Analytical chemistry of macrocyclic and supramolecular compounds:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New Delhi [u.a.]
Narosa Publ. House
2008
|
| Ausgabe: | 2. ed., repr. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XXI, 347 S. graph. Darst. |
| ISBN: | 9788173196812 |
Internformat
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| 245 | 1 | 0 | |a Analytical chemistry of macrocyclic and supramolecular compounds |c S. M. Khopkar |
| 250 | |a 2. ed., repr. | ||
| 264 | 1 | |a New Delhi [u.a.] |b Narosa Publ. House |c 2008 | |
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Datensatz im Suchindex
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|---|---|
| adam_text | Titel: Analytical chemistry of macrocyclic and supramolecular compounds
Autor: Khopkar, Shripad Moreshwar
Jahr: 2008
Contents
Preface to the Second Edition vii
Preface to the First Edition ix
Acknowledgement xiii
Symbols and Abbreviations xv
1. Introduction 1
1.1 Introduction 1
1.2 History 2
1.3 Classification of compounds 5
1.4 Nomenclature 5
1.5 Characteristics of crown compounds 7
1.6 Solubility in solvents 7
1.7 Significant properties of crown compounds 7
1.8 Recent developments in macrocyclic and supramolecular
compounds 9
1.9 Toxicological manifestations 11
1.10 Physiological properties of calixarenes 14
1.11 Toxicity of cryptands and crown compounds 14
1.12 Handling precautions 14
Conclusion 14
References 75
2. Synthesis of Crown Compounds 18
2.1 Introduction 18
2.2 Synthesis of crown ethers 19
2.3 The template effect 20
2.4 Recent developments in the synthesis of crown ethers 22
2.5 Synthesis of cryptands 24
2.6 New developments in the synthesis of cryptands 27
2.7 Synthesis of aza crown ethers 28
2.8 Synthesis of thia crown ethers and related compounds 30
2.9 Chiral crown ethers 31
2.10 Proton ionisable crown ethers 31
2.11 Diester crown ethers 31
2.12 New developments in thia and aza crown ether
synthesis 32
2.13 Synthesis of calix (n) arenes 33
2.14 Recent developments in synthesis of calixarenes 41
Conclusion 44
References 45
xviii Contents
3. Characterisation and Metal Complexation 51
3.1 Introduction 57
3.2 Metal complexes with crown ethers 52
3.3 Metal complexes with cryptands 57
3.4 Characterisation of complexes by absorption spectroscopy 58
3.5 Characterisation of crown complexes by NMR
spectroscopy 59
3.6 Metal complexes with calixarenes 65
3.7 Characterisation of calix(n)arene complexes by NMR
spectroscopy 69
3.8 Characterisation of calixarene complexes by mass
spectrometry 73
Conclusion 74
References 76
4. Metal Complexes and Their Structure 82
4.1 Introduction 82
4.2 Structure in the solution 87
4.3 Complexation and structure elucidation by classical
methods 90
4.4 Metal complexes structure studies by X-ray methods 94
4.5 Structure of complex by thermal methods 101
4.6 Structure of the complex by radiochemical methods 103
Conclusion 103
References 705
5. Solvent Extraction Separations 113
5.1 Introduction 773
5.2 Extraction equilibria with crown ethers 774
5.3 Interpretation of equilibria ¡14
5.4 Factors influencing extraction 777
5.5 Solvent extraction separations with crown ethers 725
5.6 Solvent extractions with cryptands 727
5.7 Solvent extractions with aza and thia crown ethers 135
5.8 Solvent extractions with calixarenes 7J7
Conclusion 144
References 144
6. Chromatographic Separations 155
6.1 Introduction 755
6.2 Column chromatography 756
6.3 High performance liquid chromatography 759
6.4 Gas chromatographic separations 762
6.5 Reversed phase extraction chromatography 767
6.6 Ion exchange chromatography 769
6.7 Ion chromatography separation 777
6.8 Capillary electrophoresis with crown compounds 775
Conclusion 178
References 779
Contents xix
7. Extractive Spectrophotometry 186
7.1 Introduction 186
7.2 Classification of chromoionophores 188
7.3 Neutral chromoionophores 188
7.4 Monoprotonic crown ether dyes 189
7.5 Diprotonic crown ether chromoionophores 192
7.6 Other protonic chromoionophores 193
7.7 Analytical applications of crown ethers in extraction
photometry 194
7.8 Application of cryptands in extractive photometry 197
7.9 Application of thia and aza crown ethers in extraction
photometry 204
