Modulation calorimetry: theory and applications ; with 27 tables
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Berlin [u.a.]
Springer
2004
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 282 S. graph. Darst. 24 cm |
| ISBN: | 3540210822 |
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MARC
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| 245 | 1 | 0 | |a Modulation calorimetry |b theory and applications ; with 27 tables |c Yaakov Kraftmakher |
| 264 | 1 | |a Berlin [u.a.] |b Springer |c 2004 | |
| 300 | |a XII, 282 S. |b graph. Darst. |c 24 cm | ||
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Record in the Search Index
| _version_ | 1804138992489201664 |
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| adam_text | YAAKOV KRAFTMAKHER MODULATION CALORIMETRY THEORY AND APPLICATIONS WITH
196 FIGURES AND 27 TABLES SPRINGER TABLE OF CONTENTS 1 INTRODUCTION 1
1.1 HISTORY OF MODULATION METHODS 1 1.2 FEATURES OF MODULATION
TECHNIQUES 6 2 THEORY OF MODULATION CALORIMETRY 15 2.1 BASIC EQUATION OF
MODULATION CALORIMETRY , 15 2.1.1 SAMPLE IN A TEMPERATURE-MODULATED
REGIME 15 2.1.2 BASIC EQUATION 16 2.1.3 COMPLEX-FORM PRESENTATION 17
2.1.4 TEMPERATURE OSCILLATIONS IN RESISTIVELY HEATED WIRES 17 2.2
THERMAL COUPLING IN THE CALORIMETER CELL 19 2.2.1 SULLIVAN-SEIDEL
ANALYSIS 19 2.2.2 THERMAL CONDUCTANCE OF THE SAMPLE 20 2.2.3 MODEL
INCLUDING A SUBSTRATE 21 2.2.4 CHOICE OF MODULATION FREQUENCY 22 3
MODULATION OF HEATING POWER 23 3.1 DIRECT ELECTRIC HEATING AND RESISTIVE
HEATERS 23 3.1.1 DIRECT HEATING 23 3.1.2 SEPARATE RESISTIVE HEATERS 25
3.2 MODULATED-LIGHT HEATING 26 3.3 OTHER METHODS 28 3.3.1 ELECTRON
BOMBARDMENT 29 3.3.2 INDUCTION HEATING 30 3.3.3 PELTIER HEATING 31 4
MEASUREMENT OF TEMPERATURE OSCILLATIONS 33 4.1 OSCILLATIONS IN SAMPLE S
RESISTANCE 33 4.1.1 SUPPLEMENTARY-CURRENT TECHNIQUE 33 4.1.2
THIRD-HARMONIC METHOD 35 4.1.3 EQUIVALENT-IMPEDANCE TECHNIQUE 37 4.2
PHOTOELECTRIC DETECTORS 42 4.3 PYROELECTRIC SENSORS 45 4.4 THERMOCOUPLES
AND RESISTANCE THERMOMETERS 47 4.5 LOCK-IN DETECTION OF PERIODIC SIGNALS
50 5 BRIEF REVIEW OF METHODS OF CALORIMETRY 53 5.1 ADIABATIC CALORIMETRY
53 5.2 DROP METHOD 56 5.3 PULSE AND DYNAMIC TECHNIQUES 58 5.3.1 PULSE
METHOD 58 VIII TABLE OF CONTENTS 5.3.2 DYNAMIC CALORIMETRY 59 5.4
RELAXATION TECHNIQUES 65 5.5 RAPID-HEATING EXPERIMENTS 67 6 MODULATION
CALORIMETRY 1 73 6.1 HIGH TEMPERATURES 73 6.1.1 WIRE SAMPLES 73 6.1.2
NONADIABATIC REGIME 77 6.1.3 BULK SAMPLES 81 6.1.4 MOLTEN METALS 81
6.1.5 ACTIVE THERMAL SHIELD 81 6.1.6 NONCONDUCTING MATERIALS 82 6.1.7
NONCONTACT CALORIMETRY 84 6.2 MEDIUM TEMPERATURES 87 6.3 LOW
TEMPERATURES 89 6.4 MEASUREMENTS UNDER HIGH PRESSURES 91 6.5 MEASUREMENT
OF SPECIFIC HEAT AND THERMAL DIFFUSIVITY 96 6.6 SINKU-RIKO CALORIMETER
ACC-1 98 7 MODULATION CALORIMETRY II 101 7.1 MODULATION MICROCALORIMETRY
101 7.1.1 THIN DEPOSITED FILMS 101 7.1.2 FREESTANDING FILMS 102 7.1.3
BATH MODULATION 104 7.1.4 NANOCALORIMETRY AT LOW TEMPERATURES 104 7.2
ORGANIC AND BIOLOGICAL MATERIALS 107 7.3 PHOTOACOUSTIC TECHNIQUES 113
7.4 SPECIFIC-HEAT SPECTROSCOPY 115 7.4.1 MEASUREMENT OF THERMAL
