The elements of polymer science and engineering: an introductory text and reference for engineers and chemists
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
San Diego [u.a.]
Acad. Press
1999
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| Edition: | 2. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XVII, 509 S. graph. Darst. |
| ISBN: | 0126016852 |
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Record in the Search Index
| _version_ | 1804140418159345664 |
|---|---|
| adam_text | CONTENTS PREFACE CHAPTER 1 INTRODUCTORY CONCEPTS AND DEFINITIONS 1.1
SOME DEFINITIONS 1.1.1 POLYMER 1.1.2 MONOMER 1.1.3 OLIGOMER 1.1.4
REPEATING UNIT 1.1.5 REPRESENTATIONS OF POLYMER STRUCTURES 1.1.6 END
GROUPS 1.2 DEGREE OF POLYMERIZATION 1.3 POLYMERIZATION AND FUNCTIONALITY
1.3.1 POLYMERIZATION 1.3.2 FUNCTIONALITY 1.3.3 LATENT FUNCTIONALITY 1.4
WHY ARE SYNTHETIC POLYMERS USEFUL? 1.5 COPOLYMERS 1.5.1 RANDOM COPOLYMER
1.5.2 ALTERNATING COPOLYMER 1.5.3 GRAFT COPOLYMER 1.5.4 BLOCK COPOLYMER
1.6 MOLECULAR ARCHITECTURE 1.7 THERMOPLASTICS AND THERMOSETS 1.8
ELASTOMERS, FIBERS, AND PLASTICS 1.9 MISCELLANEOUS TERMS 1.10 POLYMER
NOMENCLATURE 1 2 2 2 3 5 6 6 7 7 7 9 12 16 17 17 18 19 20 23 24 27 28
PROBLEMS REFERENCES 34 39 CHAPTER 2 BASIC PRINCIPLES OF POLYMER
MOLECULAR WEIGHTS 2.1 IMPORTANCE OF MOLECULAR WEIGHT CONTROL 41 2.2 PLAN
OF THIS CHAPTER 42 2.3 ARITHMETIC MEAN 43 2.3.1 NUMBER DISTRIBUTION, M N
44 2.3.2 WEIGHT DISTRIBUTION, M W 46 2.4 MOLECULAR WEIGHT AVERAGES AS
RATIOS OF MOMENTS 47 2.4.1 MOMENTS IN STATISTICS AND MECHANICS 47 2.4.2
DIMENSIONS 49 2.4.3 ARITHMETIC MEAN AS A RATIO OF MOMENTS 49 2.4.4
EXTENSION TO OTHER MOLECULAR WEIGHT AVERAGES 50 2.5 BREADTH OF THE
DISTRIBUTION 53 2.6 SUMMARIZING THE MOLECULAR WEIGHT/DISTRIBUTION 56 2.7
M Z M W M N 57 2.8 INTEGRAL AND SUMMATIVE EXPRESSIONS 57 2.9 DIRECT
MEASUREMENTS OF AVERAGE MOLECULAR WEIGHTS 58 2.10 COLLIGATIVE PROPERTIES
AND M N 60 2.10.1 IDEAL SOLUTIONS 60 2.10.2 OSMOTIC PRESSURE 62 2.10.3
OSMOTIC PRESSURE MEASURES, M N 65 2.11 VIRIAL EQUATIONS 65 2.12 VIRIAL
COEFFICIENTS 66 APPENDIX 2A: MOLECULAR WEIGHT AVERAGES OF BLENDS OF
BROAD DISTRIBUTION POLYMERS 67 PROBLEMS 69 REFERENCES 71 CHAPTER 3
PRACTICAL ASPECTS OF MOLECULAR WEIGHT MEASUREMENTS 3.1 M N METHODS 73
3.1.1 MEMBRANE OSMOMETRY 74 3.1.2 VAPOR PHASE OSMOMETRY 77 3.1.3
EBULLIOMETRY 79 3.1.4 CRYOSCOPY (FREEZING POINT DEPRESSION) 79 3.1.5
END-GROUP DETERMINATIONS 79 3.2 LIGHT SCATTERING 80 3.2.1 TERMINOLOGY 84
3.2.2 EFFECT OF POLYDISPERSITY 85 3.2.3 SCATTERING FROM LARGE PARTICLES
85 3.2.4 LIGHT SCATTERING INSTRUMENTATION 88 3.2.5 LIGHT SCATTERING FROM
COPOLYMERS 89 3.2.6 RADIUS OF GYRATION FROM LIGHT SCATTERING DATA 89 3.3
DILUTE SOLUTION VISCOMETRY 90 3.3.1 VISCOSITY AVERAGE MOLECULAR WEIGHT M
V 95 3.3.2 CALIBRATION OF THE MARK-HOUWINK-SAKURADA EQUATION 97 3.3.3
MEASUREMENT OF INTRINSIC VISCOSITY 99 3.3.4 SINGLE-POINT INTRINSIC