7.10 Applications of calixarene in extractive photometry 205
Conclusion 209
References 209
8. Extractive Emission Spectroscopy with Crown
Cryptands and Calixarenes 215
8.1 Introduction 215
8.2 Fluoroionophores 217
8.3 Ring substituted fluorogenic crown ethers 218
8.4 Luminescence characterisation of lanthanide by
crown ethers 279
8.5 Lanthanide complexes as supramolecular photochemical
devices 221
8.6 Analytical application in fluorescence spectroscopy 223
8.7 Atomic emission spectroscopie analysis with crown
compounds 224
8.8 Applications of emission spectroscopy for analysis 225
8.9 Atomic absorption spectroscopy with crown
compounds 228
8.10 Analytical application of AAS with crown ethers and
cryptand extractions 228
8.11 Recent advances in switched on crown ethers 231
8.12 Photoresponsive switching crown ethers 233
Conclusion 235
References 235
9. Electroanalytical Methods with Crown Compounds 240
9.1 Introduction 240
9.2 Potentiometry 241
9.3 Analytical applications of potentiometry 243
9.4 Conductometric studies of complexes with crown
ethers 245
9.5 Analytical applications of conductometry with crown
compounds 247
9.6 Polarography 248
xx Contents
9.7 Cyclic voltammetry 249
9.8 Analytical applications of voltammetry with crown
compounds 251
9.9 Coulometry and its analytical applications 254
9.10 Electrochemistry of supramolecular compounds 255
Conclusion 256
References 256
10. Ion Selective Electrodes and Membrane Transport
with Crown Compounds 261
10.1 Introduction 261
10.2 Characteristics of the electrode 262
10.3 Crown ethers as neutral carriers 265
10.4 Bis (crown ethers) in ion selective electrodes 265
10.5 Analytical applications of crown compounds in ion selective
electrodes 270
10.6 Membrane transport 273
10.7 Separations with liquid membranes 278
10.8 Experimental set up for ion transport work 279
10.9 Applications of membrane transport 280
10.10 Novel role of crown and pondant as ionophores 281
10.11 Transportation of ions across membrane 281
10.12 Analytical applications of membrane transport with crown
compounds 282
Conclusion 285
References 287
11. Chromogenic Crown Ethers in Solvent Extraction 293
11.1 Introduction 293
11.2 Modified crown ethers 293
11.3 Early work in colorimetric determination 295
11.4 Benzo crown ethers and its derivatives in extraction 296
11.5 Chromogenic crown ethers with side arms 298
11.6 Crown ethers with two replacable Hydrogen atoms 299
11.7 Uncharged crown ethers dyes 300
11.8 Photometric determinations with chromogenic crown ethers 301
11.9 Metal complexes and their characteristics 301
11.10 Selection of crown compound for photometric analysis 305
Conclusion 306
References 307
12. Rotaxanes, Synthesis, Characteristics and Applications 310
12.1 Introduction 310
12.2 Classification of rotaxanes 312
12.3 Mode of synthesis of rotaxanes 313
12.4 Characterisation of rotaxanes 314
12.5 Rotaxane—synthesis and characteristics 575
12.6 Polyrotaxane—synthesis and characteristics 318
Contents xxi
12.7 Substituted rotaxanes—Synthesis and Characteristics 321
12.8 Metal complexes with Rotaxanes 326
12.9 The [2] rotaxanes and their alkali metal complexation 329
12.10 Applications of rotaxanes 331
12.11 Chromatographie separations by rotaxane polymer 331
12.12 Solvent extraction separations with rotaxanes 332
Conclusion 333
References 334
Index 340
|
| adam_txt |
Titel: Analytical chemistry of macrocyclic and supramolecular compounds
Autor: Khopkar, Shripad Moreshwar
Jahr: 2008
Contents
Preface to the Second Edition vii
Preface to the First Edition ix
Acknowledgement xiii
Symbols and Abbreviations xv
1. Introduction 1
1.1 Introduction 1
1.2 History 2
1.3 Classification of compounds 5
1.4 Nomenclature 5
1.5 Characteristics of crown compounds 7
1.6 Solubility in solvents 7
1.7 Significant properties of crown compounds 7
1.8 Recent developments in macrocyclic and supramolecular
compounds 9
1.9 Toxicological manifestations 11
1.10 Physiological properties of calixarenes 14
1.11 Toxicity of cryptands and crown compounds 14
1.12 Handling precautions 14
Conclusion 14
References 75
2. Synthesis of Crown Compounds 18
2.1 Introduction 18
2.2 Synthesis of crown ethers 19
2.3 The template effect 20