EFFIISIVITY 115 7.4.2 FREQUENCY-DEPENDENT EFFUSIVITY 118 7.4.3 HOW TO
EXTEND THE FREQUENCY BAND - A PROPOSAL 121 7.4.4 WHAT IS WORTH
REMEMBERING 123 7.5 MODULATED DIFFERENTIAL SCANNING CALORIMETRY 124
7.5.1 PRINCIPLE OF MODULATED DIFFERENTIAL SCANNING CALORIMETRY 124 7.5.2
WHAT IS WORTH REMEMBERING 125 8 MODULATION DILATOMETRY 129 8.1 BRIEF
REVIEW OF DILATOMETIC TECHNIQUES 129 8.1.1 OPTICAL METHODS 130 8.1.2
CAPACITANCE DILATOMETERS 131 8.1.3 DYNAMIC TECHNIQUES 132 8.2 PRINCIPLE
OF MODULATION DILATOMETRY 135 8.2.1 WIRE SAMPLES . 135 8.2.2
DIFFERENTIAL METHOD 137 8.2.3 BULK SAMPLES 139 8.2.4 INTERFEROMETRIC
MODULATION DILATOMETER 140 8.2.5 NONCONDUCTING MATERIALS 142 8.3
EXTREMELY SMALL PERIODIC DISPLACEMENTS 143 TABLE OF CONTENTS IX 9 OTHER
MODULATION TECHNIQUES 147 9.1 TEMPERATURE DERIVATIVE OF RESISTANCE 147
9.2 DIRECT MEASUREMENT OF THERMOPOWER 151 9.3 SPECTRAL ABSORPTANCE 153
9.3.1 CALORIMETRIC TECHNIQUES 153 9.3.2 COMPENSATION METHOD. 156 10
NOISE THERMOMETRY OF WIRE SAMPLES 159 10.1 BRIEF HISTORY OF NOISE
THERMOMETRY 159 10.2 NOISE CORRELATION THERMOMETER 164 10.2.1
CORRELATION AMPLIFIER 164 10.2.2 COMPENSATION METHOD 165 10.2.3
TEMPERATURE DERIVATIVE OF RESISTANCE 167 10.2.4 NYQUIST S FORMULA FOR
HIGH CURRENT DENSITIES 168 11 ELECTRONICS FOR MODULATION MEASUREMENTS
169 11.1 ELECTRONIC INSTRUMENTS 169 11.2 EXAMPLES OF MODULATION SET-UPS
172 12 ACCURACY OF MODULATION MEASUREMENTS 177 12.1 REQUIREMENTS FOR
MODULATION EXPERIMENTS 177 12.2 COMPARISON WITH RECOMMENDED VALUES 180
12.2.1 SPECIFIC HEAT OF TUNGSTEN, COPPER, AND IRON 180 12.2.2 SPECIFIC
HEAT OF MOLYBDENUM AND PLATINUM 182 12.2.3 THERMAL EXPANSION OF TUNGSTEN
AND PLATINUM 183 12.2.4 ELECTRICAL RESISTIVITY OF PLATINUM 185 13
STUDIES AT HIGH TEMPERATURES 187 13.1 EQUILIBRIUM POINT DEFECTS IN
METALS 187 13.1.1 SPECIFIC HEAT 189 13.1.2 THERMAL EXPANSION 191 13.1.3
ELECTRICAL RESISTIVITY 192 13.1.4 EQUILIBRIUM CONCENTRATIONS OF POINT
DEFECTS 193 13.2 TEMPERATURE COEFFICIENT OF SPECIFIC HEAT 196 13.3
UNEXPECTED PREMELTING ANOMALY 199 13.4 ISOCHORIC SPECIFIC HEAT OF SOLDS
201 13.4.1 TEMPERATURE FLUCTUATIONS 201 13.4.2 EXPERIMENTAL 202 13.4.3
DETERMINATION OF THE CP/C V RATIO 204 14 PHASE TRANSITIONS 207 14.1
FIRST- AND SECOND-ORDER PHASE TRANSITIONS 207 14.2 FERRO- AND
ANTIFERROMAGNETS 211 14.3 SUPERCONDUCTORS 217 14.4 THIN FILMS AND
CONFINED SYSTEMS 222 15 RELAXATION PHENOMENA 227 15.1 FORMULAS FOR
RELAXATION 228 15.2 GLASS TRANSITIONS 230 15.3 POINT-DEFECT
EQUILIBRATION IN METALS 232 15.3.1 ENHANCEMENT OF MODULATION FREQUENCY
232 TABLE OF CONTENTS ; 15.3.2 RELAXATION PHENOMENON IN TUNGSTEN AND
PLATINUM 234 15.3.3 EQUILIBRATION TIMES 235 15.3.4 TWO PROPOSALS FOR
STUDIES OF VACANCY EQUILIBRATION 236 ; 15.3.5 QUESTIONS TO BE ANSWERED
BY RAPID-HEATING EXPERIMENTS.... 237 J 15.3.6 DETERMINATION OF
VACANCY-RELATED ENTHALPY - A PROPOSAL.... 239 I 15.4 OTHER EXAMPLES OF
RELAXATION IN SPECIFIC HEAT 242 1 16 FIVE STUDENT EXPERIMENTS 245 16.1
PULSE CALORIMETRY 245 16.2 PRINCIPLES OF MODULATION CALORIMETRY 248 16.3
