Industrial analysis with vibrational spectroscopy:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
Cambridge
Royal Soc. of Chemistry
1997
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| Schriftenreihe: | RSC analytical spectroscopy monographs
|
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | X, 380 S. Ill., graph. Darst. |
| ISBN: | 0854045651 |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804140400714186752 |
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| adam_text | ^SV^E RSC ANALYTICAL SPECTROSCOPY MONOGRAPHS INDUSTRIELL ANALYSIS WITH
VIBRATIONAL SPECTROSCOPY JOHN M. CHALMERS ICI TECHNOLOGY, RESEARCH &
TECHNOLOGY CENTRE, WILTON, UK GEOFFREY DENT ZENECA SPECIALTIES,
BLACKLEY, UK S ^ THE ROYAL JZ? SOCIETY OF CHEMISTRY INFORMATION
SERVICES CONTENTS CHAPTER 1 INTRODUCTION, BASIC THEORY, AND PRINCIPLES 1
1 INTRODUCTION 1 2 SIMPLE THEORY 3 3 MOLECULAR VIBRATIONS 3 4 SELECTION
RULES 5 5 PRACTICAL INTERPRETATION OF SPECTRA 9 SAMPLE PRESENTATION
FACTORS AFFECTING INTERPRETATION 12 INSTRUMENTATION FEATURES 15 BEWARE
THE COMPUTER - SPECTRUM MANIPULATION 17 STEP-BY-STEP APPROACH TO
INTERPRETATION 21 6 COMPUTER-AIDED SPECTRUM INTERPRETATION 25 LIBRARY
SEARCH SYSTEMS 25 STRUCTURAL DETERMINATION AIDS 25 SPECTRA FORMATS FOR
TRANSFER AND EXCHANGE OF DATA 26 THE INTERNET 26 7 INSTRUMENT
PERFORMANCE CHECKS 27 THE ICI/ZENECA POLYSTYRENE ROUND-ROBIRC TRIAL 27
COMMERCIALLY AVAILABLE TRACEABLE STANDARDS FOR INFRARED 32 RAMAN
SPECTROSCOPY CALIBRATION STANDARDS 32 8 QUANTIFICATION 33 9 CLOSING
REMARKS 33 10 BIBLIOGRAPHY 33 CHAPTER 2 SAMPLE TYPES AND ANALYSES 37 1
INTRODUCTION 37 2 STRUCTURAL INFORMATION 38 POLYMORPHISM 38 TAUTOMERISM
41 HYDROGEN BONDING 42 RACEMATES 45 3 FORMULATIONS 47 4 POLYMERS 47 5
FIBRES 47 VLLL CONTENTS 6 SURFACE ANALYSIS 54 7 INORGANICS, METAL
CO-ORDINATION COMPOUNDS, AND SEMI-CONDUCTORS 56 8 LIQUIDS 59 9 GASES AND
VAPOURS 60 10 CLOSING REMARKS 61 CHAPTER 3 INSTRUMENTATION 62 1
INTRODUCTION 62 2 INFRARED SPECTROMETERS 63 3 RAMAN SPECTROMETERS 63 4
SOURCES 65 INFRARED SOURCES 66 RAMAN SOURCES 66 5 DETECTORS 69 INFRARED
DETECTORS 69 RAMAN DETECTORS 79 6 FILTERS, PRISMS, GRAETINGS,
MONOCHROMATORS, AND INTERFEROMETERS 76 FILTERS 76 PRISMS AND GRAETINGS 78
MONOCHROMATORS (DISPERSIVE SPECTROMETERS) 79 INTERFEROMETERS 86 7
CLOSING REMARKS 117 CHAPTER 4 SAMPLING TECHNIQUES AND ACCESSORIES 120 1
GENERAL INTRODUCTION 120 2 BASIC PRINCIPLES OF SAMPLE PREPARATION FOR
INFRARED SPECTROSCOPY 120 3 WINDOW MATERIALS FOR INFRARED SPECTROSCOPY
121 4 PREPARATION AND CLEANING OF WINDOWS FOR INFRARED SPECTROSCOPY 123
5 TRANSMISSION TECHNIQUES FOR INFRARED SPECTROSCOPY 125 CAPILLARY FILMS
125 CAST FILMS 126 SPECTRUM QUALITY OF CAPILLARY AND CAST FILMS 127
FILMS FROM THE MELT 128 FIXED AND VARIABLE PATH-LENGTH CELLS 131 POWDER
SAMPLING METHODS 133 GASES AND VAPOURS 141 VARIABLE TEMPERATURE AND
PRESSURE 143 6 REFLECTION TECHNIQUES FOR INFRARED SPECTROSCOPY 144
INTERNAL REFLECTION SPECTROSCOPY (IRS) TECHNIQUES 145 DIFFUSE
REFLECTANCE INFRARED FOURIER TRANSFORM SPECTROSCOPY (DRIFTS) 153
CONTENTS IX SPECULAR REFLECTANCE 160 REFLECTION-ABSORPTION SPECTROSCOPY
162 7 PHOTOACOUSTIC SPECTROSCOPY (PAS) 165 8 EMISSION SPECTROSCOPY 168 9
RAMAN SAMPLE PREPARATION AND HANDLING 169 10 CLOSING REMARKS 174 11
BIBLIOGRAPHY 175 CHAPTER 5 QUANTITATIVE ANALYSIS 176 1 INTRODUCTION 176
2 INFRARED ABSORPTION 177 BEER S LAW 177 ABSORBANCE INTENSITY 181
MEASUREMENT OF PATH-LENGTH FOR TRANSMISSION MEASUREMENTS 183 NORMALISED
ABSORBANCE INTENSITY 186 3 RAMAN SCATTER INTENSITY 188 4 QUANTITATIVE
ANALYSIS OF VIBRATIONAL SPECTROSCOPIC DATA 190 CALIBRATION OF
QUANTITATIVE METHODS 191 BAND RATIO MEASUREMENTS 192 RATIO OF SPECTRA
METHOD 194 LEAST-SQUARES DETERMINATIONS AND MULTIPLE LINEAR REGRESSION
197 5 MULTICOMPONENT ANALYSES AND MULTIVARIATE TECHNIQUES 201 GENERAL
INTRODUCTION TO QUANTITATIVE MULTICOMPONENT ANALYSIS 202 THE AET-MATRIX
AND / -MATRIX METHODS 203 PRINCIPAL COMPONENT ANALYSIS (PCA) AND FACTOR