VISCOSITIES 101 3.3.5 SOLUTION VISCOSITY TERMINOLOGY 102 3.3.6 SOLUTION
VISCOSITIES IN POLYMER QUALITY CONTROL 103 3.3.7 COPOLYMERS AND BRANCHED
POLYMERS 103 3.4 SIZE EXCLUSION CHROMATOGRAPHY 103 3.4.1 EXPERIMENTAL
ARRANGEMENT 104 3.4.2 DATA INTERPRETATION 105 3.4.3 UNIVERSAL
CALIBRATION FOR LINEAR HOMOPOLYMERS 106 3.4.4 BRANCHED POLYMERS 111
3.4.5 AQUEOUS SEC 112 3.4.6 INHOMOGENEOUS POLYMERS 113 3.4.7 MALDI-MS
113 APPENDIX 3 A: MULTIGRADE MOTOR OILS 114 PROBLEMS 115 REFERENCES 119
CHAPTER 4 EFFECTS OF POLYMER ISOMERISM AND CONFORMATIONAL CHANGES 4.1
CONSTITUTIONAL ISOMERISM 121 4.1.1 POSITIONAL ISOMERISM 122 4.1.2
BRANCHING 124 4.2 CONFIGURATIONAL ISOMERISM 126 4.2.1 GEOMETRICAL
ISOMERISM 126 4.2.2 STEREOISOMERISM 127 4.3 POLYMER CONFORMATION 132 4.4
MOLECULAR DIMENSIONS IN THE AMORPHOUS STATE 135 4.4.1 RADIUS OF GYRATION
AND END-TO-END DISTANCE OF FLEXIBLE MACROMOLECULES 136 4.4.2 ROOT MEAN
SQUARE END-TO-END DISTANCE OF FLEXIBLE MACROMOLECULES 137 4.5 RUBBER
ELASTICITY 141 4.5.1 QUALITATIVE DESCRIPTION OF ELASTOMER BEHAVIOR 141
4.5.2 RUBBER AS AN ENTROPY SPRING 143 4.6 RODLIKE MACROMOLECULES 150
PROBLEMS 151 REFERENCES 153 CHAPTER 5 STEP-GROWTH POLYMERIZATIONS 5.1
CONDENSATION AND ADDITION POLYMERS 155 5.2 STEP-GROWTH AND CHAIN-GROWTH
POLYMERIZATIONS 158 5.3 REQUIREMENTS FOR STEP-GROWTH POLYMERIZATION 161
5.3.1 SPEED OF STEP-GROWTH POLYMERIZATIONS 164 5.3.2 SIDE REACTIONS IN
STEP-GROWTH POLYMERIZATION 164 5.4 POLYMER SIZE AND EXTENT OF CONVERSION
OF FUNCTIONAL GROUPS IN EQUILIBRIUM STEP-GROWTH POLYMERIZATIONS 166
5.4.1 BASIC ASSUMPTIONS 166 5.4.2 NUMBER AVERAGE DEGREE OF
POLYMERIZATION IN STEP-GROWTH REACTIONS 168 5.4.3 MOLECULAR WEIGHT
DISTRIBUTION IN EQUILIBRIUM STEP-GROWTH POLYMERIZATIONS 1 15 5.5
INTERFACIAL AND SOLUTION POLYMERIZATIONS OF ACID CHLORIDES AND OTHER
REACTIVE MONOMERS 182 5.6 STEP-GROWTH COPOLYMERIZATIONS 184 PROBLEMS 185
REFERENCES 188 CHAPTER 6 FREE-RADICAL POLYMERIZATION 6.1 SCOPE 189 6.2
POLYMERIZABILITY OF MONOMERS 190 6.3 OVERALL KINETICS OF RADICAL
POLYMERIZATION 192 6.3.1 INITIATION 192 6.3.2 PROPAGATION 193 6.3.3
TERMINATION 195 6.3.4 RATE OF POLYMERIZATION 196 6.3.5 INTEGRATED RATE
OF POLYMERIZATION EXPRESSION 198 6.4 A NOTE ON TERMINATION RATE
CONSTANTS 198 6.5 METHODS OF PRODUCING RADICALS 199 6.5.1 THERMAL
DECOMPOSITION OF INITIATORS 199 6.5.2 REDOX SOURCES 202 6.5.3
PHOTOCHEMICAL INITIATION 203 6.5.4 OTHER INITIATION METHODS 203 6.5.5
INITIATOR EFFICIENCY 204 6.5.6 MEASUREMENT OF K D 205 6.6 LENGTH OF THE
KINETIC CHAIN AND NUMBER AVERAGE DEGREE OF POLYMERIZATION OF THE POLYMER
206 6.7 MODES OF TERMINATION 207 6.8 CHAIN TRANSFER 208 6.8.1 TRANSFER
TO INITIATOR 210 6.8.2 TRANSFER TO MONOMER 211 6.8.3 TRANSFER TO SOLVENT
AND CHAIN AND TRANSFER AGENTS 213 6.8.4 CHAIN TRANSFER TO POLYMER 216
6.8.5 ALLYLIC TRANSFER 218 6.9 INHIBITION AND RETARDATION 219 6.10
READILY OBSERVABLE FEATURES OF FREE-RADICAL POLYMERIZATIONS 221 6.11
