (DE-588)4120806-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Translationsbewegung (DE-588)4268491-2 gnd |
| subject_GND | (DE-588)4199712-8 (DE-588)4120806-7 (DE-588)4075421-2 (DE-588)4268491-2 |
| title | NMR studies of translational motion [principles and applications] |
| title_auth | NMR studies of translational motion [principles and applications] |
| title_exact_search | NMR studies of translational motion [principles and applications] |
| title_full | NMR studies of translational motion [principles and applications] William S. Price |
| title_fullStr | NMR studies of translational motion [principles and applications] William S. Price |
| title_full_unstemmed | NMR studies of translational motion [principles and applications] William S. Price |
| title_short | NMR studies of translational motion |
| title_sort | nmr studies of translational motion principles and applications |
| title_sub | [principles and applications] |
| topic | Diffusionsmessung (DE-588)4199712-8 gnd Kernspintomografie (DE-588)4120806-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Translationsbewegung (DE-588)4268491-2 gnd |
| topic_facet | Diffusionsmessung Kernspintomografie NMR-Spektroskopie Translationsbewegung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=020198736&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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