Handbook of laser induced breakdown spectroscopy:
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Chichester
Wiley
2006
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Includes bibliographical references and index. - Formerly CIP |
| Physical Description: | XVIII, 283 S. Ill., graph. Darst. |
| ISBN: | 0470092998 9780470092996 |
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MARC
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| 020 | |a 0470092998 |9 0-470-09299-8 | ||
| 020 | |a 9780470092996 |9 978-0-470-09299-6 | ||
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| 035 | |a (DE-599)BVBBV024613328 | ||
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| 100 | 1 | |a Cremers, David A. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Handbook of laser induced breakdown spectroscopy |c David A. Cremers and Leon J. Radziemski |
| 246 | 1 | 3 | |a Handbook of laser-induced breakdown spectroscopy |
| 264 | 1 | |a Chichester |b Wiley |c 2006 | |
| 300 | |a XVIII, 283 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Includes bibliographical references and index. - Formerly CIP | ||
| 650 | 0 | 7 | |a Laserinduzierte Breakdown-Spektroskopie |0 (DE-588)4745837-9 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Laserinduzierte Breakdown-Spektroskopie |0 (DE-588)4745837-9 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Radziemski, Leon J. |e Verfasser |4 aut | |
| 856 | 4 | 2 | |m Digitalisierung UB Bayreuth |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018585867&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-018585867 | ||
Record in the Search Index
| _version_ | 1804140631010836480 |
|---|---|
| adam_text | Contents
Foreword
xi
Preface
xiii
Acronyms, Constants and Symbols
xvii
1
History
1
1.1
Atomic Optical Emission Spectrochemistry
(OES)
1
1.1.1
Conventional
OES
1
1.1.2
Laser
OES
1
1.2
Laser-Induced Breakdown Spectroscopy (LIBS)
2
1.3
LIBS History
1960-1980 6
1.4
LIBS History
1980-1990 9
1.5
LIBS History
1990-2000 11
1.6
Active Areas of Investigation,
2000-2002 15
References
16
2
Basics of the LIBS Plasma
23
2.1
LIBS Plasma Fundamentals
23
2.1.1
Spectral Lines and Line Profiles
25
2.1.2
Determining Electron Densities from Spectral
Line Widths
27
2.1.3
Plasma Opacity
30
2.1.4
Temperature and Thermodynamic Equilibrium
31
2.2
Laser-Induced Breakdown
36
2.2.1
Breakdown in Gases
36
2.2.2
Post-Breakdown Phenomena in Gases
39
2.2.3
Breakdown In and On Solids, Aerosols
and Liquids
39
2.2.4
Post-Breakdown Phenomena on Solid Surfaces
41
2.3
Laser Ablation
43
2.4
Double or Multiple Pulse LIBS
47
2.5
Summary
49
References
50
3
Apparatus Fundamentals
53
3.1
Basic LIBS Apparatus
53
3.2
Lasers
54
viu
Contents
3.2.1
Laser
Fundamentals
54
3.2.2
Types of Lasers
55
3.2.3
Properties of Laser Light Important for LIBS
58
3.2.4
Generation of Additional Wavelengths
60
3.2.5
Double Pulse Operation
61
3.3
Optical Systems
62
3.3.1
Focusing and Light Collection
62
3.3.2
Lenses
63
3.3.3
Fiber Optic Cables
65
3.4
Methods of Spectral Resolution
69
3.4.1
Introduction
69
3.4.2
Spectral Resolution Devices
70
3.5
Detectors
83
3.6
Detection System Calibrations
88
3.6.1
Wavelength Calibration
88
3.6.2
Spectral Response Calibration
90
3.7
Timing Considerations
93
3.8
Methods of LIBS Deployment
94
References
96
4
Determining LIBS Analytical Figures-of-Merit
99
4.1
Introduction
99
4.2
Basics of LIBS Measurements
99
4.3
Precision
105
4.4
Calibration
107
4.4.1
Calibration Curves
107
4.4.2
Calibration Standards
113
4.5
Detection Limit
115
4.6
Accuracy
115
References
116
5
Qualitative LIBS Analysis
119
5.1
Introduction
119
5.2
Identifying Elements
119
5.3
Material Identification
122
5.4
Process Monitoring
125
5.4.1
Experimental
126
5.4.2
Results
127
5.4.3
Conclusions
133
5.5
Material Sorting/Distinguishing
133
5.5.1
Surface Condition
134
5.5.2
Type of Analysis
134
5.5.3
Sorting Materials of Close Composition
136
5.6
Site Screening Using LIBS
137
References
141
Contents ix
6 Quantitative
LIBS Analysis
143
6.1
Introduction
143
6.2
Effects of Sampling Geometry
143
6.3
Other Sampling Considerations
147
6.4
Particle Size and Incomplete Vaporization
151
6.5
Use of Internal Standardization
152
6.6
Chemical Matrix Effects
153
6.7
Example of LIBS Measurement: Impurities in Lithium
Solutions
155
6.7.1
Objective
155
6.7.2
Experimental
156
6.7.3
Results
158
6.7.4
Discussion of Results
163
6.8
Reported Figures-of-Merit for LIBS Measurements
164
6.9
Conclusions
168
References
168
7
Remote LIBS Measurements
171
7.1
Introduction
171
7.2
Conventional Open Path LIBS
173
7.2.1
Apparatus
173
7.2.2
Focusing the Laser Pulse
174
7.2.3
Collecting the Plasma Light
178
7.2.4
Results Using Conventional LIBS