RADICAL LIFETIMES AND CONCENTRATIONS 222 6.12 DETERMINATION OF K P AND K
T 224 6.13 DEVIATIONS FROM IDEAL KINETICS 224 6.13.1 DIFFUSION CONTROL
OF TERMINATION 225 6.13.2 AUTOACCELERATION 226 6.14 MOLECULAR WEIGHT
DISTRIBUTION 227 6.14.1 LOW-CONVERSION POLYMERIZATION 227 6.14.2
HIGH-CONVERSION POLYMERIZATION 230 6.15 FREE-RADICAL TECHNIQUES FOR
POLYMERS WITH NARROWER MOLECULAR WEIGHT DISTRIBUTIONS 231 6.16 EFFECTS
OF TEMPERATURE 232 6.16.1 RATE AND DEGREE OF POLYMERIZATION 232 6.16.2
POLYMERIZATION-DEPOLYMERIZATION EQUILIBRIUM 233 6.17 FREE-RADICAL
POLYMERIZATION PROCESSES 236 PROBLEMS 236 REFERENCES 239 CHAPTER 7
COPOLYMERIZATION 7.1 CHAIN-GROWTH COPOLYMERIZATION 241 7.2 SIMPLE
COPOLYMER EQUATION 242 7.3 COPOLYMER STRUCTURE INFERENCES FROM
REACTIVITY RATIOS 245 7.3.1 RANDOM COPOLYMERS 245 7.3.2 ALTERNATING
COPOLYMERS 248 7.3.3 LONG SEQUENCES OF ONE MONOMER 248 7.3.4 BLOCK
COPOLYMERS 249 7.4 AZEOTROPIC COMPOSITIONS 249 7.5 INTEGRATED BINARY
COPOLYMER EQUATION 250 7.6 DETERMINATION OF REACTIVITY RATIOS 253 7.7
MULTICOMPONENT COPOLYMERIZATIONS 257 7.8 SEQUENCE DISTRIBUTION IN
COPOLYMERS 258 7.9 GEL FORMATION DURING COPOLYMERIZATION AND
CROSS-LINKING 260 7.10 REACTIVITIES OF RADICALS AND MONOMERS 263 7.10.1
RESONANCE EFFECTS 263 7.10.2 POLAR EFFECTS 264 7.10.3 STERIC EFFECTS 266
7.11 ANALYSIS OF REACTIVITY DATA 266 7.12 EFFECT OF REACTION CONDITIONS
268 7.12.1 TEMPERATURE 268 7.12.2 PRESSURE 269 7.12.3 MEDIUM 270 7.12.4
EFFECTS OF COMPLEX FORMATION 270 7.13 RATES OF FREE-RADICAL
COPOLYMERIZATIONS 271 7.14 ALTERNATIVE COPOLYMERIZATION MODELS 272
PROBLEMS 273 REFERENCES 276 CHAPTER 8 DISPERSION AND EMULSION
POLYMERIZATIONS 8.1 DISPERSION POLYMERIZATION 277 8.2 EMULSION
POLYMERIZATION 281 8.2.1 HARKINS-SMITH-EWART MECHANISM 285 8.2.2 ROLE OF
SURFACTANTS 288 8.2.3 SURFACTANT-FREE EMULSION POLYMERIZATIONS 289 8.2.4
MECHANISM OF EMULSION POLYMERIZATION 290 8.2.5 HETEROGENEOUS POLYMER
PARTICLES 292 8.3 OTHER INGREDIENTS IN EMULSION RECIPES 296 8.4 EMULSION
POLYMERIZATION PROCESSES 297 PROBLEMS 298 REFERENCES 298 CHAPTER 9 IONIC
AND COORDINATED POLYMERIZATIONS 9.1 COMPARISON OF IONIC AND FREE-RADICAL
POLYMERIZATIONS 301 9.2 ANIONIC POLYMERIZATION 303 9.2.1 OVERVIEW 303
9.2.2 ANIONIC INITIATION 305 9.2.3 ANIONIC PROPAGATION 310 9.2.4
TERMINATION REACTIONS 313 9.2.5 TEMPERATURE EFFECTS 313 9.2.6 ANIONIC
COPOLYMERIZATION REACTIONS 314 9.2.7 STEREOCHEMISTRY OF ANIONIC DIENE
POLYMERIZATION 316 9.3 GROUP TRANSFER POLYMERIZATION 318 9.4 CATIONIC
POLYMERIZATION 320 9.4.1 OVERVIEW 320 9.4.2 INITIATION OF POLYMERIZATION
OF VINYL MONOMERS 322 9.4.3 PROPAGATION REACTIONS 326 9.4.4 TERMINATION
AND TRANSFER PROCESSES 327 9.4.5 KINETICS OF CATIONIC POLYMERIZATION OF
OLEFINS 328 9.4.6 TEMPERATURE EFFECTS 330 9.4.7 POLYMERIZATION OF VINYL
AND CYCLIC ETHERS 332 9.4.8 LIVING CATIONIC POLYMERIZATIONS 333 9.5
COORDINATION POLYMERIZATION 333 9.5.1 ZIEGLER-NATTA CATALYSTS 334 9.5.2