2.4 Recent developments in the synthesis of crown ethers 22
2.5 Synthesis of cryptands 24
2.6 New developments in the synthesis of cryptands 27
2.7 Synthesis of aza crown ethers 28
2.8 Synthesis of thia crown ethers and related compounds 30
2.9 Chiral crown ethers 31
2.10 Proton ionisable crown ethers 31
2.11 Diester crown ethers 31
2.12 New developments in thia and aza crown ether
synthesis 32
2.13 Synthesis of calix (n) arenes 33
2.14 Recent developments in synthesis of calixarenes 41
Conclusion 44
References 45
xviii Contents
3. Characterisation and Metal Complexation 51
3.1 Introduction 57
3.2 Metal complexes with crown ethers 52
3.3 Metal complexes with cryptands 57
3.4 Characterisation of complexes by absorption spectroscopy 58
3.5 Characterisation of crown complexes by NMR
spectroscopy 59
3.6 Metal complexes with calixarenes 65
3.7 Characterisation of calix(n)arene complexes by NMR
spectroscopy 69
3.8 Characterisation of calixarene complexes by mass
spectrometry 73
Conclusion 74
References 76
4. Metal Complexes and Their Structure 82
4.1 Introduction 82
4.2 Structure in the solution 87
4.3 Complexation and structure elucidation by classical
methods 90
4.4 Metal complexes structure studies by X-ray methods 94
4.5 Structure of complex by thermal methods 101
4.6 Structure of the complex by radiochemical methods 103
Conclusion 103
References 705
5. Solvent Extraction Separations 113
5.1 Introduction 773
5.2 Extraction equilibria with crown ethers 774
5.3 Interpretation of equilibria ¡14
5.4 Factors influencing extraction 777
5.5 Solvent extraction separations with crown ethers 725
5.6 Solvent extractions with cryptands 727
5.7 Solvent extractions with aza and thia crown ethers 135
5.8 Solvent extractions with calixarenes 7J7
Conclusion 144
References 144
6. Chromatographic Separations 155
6.1 Introduction 755
6.2 Column chromatography 756
6.3 High performance liquid chromatography 759
6.4 Gas chromatographic separations 762
6.5 Reversed phase extraction chromatography 767
6.6 Ion exchange chromatography 769
6.7 Ion chromatography separation 777
6.8 Capillary electrophoresis with crown compounds 775
Conclusion 178
References 779
Contents xix
7. Extractive Spectrophotometry 186
7.1 Introduction 186
7.2 Classification of chromoionophores 188
7.3 Neutral chromoionophores 188
7.4 Monoprotonic crown ether dyes 189
7.5 Diprotonic crown ether chromoionophores 192
7.6 Other protonic chromoionophores 193
7.7 Analytical applications of crown ethers in extraction
photometry 194
7.8 Application of cryptands in extractive photometry 197
7.9 Application of thia and aza crown ethers in extraction
photometry 204
7.10 Applications of calixarene in extractive photometry 205
Conclusion 209
References 209
8. Extractive Emission Spectroscopy with Crown
Cryptands and Calixarenes 215
8.1 Introduction 215
8.2 Fluoroionophores 217
8.3 Ring substituted fluorogenic crown ethers 218
8.4 Luminescence characterisation of lanthanide by
crown ethers 279
8.5 Lanthanide complexes as supramolecular photochemical
devices 221
8.6 Analytical application in fluorescence spectroscopy 223
8.7 Atomic emission spectroscopie analysis with crown
compounds 224
8.8 Applications of emission spectroscopy for analysis 225
8.9 Atomic absorption spectroscopy with crown
compounds 228
8.10 Analytical application of AAS with crown ethers and
cryptand extractions 228
8.11 Recent advances in switched on crown ethers 231
8.12 Photoresponsive switching crown ethers 233
Conclusion 235
References 235
9. Electroanalytical Methods with Crown Compounds 240
9.1 Introduction 240
9.2 Potentiometry 241
9.3 Analytical applications of potentiometry 243
9.4 Conductometric studies of complexes with crown
ethers 245
9.5 Analytical applications of conductometry with crown
compounds 247
9.6 Polarography 248
xx Contents
9.7 Cyclic voltammetry 249
9.8 Analytical applications of voltammetry with crown
compounds 251
9.9 Coulometry and its analytical applications 254
9.10 Electrochemistry of supramolecular compounds 255
Conclusion 256
References 256
10. Ion Selective Electrodes and Membrane Transport
with Crown Compounds 261
10.1 Introduction 261
10.2 Characteristics of the electrode 262