THIRD-HARMONIC TECHNIQUE 250 16.4 EQUIVALENT-IMPEDANCE METHOD 252 16.5
DETERMINATION OF BOLTZMANN S CONSTANT 254 CONCLUSION 259 REFERENCES 261
INDEX 283
|
| any_adam_object | 1 |
| author | Kraftmakher, Yaakov |
| author_facet | Kraftmakher, Yaakov |
| author_role | aut |
| author_sort | Kraftmakher, Yaakov |
| author_variant | y k yk |
| building | Verbundindex |
| bvnumber | BV023796349 |
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| dewey-full | 536.6 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 536 - Heat |
| dewey-raw | 536.6 |
| dewey-search | 536.6 |
| dewey-sort | 3536.6 |
| dewey-tens | 530 - Physics |
| discipline | Chemie / Pharmazie Physik Mess-/Steuerungs-/Regelungs-/Automatisierungstechnik / Mechatronik |
| format | Book |
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| id | DE-604.BV023796349 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T21:37:00Z |
| institution | BVB |
| isbn | 3540210822 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017438553 |
| oclc_num | 249146766 |
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| owner | DE-634 DE-11 |
| owner_facet | DE-634 DE-11 |
| physical | XII, 282 S. graph. Darst. 24 cm |
| publishDate | 2004 |
| publishDateSearch | 2004 |
| publishDateSort | 2004 |
| publisher | Springer |
| record_format | marc |
| spelling | Kraftmakher, Yaakov Verfasser aut Modulation calorimetry theory and applications ; with 27 tables Yaakov Kraftmakher Berlin [u.a.] Springer 2004 XII, 282 S. graph. Darst. 24 cm txt rdacontent n rdamedia nc rdacarrier Kalorimetrie (DE-588)4029367-1 gnd rswk-swf Temperaturmodulation (DE-588)4184692-8 gnd rswk-swf Kalorimetrie (DE-588)4029367-1 s Temperaturmodulation (DE-588)4184692-8 s DE-604 HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017438553&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kraftmakher, Yaakov Modulation calorimetry theory and applications ; with 27 tables Kalorimetrie (DE-588)4029367-1 gnd Temperaturmodulation (DE-588)4184692-8 gnd |
| subject_GND | (DE-588)4029367-1 (DE-588)4184692-8 |
| title | Modulation calorimetry theory and applications ; with 27 tables |
| title_auth | Modulation calorimetry theory and applications ; with 27 tables |
| title_exact_search | Modulation calorimetry theory and applications ; with 27 tables |
| title_full | Modulation calorimetry theory and applications ; with 27 tables Yaakov Kraftmakher |
| title_fullStr | Modulation calorimetry theory and applications ; with 27 tables Yaakov Kraftmakher |
| title_full_unstemmed | Modulation calorimetry theory and applications ; with 27 tables Yaakov Kraftmakher |
| title_short | Modulation calorimetry |
| title_sort | modulation calorimetry theory and applications with 27 tables |
| title_sub | theory and applications ; with 27 tables |
| topic | Kalorimetrie (DE-588)4029367-1 gnd Temperaturmodulation (DE-588)4184692-8 gnd |
| topic_facet | Kalorimetrie Temperaturmodulation |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017438553&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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