KINETICS OF ZIEGLER-NATTA POLYMERIZATIONS 337 9.5.3 PRACTICAL FEATURES
OF ZIEGLER-NATTA POLYMERIZATIONS 338 9.5.4 COMPARISONS OF
CIS-1,4-POLYDIENES 340 9.5.5 METALLOCENE CATALYSTS 341 9.6 OLEFIN
METATHESIS CATALYSTS 344 PROBLEMS 346 REFERENCES 347 CHAPTER 10 POLYMER
REACTION ENGINEERING 10.1 SCOPE 349 10.2 STEP-GROWTH POLYMERIZATIONS 349
10.3 CHAIN-GROWTH POLYMERIZATIONS 353 10.4 HOMOGENEOUS AND HETEROGENEOUS
POLYMERIZATION PROCESSES 354 10.4.1 HOMOGENEOUS SYSTEMS 354 10.4.2
HETEROGENEOUS SYSTEMS 356 10.5 BATCH, SEMIBATCH, AND CONTINUOUS
PROCESSES 365 10.6 POLYMERIZATION REACTORS 366 10.6.1 BATCH REACTORS 366
10.6.2 TUBULAR REACTORS 368 10.6.3 CONTINUOUS STIRRED TANK REACTORS 369
PROBLEMS 374 REFERENCES 376 CHAPTER 11 MECHANICAL PROPERTIES OF POLYMER
SOLIDS AND LIQUIDS 11.1 INTRODUCTION 377 11.2 THERMAL TRANSITIONS 378
11.3 CRYSTALLIZATION OF POLYMERS 382 11.3.1 DEGREE OF CRYSTALLINITY 383
11.3.2 MICROSTRUCTURE OF SEMICRYSTALLINE POLYMERS 386 11.4 THE GLASS
TRANSITION 394 11.4.1 MODULUS-TEMPERATURE RELATIONS 394 11.4.2 EFFECT OF
POLYMER STRUCTURE ON T G 398 11.4.3 CORRELATIONS BETWEEN T M AND T G 401
11.4.4 MEASUREMENT OF T G 402 11.5 POLYMER VISCOELASTICITY 403 11.5.1
PHENOMENOLOGICAL VISCOELASTICITY 405 11.5.2 LINEAR VISCOELASTICITY 410
11.6 DYNAMIC MECHANICAL BEHAVIOR AT THERMAL TRANSITIONS 416 11.6.1
RELAXATIONS AT TEMPERATURES BELOW T G 418 11.7 STRESS-STRAIN TESTS 419
11.7.1 RATE AND TEMPERATURE EFFECTS 423 11.8 CRAZING IN GLASSY POLYMERS
423 11.9 FRACTURE MECHANICS 426 11.10 TOUGHNESS AND BRITTLENESS 429
11.11 RHEOLOGY 432 11.12 EFFECTS OF FABRICATION PROCESSES 440 PROBLEMS
441 REFERENCES 443 CHAPTER 12 POLYMER MIXTURES 12.1 COMPATIBILITY 445
12.2 THERMODYNAMIC THEORIES 446 12.2.1 REGULAR SOLUTIONS; SOLUBILITY
PARAMETER 447 12.2.2 FLORY-HUGGINS THEORY 454 12.2.3 MODIFIED SOLUBILITY
PARAMETER MODELS 458 12.3 SOLVENTS AND PLASTICIZERS 460 12.3.1 SOLVENTS
FOR COATING RESINS 460 12.3.2 PLASTICIZATION OF POLYMERS 461 12.4
FRACTIONATION 462 12.5 PRACTICAL ASPECTS OF POLYMER BLENDING 464 12.5.1
OBJECTIVES IN MAKING BLENDS 465 12.5.2 BLENDING OPERATIONS 465 12.5.3
PROCEDURES TO RETARD OR ELIMINATE DEMIXING OF POLYMER MIXTURES 468 12.6
REINFORCED ELASTOMERS 477 12.7 REINFORCED PLASTICS 478 PROBLEMS 481
REFERENCES 482 APPENDIX A: CONVERSION OF UNITS 485 APPENDIX B: LIST OF
SYMBOLS 487 INDEX 497
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| any_adam_object | 1 |
| author | Rudin, Alfred |
| author_facet | Rudin, Alfred |
| author_role | aut |
| author_sort | Rudin, Alfred |
| author_variant | a r ar |
| building | Verbundindex |
| bvnumber | BV024441188 |
| classification_rvk | VK 8000 |
| ctrlnum | (OCoLC)854670936 (DE-599)BVBBV024441188 |
| discipline | Chemie / Pharmazie |
| edition | 2. ed. |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T21:59:39Z |
| institution | BVB |
| isbn | 0126016852 |
| language | English |
