Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English German |
| Published: |
Pirna
Forum für Abfallwirtschaft und Altlasten
2008
|
| Edition: | 1. Aufl. |
| Series: | Beiträge zu Abfallwirtschaft, Altlasten
55 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | IX, 114 S. Ill., graph. Darst. |
| ISBN: | 9783934253476 |
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| 245 | 1 | 0 | |a Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites |c Catalin Stefan |
| 250 | |a 1. Aufl. | ||
| 264 | 1 | |a Pirna |b Forum für Abfallwirtschaft und Altlasten |c 2008 | |
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Record in the Search Index
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| adam_text | DISSERTATION IMPROVEMENTS OF CHARACTERIZATION OF SINGLE AND MULTISOLUTE
ADSORPTION OF METHYL TERF-BUTYL ETHER (MTBE) ON ZEOLITES CATALIN STEFAN
HERAUSGEBER PROF. DR.-ING. HABIL. DR. H. C. B. BILITEWSKI PROF. DR. RER.
NAT. P. WERNER BEITRAGE ZU ABFALLWIRTSCHAFT/ALTLASTEN SCHRIFTENREIHE DES
INSTITUTES FUR ABFALLWIRTSCHAFT UND ALTLASTEN TECHNISCHE UNIVERSITAT
DRESDEN BAND 55 ISBN 978-3-934253-47-6 2008 1. AUFLAGE TABLE OF CONTENTS
TABLE OF CONTENTS 1. INTRODUCTION 1 1.1 SHORT INTRODUCTION 1 1.2
OBJECTIVES 1 1.2.1 OVERALL OBJECTIVE 1 1.2.2 SPECIFIC OBJECTIVES 2 2.
ABOUT MTBE 3 2.1 GENERAL FACTS 3 2.2 PRODUCTION AND DEMAND RATES 3 2.3
OCCURRENCE OF MTBE IN GERMANY 6 2.3.1 OCCURRENCE OF MTBE IN GROUNDWATER
: 7 2.3.2 MTBE IN RIVER AND WASTE WATER 7 2.3.3 MTBE IN DRINKING WATER 7
2.3.4. MTBE IN URBAN AND RURAL PRECIPITATIONS 8 2.4 SOURCES OF
CONTAMINATION WITH MTBE 8 2.4.1 POINT SOURCES 8 2.4.2 NON-POINT SOURCES
8 2.5 TRANSPORT 9 2.6 PHYSICAL - CHEMICAL PROPERTIES 9 2.6.1 CRITICAL
PROPERTIES-INFLUENCING THE BEHAVIOR OF MTBE 10 2.7 TOXICITY AND IMPACT
ON HUMAN HEALTH 11 2.8 MTBE REGULATIONS 11 2.8.1 IN THE US 11 2.8.2 IN
EUROPE , 12 3. EVALUATION OF ACTUAL MTBE TREATMENT TECHNOLOGIES 13 3.1
BIODEGRADATION 13 3.2. AIR STRIPPING 14 3.3 ADVANCED OXIDATION 14 3.4
HOLLOW FIBER MEMBRANES (HFM) 14 3.5 PERVAPORATION 15 3.6
PHYTOREMEDIATION 15 3.7 SORPTION PROCESSES 15 3.8 CONCLUSIONS 16 4.
ZEOLITES 17 4.1 HISTORY 17 4.2 USES 17 4.3 COMPOSITION 17 4.4 ZEOLITE
ZSM-5 19 5. THEORY OF SORPTION 21 5.1 SORPTION MECHANISMS 21 5.1.1
PARTITIONING 21 5.1.2 MONOLAYER, MULTILAYER AND PORE-FILLING 22 5.1.3
ADSORPTION ISOTHERMS 23 5.2 FITTING DATA WITH DIFFERENT MODELS 24 5.2.1
DATA PREPARATION 25 5.2.2 CHOOSING THE ADSORPTION MODEL 27 5.2.2.1
LINEAR ISOTHERM - ONE FITTING PARAMETER 27 - I - TABLE OF CONTENTS
5.2.2.2 NON-LINEAR ISOTHERMS - TWO FITTING PARAMETERS 28 5.2.2.3
NON-LINEAR ISOTHERMS - THREE FITTING PARAMETERS 30 5.2.2.4 NON-LINEAR
ISOTHERMS - FOUR FITTING PARAMETERS 32 5.2.2.5 OTHER ISOTHERMS 32 5.2.3
GOODNESS-OF-FIT 33 5.3 CONCLUSION 35 5.4 DEVELOPMENT OF ADSORPTION
SOFTWARE 36 6. MATERIALS AND METHODS 37 6.1 ADSORBENTS 37 6.1.1 ZEOLITES
37 6.1.2 ACTIVATED CARBON 37 6.2 ADSORBATES 38 6.2.1 MTBE 38 6.2.2 BTEX
38 6.3 METHODS 38 6.3.1 BATCH TESTS PREPARATION 38 6.3.2 ANALYTICS 38 7.