179
7.3
Stand-off LIBS Using Femtosecond Pulses
182
7.3.1
Conventional Remote LIBS Using Femtosecond
Laser Pulses
182
7.3.2
Remote Analysis by Femtosecond Pulse Produced
Filamen
tation
184
7.3.3
Teramobile
185
7.3.4
Remote LIBS Using Femtosecond Pulses
186
7.4
Fiber Optic LIBS
187
7.4.1
Fiber Optics for Light Collection
187
7.4.2
Fibers for Laser Pulse Delivery
189
7.4.3
Applications of Fiber Optics
192
References
195
8
Examples of Recent LIBS Fundamental Research, Instruments and
Novel Applications
197
8.1
Introduction
197
8.2
Fundamentals
197
8.3
Calibration-Free LIBS (CF-LIBS)
201
8.4
Laser and Spectrometer Advances
203
8.5
Surface Analysis
205
x
Contents
8.6 Double Pulse
Studies and Applications
208
8.7
Steel Applications
210
8.8
LIBS for Biological Materials
211
8.9
Nuclear Reactor Applications
212
8.10
LIBS for Space Applications
214
References
223
9
The Future of LIBS
227
9.1
Introduction
227
9.2
Expanding the Understanding and Capability of the LIBS Process
227
9.3
Widening the Universe of LIBS Applications
229
9.4
Factors that will Speed the Commercialization of LIBS
230
9.4.1
LIBS Standardization and Quantification
230
9.4.2
Routine LIBS use in Industrial Applications
230
9.4.3
Availability of Components and Systems
231
9.5
Conclusion
232
References
233
Appendix A Safety Considerations in LIBS
237
A.I Safety Plans
237
A.2 Laser Safety
237
A.3 Generation of Aerosols
238
A.4 Laser Pulse Induced Ignition
239
References
239
Appendix
В
Recommended Methods for Commencing LIBS
Research on a Variety of Samples
241
References
243
Appendix
С
Representative LIBS Detection Limits
245
C.I Detection Limits from the Literature
245
C.2 Uniform Detection Limits
263
References
265
Appendix
D
Major LIBS References
271
Index
275
|
| any_adam_object | 1 |
| author | Cremers, David A. Radziemski, Leon J. |
| author_facet | Cremers, David A. Radziemski, Leon J. |
| author_role | aut aut |
| author_sort | Cremers, David A. |
| author_variant | d a c da dac l j r lj ljr |
| building | Verbundindex |
| bvnumber | BV024613328 |
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| dewey-full | 543.52 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543.52 |
| dewey-search | 543.52 |
| dewey-sort | 3543.52 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik |
| format | Book |
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| id | DE-604.BV024613328 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T22:03:02Z |
| institution | BVB |
| isbn | 0470092998 9780470092996 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-018585867 |
| oclc_num | 255431085 |
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| owner | DE-83 DE-703 |
| owner_facet | DE-83 DE-703 |
| physical | XVIII, 283 S. Ill., graph. Darst. |
| publishDate | 2006 |
| publishDateSearch | 2006 |
| publishDateSort | 2006 |
| publisher | Wiley |
| record_format | marc |
| spelling | Cremers, David A. Verfasser aut Handbook of laser induced breakdown spectroscopy David A. Cremers and Leon J. Radziemski Handbook of laser-induced breakdown spectroscopy Chichester Wiley 2006 XVIII, 283 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references and index. - Formerly CIP Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 gnd rswk-swf Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 s DE-604 Radziemski, Leon J. Verfasser aut Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018585867&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Cremers, David A. Radziemski, Leon J. Handbook of laser induced breakdown spectroscopy Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 gnd |
| subject_GND | (DE-588)4745837-9 |
| title | Handbook of laser induced breakdown spectroscopy |
| title_alt | Handbook of laser-induced breakdown spectroscopy |
| title_auth | Handbook of laser induced breakdown spectroscopy |
| title_exact_search | Handbook of laser induced breakdown spectroscopy |
| title_full | Handbook of laser induced breakdown spectroscopy David A. Cremers and Leon J. Radziemski |
| title_fullStr | Handbook of laser induced breakdown spectroscopy David A. Cremers and Leon J. Radziemski |
| title_full_unstemmed | Handbook of laser induced breakdown spectroscopy David A. Cremers and Leon J. Radziemski |
| title_short | Handbook of laser induced breakdown spectroscopy |
| title_sort | handbook of laser induced breakdown spectroscopy |
| topic | Laserinduzierte Breakdown-Spektroskopie (DE-588)4745837-9 gnd |
| topic_facet | Laserinduzierte Breakdown-Spektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018585867&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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