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| oclc_num | 854670936 |
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| owner_facet | DE-83 DE-703 |
| physical | XVII, 509 S. graph. Darst. |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| publisher | Acad. Press |
| record_format | marc |
| spelling | Rudin, Alfred Verfasser aut The elements of polymer science and engineering an introductory text and reference for engineers and chemists Alfred Rudin 2. ed. San Diego [u.a.] Acad. Press 1999 XVII, 509 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polymerisation (DE-588)4046704-1 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Makromolekulare Chemie (DE-588)4168684-6 gnd rswk-swf 1\p (DE-588)4123623-3 Lehrbuch gnd-content Makromolekulare Chemie (DE-588)4168684-6 s 2\p DE-604 Polymere (DE-588)4046699-1 s 3\p DE-604 Polymerisation (DE-588)4046704-1 s 4\p DE-604 OEBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018418057&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 4\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Rudin, Alfred The elements of polymer science and engineering an introductory text and reference for engineers and chemists Polymerisation (DE-588)4046704-1 gnd Polymere (DE-588)4046699-1 gnd Makromolekulare Chemie (DE-588)4168684-6 gnd |
| subject_GND | (DE-588)4046704-1 (DE-588)4046699-1 (DE-588)4168684-6 (DE-588)4123623-3 |
| title | The elements of polymer science and engineering an introductory text and reference for engineers and chemists |
| title_auth | The elements of polymer science and engineering an introductory text and reference for engineers and chemists |
| title_exact_search | The elements of polymer science and engineering an introductory text and reference for engineers and chemists |
| title_full | The elements of polymer science and engineering an introductory text and reference for engineers and chemists Alfred Rudin |
| title_fullStr | The elements of polymer science and engineering an introductory text and reference for engineers and chemists Alfred Rudin |
| title_full_unstemmed | The elements of polymer science and engineering an introductory text and reference for engineers and chemists Alfred Rudin |
| title_short | The elements of polymer science and engineering |
| title_sort | the elements of polymer science and engineering an introductory text and reference for engineers and chemists |
| title_sub | an introductory text and reference for engineers and chemists |
| topic | Polymerisation (DE-588)4046704-1 gnd Polymere (DE-588)4046699-1 gnd Makromolekulare Chemie (DE-588)4168684-6 gnd |
| topic_facet | Polymerisation Polymere Makromolekulare Chemie Lehrbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018418057&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT rudinalfred theelementsofpolymerscienceandengineeringanintroductorytextandreferenceforengineersandchemists |