RESULTS AND DISCUSSION 39 7.1 SCREENING BETWEEN DIFFERENT ADSORBENTS 39
7.2 ADSORPTION KINETIC 41 7.3 CHARACTERIZATION OF ZEOLITES 42 7.3.1
SCANNING ELECTRON MICROSCOPY (SEM) 42 7.3.2 BET ANALYSIS DATA 43 7.3.3
PARTICLE SIZE CALCULATION 44 7.4 ADSORPTION OF MTBE AND BTEX ON ZEOLITE
ZSM-5 (600) 45 7.4.1 LINEAR ADSORPTION 45 7.4.2 FREUNDLICH ADSORPTION
ISOTHERMS . . 46 7.4.3 SOLUBILITY NORMALIZED FREUNDLICH ISOTHERMS 47
7.4.4 LANGMUIR ADSORPTION ISOTHERMS 48 7.4.5 T6TH ADSORPTION ISOTHERMS
50 7.4.6 DUBININ-POLANYI ISOTHERMS (SOLUBILITY NORMALIZED) 52 7.4.7
LANGMUIR - FREUNDLICH ADSORPTION ISOTHERMS 53 7.4.8 GENERALIZED LANGMUIR
ADSORPTION ISOTHERM 55 7.4.9 MTBE SORPTION MECHANISM 55 7.4.10
ADSORPTION CAPACITIES FOR MTBE AND BTEX 56 7.4.11 GOODNESS OF FIT 58
7.4.12 EFFECT OF NORMALIZATION 60 7.4.13 OPTIMISATION OF NON-LINEAR
REGRESSION BY ERROR ANALYSIS 62 7.5 EFFECT OF COMPETITIVE SORPTION
(INFLUENCE OF BTEX) 66 7.6 IMPACT OF NATURAL ORGANIC MATTER (NOM) 69 8.
PRACTICAL IMPLICATIONS 71 8.1 ADSORBENT REGENERATION 71 8.2 ADSORBENT
USAGE RATES 73 8.3 PACKED BED LIFE 74 8.4 COSTS EVALUATION 76 9.
COMPARISON OF OWN RESULTS WITH REFERENCES 78 9.1 DATA INTERPRETATION 78
9.2 REMOVAL OF MTBE BY ADSORPTION ON ZEOLITES AND RESINS 78 9.3 REMOVAL
OF MTBE BY ADSORPTION ON ACTIVATED CARBON 82 -II - TABLE OF CONTENTS 9.4
EFFECT OF CO-CONTAMINATION 83 9.5 SUMMARY 84 10. GENERAL CONCLUSIONS 86
11. PERSPECTIVES (FURTHER WORK) 88 12. REFERENCES 89 APPENDICES 108
APPENDIX A. ADSORPTION EXPERIMENTAL DATA 109 APPENDIX A. 1 - ADSORPTION
OF MTBE ON ZEOLITE ZSM-5 (600) GRANULES 110 APPENDIX A.2 - EFFECT OF
BTEX CO-CONTAMINATION ON MTBE ADSORPTION 111 APPENDIX A.3 - ADSORPTION
OF MTBE AND BTEX ON ZEOLITE ZSM-5 (600) 112 APPENDIX A.4 - ADSORPTION OF
MTBE ON ZSM-5 (600) - ELBE RIVER WATER 114
|
| adam_txt |
DISSERTATION IMPROVEMENTS OF CHARACTERIZATION OF SINGLE AND MULTISOLUTE
ADSORPTION OF METHYL TERF-BUTYL ETHER (MTBE) ON ZEOLITES CATALIN STEFAN
HERAUSGEBER PROF. DR.-ING. HABIL. DR. H. C. B. BILITEWSKI PROF. DR. RER.
NAT. P. WERNER BEITRAGE ZU ABFALLWIRTSCHAFT/ALTLASTEN SCHRIFTENREIHE DES
INSTITUTES FUR ABFALLWIRTSCHAFT UND ALTLASTEN TECHNISCHE UNIVERSITAT
DRESDEN BAND 55 ISBN 978-3-934253-47-6 2008 1. AUFLAGE TABLE OF CONTENTS
TABLE OF CONTENTS 1. INTRODUCTION 1 1.1 SHORT INTRODUCTION 1 1.2
OBJECTIVES 1 1.2.1 OVERALL OBJECTIVE 1 1.2.2 SPECIFIC OBJECTIVES 2 2.