ANALYSIS (FA) 206 PRINCIPAL COMPONENT REGRESSION (PCR) AND PARTIAL LEAST
SQUARES (PLS) MODELLING 213 6 SPECTRAL ENHANCEMENT AND BAND RESOLUTION
TECHNIQUES 219 DERIVATIVE SPECTROSCOPY 220 FOURIER DOMAIN PROCESSING 224
CURVE-FITTING 228 MAXIMUM ENTROPY METHOD (MEM) AND MAXIMUM LIKELIHOOD
232 7 STATISTICAL EXPRESSIONS 235 8 CLOSING REMARKS 239 CHAPTER 6
VIBRATIONAL SPECTROSCOPY - MICROSAMPLING AND MICROSCOPY 241 1
INTRODUCTION 241 2 MICRO-SAMPLING BY RAMAN SPECTROSCOPY 242 X CONTENTS 3
MICRO-SAMPLING BY INFRARED SPECTROSCOPY 244 MICRO-SAMPLING OF GASES 244
MICRO-SAMPLING OF LIQUIDS 245 MICRO-SAMPLING OF SOLIDS 245 4 VIBRATIONAL
SPECTROSCOPY-MICROSCOPY 255 VIBRATIONAL SPECTROSCOPY-MICROSCOPY
INSTRUMENTATION 256 VIBRATIONAL SPECTROSCOPY-MICROSCOPY SAMPLE
PRESENTATION METHODS 269 5 VIBRATIONAL SPECTROSCOPY-MICROSCOPY
APPLICATIONS 277 VIBRATIONAL SPECTROSCOPY-MICROSCOPY APPLICATIONS:
CHEMICAL STUDIES 278 VIBRATIONAL SPECTROSCOPY-MICROSCOPY APPLICATIONS:
PHYSICAL CHARACTERISATIONS 304 6 CLOSING REMARKS 329 CHAPTER 7
HYPHENATED TECHNIQUES 331 1 INTRODUCTION 331 2 GAS CHROMATOGRAPHY-FTIR
(GC-FTIR) 332 COUPLED SYSTEMS 333 EFFECT OF GC COLUMN SELECTION 335 COLD
SPOTS 335 DEDICATED GC-FTIR SYSTEMS 335 COMPARISON OF DETECTOR SYSTEMS
AND THEIR SPECTRA 341 3 LIQUID AND GEL PERMEATION CHROMATOGRAPHY-FTIR
(HPLC-FTIR, GPC-FTIR) 351 FLOW-THROUGH TECHNIQUES 351 DEPOSITION
TECHNIQUES 353 4 SUPERCRITICAL FLUID CHROMATOGRAPHY-FTIR (SFC-FTIR) 359
5 OTHER HYPHENATED/COMBINATION TECHNIQUES 361 THIN LAYER CHROMATOGRAPHY
(TLC-FTIR, TLC-RAMAN) 361 EVOLVED GAS ANALYSIS (EGA-FTIR) 364
THERMOGRAVIMETRIC ANALYSIS (TGA-FTIR) 365 DIFFERENTIAL SCANNING
CALORIMETRY (DSC-FTIR, DSC-FT-RAMAN) 367 6 CLOSING REMARKS 368 SUBJECT
INDEX 371
|
| any_adam_object | 1 |
| author | Chalmers, John M. |
| author_facet | Chalmers, John M. |
| author_role | aut |
| author_sort | Chalmers, John M. |
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| building | Verbundindex |
| bvnumber | BV024427561 |
| classification_rvk | VG 9300 |
| ctrlnum | (OCoLC)636812078 (DE-599)BVBBV024427561 |
| discipline | Chemie / Pharmazie |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T21:59:23Z |
| institution | BVB |
| isbn | 0854045651 |
| language | Undetermined |
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| physical | X, 380 S. Ill., graph. Darst. |
| publishDate | 1997 |
| publishDateSearch | 1997 |
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| publisher | Royal Soc. of Chemistry |
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| series2 | RSC analytical spectroscopy monographs |
| spelling | Chalmers, John M. Verfasser aut Industrial analysis with vibrational spectroscopy John M. Chalmers ; Geoffrey Dent Cambridge Royal Soc. of Chemistry 1997 X, 380 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier RSC analytical spectroscopy monographs Dent, Geoffrey Sonstige oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018404944&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Chalmers, John M. Industrial analysis with vibrational spectroscopy |
| title | Industrial analysis with vibrational spectroscopy |
| title_auth | Industrial analysis with vibrational spectroscopy |
| title_exact_search | Industrial analysis with vibrational spectroscopy |
| title_full | Industrial analysis with vibrational spectroscopy John M. Chalmers ; Geoffrey Dent |
| title_fullStr | Industrial analysis with vibrational spectroscopy John M. Chalmers ; Geoffrey Dent |
| title_full_unstemmed | Industrial analysis with vibrational spectroscopy John M. Chalmers ; Geoffrey Dent |
| title_short | Industrial analysis with vibrational spectroscopy |
| title_sort | industrial analysis with vibrational spectroscopy |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=018404944&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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