10.3 Crown ethers as neutral carriers 265
10.4 Bis (crown ethers) in ion selective electrodes 265
10.5 Analytical applications of crown compounds in ion selective
electrodes 270
10.6 Membrane transport 273
10.7 Separations with liquid membranes 278
10.8 Experimental set up for ion transport work 279
10.9 Applications of membrane transport 280
10.10 Novel role of crown and pondant as ionophores 281
10.11 Transportation of ions across membrane 281
10.12 Analytical applications of membrane transport with crown
compounds 282
Conclusion 285
References 287
11. Chromogenic Crown Ethers in Solvent Extraction 293
11.1 Introduction 293
11.2 Modified crown ethers 293
11.3 Early work in colorimetric determination 295
11.4 Benzo crown ethers and its derivatives in extraction 296
11.5 Chromogenic crown ethers with side arms 298
11.6 Crown ethers with two replacable Hydrogen atoms 299
11.7 Uncharged crown ethers dyes 300
11.8 Photometric determinations with chromogenic crown ethers 301
11.9 Metal complexes and their characteristics 301
11.10 Selection of crown compound for photometric analysis 305
Conclusion 306
References 307
12. Rotaxanes, Synthesis, Characteristics and Applications 310
12.1 Introduction 310
12.2 Classification of rotaxanes 312
12.3 Mode of synthesis of rotaxanes 313
12.4 Characterisation of rotaxanes 314
12.5 Rotaxane—synthesis and characteristics 575
12.6 Polyrotaxane—synthesis and characteristics 318
Contents xxi
12.7 Substituted rotaxanes—Synthesis and Characteristics 321
12.8 Metal complexes with Rotaxanes 326
12.9 The [2] rotaxanes and their alkali metal complexation 329
12.10 Applications of rotaxanes 331
12.11 Chromatographie separations by rotaxane polymer 331
12.12 Solvent extraction separations with rotaxanes 332
Conclusion 333
References 334
Index 340 |
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| id | DE-604.BV023319338 |
| illustrated | Illustrated |
| index_date | 2024-07-02T20:53:07Z |
| indexdate | 2024-07-09T21:15:46Z |
| institution | BVB |
| isbn | 9788173196812 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016503456 |
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| physical | XXI, 347 S. graph. Darst. |
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| publisher | Narosa Publ. House |
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| spelling | Khopkar, Shripad Moreshwar Verfasser aut Analytical chemistry of macrocyclic and supramolecular compounds S. M. Khopkar 2. ed., repr. New Delhi [u.a.] Narosa Publ. House 2008 XXI, 347 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Literaturangaben Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Kronenether (DE-588)4165804-8 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s Kronenether (DE-588)4165804-8 s DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016503456&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Khopkar, Shripad Moreshwar Analytical chemistry of macrocyclic and supramolecular compounds Analytische Chemie (DE-588)4129906-1 gnd Kronenether (DE-588)4165804-8 gnd |
| subject_GND | (DE-588)4129906-1 (DE-588)4165804-8 |
| title | Analytical chemistry of macrocyclic and supramolecular compounds |
| title_auth | Analytical chemistry of macrocyclic and supramolecular compounds |
| title_exact_search | Analytical chemistry of macrocyclic and supramolecular compounds |
| title_exact_search_txtP | Analytical chemistry of macrocyclic and supramolecular compounds |
| title_full | Analytical chemistry of macrocyclic and supramolecular compounds S. M. Khopkar |
| title_fullStr | Analytical chemistry of macrocyclic and supramolecular compounds S. M. Khopkar |
| title_full_unstemmed | Analytical chemistry of macrocyclic and supramolecular compounds S. M. Khopkar |
| title_short | Analytical chemistry of macrocyclic and supramolecular compounds |
| title_sort | analytical chemistry of macrocyclic and supramolecular compounds |
| topic | Analytische Chemie (DE-588)4129906-1 gnd Kronenether (DE-588)4165804-8 gnd |
| topic_facet | Analytische Chemie Kronenether |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016503456&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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