ABOUT MTBE 3 2.1 GENERAL FACTS 3 2.2 PRODUCTION AND DEMAND RATES 3 2.3
OCCURRENCE OF MTBE IN GERMANY 6 2.3.1 OCCURRENCE OF MTBE IN GROUNDWATER
: 7 2.3.2 MTBE IN RIVER AND WASTE WATER 7 2.3.3 MTBE IN DRINKING WATER 7
2.3.4. MTBE IN URBAN AND RURAL PRECIPITATIONS 8 2.4 SOURCES OF
CONTAMINATION WITH MTBE 8 2.4.1 POINT SOURCES 8 2.4.2 NON-POINT SOURCES
8 2.5 TRANSPORT 9 2.6 PHYSICAL - CHEMICAL PROPERTIES 9 2.6.1 CRITICAL
PROPERTIES-INFLUENCING THE BEHAVIOR OF MTBE 10 2.7 TOXICITY AND IMPACT
ON HUMAN HEALTH 11 2.8 MTBE REGULATIONS 11 2.8.1 IN THE US 11 2.8.2 IN
EUROPE , 12 3. EVALUATION OF ACTUAL MTBE TREATMENT TECHNOLOGIES 13 3.1
BIODEGRADATION 13 3.2. AIR STRIPPING 14 3.3 ADVANCED OXIDATION 14 3.4
HOLLOW FIBER MEMBRANES (HFM) 14 3.5 PERVAPORATION 15 3.6
PHYTOREMEDIATION 15 3.7 SORPTION PROCESSES 15 3.8 CONCLUSIONS 16 4.
ZEOLITES 17 4.1 HISTORY 17 4.2 USES 17 4.3 COMPOSITION 17 4.4 ZEOLITE
ZSM-5 19 5. THEORY OF SORPTION 21 5.1 SORPTION MECHANISMS 21 5.1.1
PARTITIONING 21 5.1.2 MONOLAYER, MULTILAYER AND PORE-FILLING 22 5.1.3
ADSORPTION ISOTHERMS 23 5.2 FITTING DATA WITH DIFFERENT MODELS 24 5.2.1
DATA PREPARATION 25 5.2.2 CHOOSING THE ADSORPTION MODEL 27 5.2.2.1
LINEAR ISOTHERM - ONE FITTING PARAMETER 27 - I - TABLE OF CONTENTS
5.2.2.2 NON-LINEAR ISOTHERMS - TWO FITTING PARAMETERS 28 5.2.2.3
NON-LINEAR ISOTHERMS - THREE FITTING PARAMETERS 30 5.2.2.4 NON-LINEAR
ISOTHERMS - FOUR FITTING PARAMETERS 32 5.2.2.5 OTHER ISOTHERMS 32 5.2.3
GOODNESS-OF-FIT 33 5.3 CONCLUSION 35 5.4 DEVELOPMENT OF ADSORPTION
SOFTWARE 36 6. MATERIALS AND METHODS 37 6.1 ADSORBENTS 37 6.1.1 ZEOLITES
37 6.1.2 ACTIVATED CARBON 37 6.2 ADSORBATES 38 6.2.1 MTBE 38 6.2.2 BTEX
38 6.3 METHODS 38 6.3.1 BATCH TESTS PREPARATION 38 6.3.2 ANALYTICS 38 7.
RESULTS AND DISCUSSION 39 7.1 SCREENING BETWEEN DIFFERENT ADSORBENTS 39
7.2 ADSORPTION KINETIC 41 7.3 CHARACTERIZATION OF ZEOLITES 42 7.3.1
SCANNING ELECTRON MICROSCOPY (SEM) 42 7.3.2 BET ANALYSIS DATA 43 7.3.3
PARTICLE SIZE CALCULATION 44 7.4 ADSORPTION OF MTBE AND BTEX ON ZEOLITE
ZSM-5 (600) 45 7.4.1 LINEAR ADSORPTION 45 7.4.2 FREUNDLICH ADSORPTION
ISOTHERMS .'. 46 7.4.3 SOLUBILITY NORMALIZED FREUNDLICH ISOTHERMS 47
7.4.4 LANGMUIR ADSORPTION ISOTHERMS 48 7.4.5 T6TH ADSORPTION ISOTHERMS
50 7.4.6 DUBININ-POLANYI ISOTHERMS (SOLUBILITY NORMALIZED) 52 7.4.7
LANGMUIR - FREUNDLICH ADSORPTION ISOTHERMS 53 7.4.8 GENERALIZED LANGMUIR
ADSORPTION ISOTHERM 55 7.4.9 MTBE SORPTION MECHANISM 55 7.4.10
ADSORPTION CAPACITIES FOR MTBE AND BTEX 56 7.4.11 GOODNESS OF FIT 58
7.4.12 EFFECT OF NORMALIZATION 60 7.4.13 OPTIMISATION OF NON-LINEAR
REGRESSION BY ERROR ANALYSIS 62 7.5 EFFECT OF COMPETITIVE SORPTION
(INFLUENCE OF BTEX) 66 7.6 IMPACT OF NATURAL ORGANIC MATTER (NOM) 69 8.
PRACTICAL IMPLICATIONS 71 8.1 ADSORBENT REGENERATION 71 8.2 ADSORBENT
USAGE RATES 73 8.3 PACKED BED LIFE 74 8.4 COSTS EVALUATION 76 9.
COMPARISON OF OWN RESULTS WITH REFERENCES 78 9.1 DATA INTERPRETATION 78
9.2 REMOVAL OF MTBE BY ADSORPTION ON ZEOLITES AND RESINS 78 9.3 REMOVAL
OF MTBE BY ADSORPTION ON ACTIVATED CARBON 82 -II - TABLE OF CONTENTS 9.4
EFFECT OF CO-CONTAMINATION 83 9.5 SUMMARY 84 10. GENERAL CONCLUSIONS 86
11. PERSPECTIVES (FURTHER WORK) 88 12. REFERENCES 89 APPENDICES 108
APPENDIX A. ADSORPTION EXPERIMENTAL DATA 109 APPENDIX A. 1 - ADSORPTION
OF MTBE ON ZEOLITE ZSM-5 (600) GRANULES 110 APPENDIX A.2 - EFFECT OF
BTEX CO-CONTAMINATION ON MTBE ADSORPTION 111 APPENDIX A.3 - ADSORPTION
OF MTBE AND BTEX ON ZEOLITE ZSM-5 (600) 112 APPENDIX A.4 - ADSORPTION OF
MTBE ON ZSM-5 (600) - ELBE RIVER WATER 114 |
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| classification_tum | UMW 331d UMW 196d |
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| dewey-full | 628.1683 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 628 - Sanitary engineering |
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| dewey-sort | 3628.1683 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Allgemeines Bauingenieurwesen Umwelt |
| discipline_str_mv | Allgemeines Bauingenieurwesen Umwelt |
| edition | 1. Aufl. |
| format | Thesis Book |
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| index_date | 2024-07-02T20:37:02Z |
| indexdate | 2024-07-09T21:14:41Z |
| institution | BVB |
| isbn | 9783934253476 |
| language | English German |
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| series2 | Beiträge zu Abfallwirtschaft, Altlasten |
| spelling | Stefan, Catalin Verfasser aut Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites Catalin Stefan 1. Aufl. Pirna Forum für Abfallwirtschaft und Altlasten 2008 IX, 114 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Beiträge zu Abfallwirtschaft, Altlasten 55 Zugl.: Dresden, Techn. Univ., Diss., 2007 Grundwassersanierung (DE-588)4510696-4 gnd rswk-swf Butylmethylether tertiär- (DE-588)4279820-6 gnd rswk-swf Zeolith ZSM5 (DE-588)4336638-7 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Grundwassersanierung (DE-588)4510696-4 s Butylmethylether tertiär- (DE-588)4279820-6 s Zeolith ZSM5 (DE-588)4336638-7 s DE-604 Beiträge zu Abfallwirtschaft, Altlasten 55 (DE-604)BV035421245 55 HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016458725&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Stefan, Catalin Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites Beiträge zu Abfallwirtschaft, Altlasten Grundwassersanierung (DE-588)4510696-4 gnd Butylmethylether tertiär- (DE-588)4279820-6 gnd Zeolith ZSM5 (DE-588)4336638-7 gnd |
| subject_GND | (DE-588)4510696-4 (DE-588)4279820-6 (DE-588)4336638-7 (DE-588)4113937-9 |
| title | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites |
| title_auth | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites |
| title_exact_search | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites |
| title_exact_search_txtP | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites |
| title_full | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites Catalin Stefan |
| title_fullStr | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites Catalin Stefan |
| title_full_unstemmed | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites Catalin Stefan |
| title_short | Improvements of characterization of single and multisolute adsorption of Methyl tert-Butyl ether (MTBE) on zeolites |
| title_sort | improvements of characterization of single and multisolute adsorption of methyl tert butyl ether mtbe on zeolites |
| topic | Grundwassersanierung (DE-588)4510696-4 gnd Butylmethylether tertiär- (DE-588)4279820-6 gnd Zeolith ZSM5 (DE-588)4336638-7 gnd |
| topic_facet | Grundwassersanierung Butylmethylether tertiär- Zeolith ZSM5 Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016458725&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV035421245 |
| work_keys_str_mv | AT stefancatalin improvementsofcharacterizationofsingleandmultisoluteadsorptionofmethyltertbutylethermtbeonzeolites |