Holdings: Transport phenomena in micro process engineering

Transport phenomena in micro process engineering: with 17 tables

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Bibliographic Details
Main Author:	Kockmann, Norbert (Author)
Format:	Book
Language:	English
Published:	Berlin [u.a.] Springer 2008
Series:	Heat and mass transfer
Subjects:	Chemical engineering Microchemistry Transport theory Mikrosystemtechnik Chemische Verfahrenstechnik Mikroreaktor Transportprozess Chemieanlage
Online Access:	Inhaltsverzeichnis
Item Description:	Literaturverz. S. 339 - 359
Physical Description:	XX, 365 S. Ill., graph. Darst.
ISBN:	9783540746164 3540746161

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245	1	0	\|a Transport phenomena in micro process engineering \|b with 17 tables \|c Norbert Kockmann
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500			\|a Literaturverz. S. 339 - 359
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adam_text	CONTENTS PREFACE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. VII* CONTENTS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. XII* NOMENC1ATURE XIII* 1 MICRO PROCESS ENGINEERING - AN INTERDISCIPLINARY APPROACH. . . . . . . . I* 1.1 INTRODUCTION AND MOTIVATION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1* 1.2 ORIENTATION OF MICRO PROCESS ENGINEERING . . . . . . . . . . . . . . . . . . . . . . 2* 1.3 THE RO1E OF TRANSPORT PROCESSES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3* 1.4 MAIN ISSUES OF SUCCESSFU1 MICROSTRUCTURES. . . . . . . . . . . . . . . . . . . . . . 9* 1.4.1 WALL HEAT CONDUCTIVITY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10* 1.4.2 PRESSURE 10SS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10* 1.4.3 CORROSION, FOULING, AND CATA1YST DEACTIVATION. . . . . . . . . . . . . . 12* 1.5 SCALING DIMENSIONS AND ISSUES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13* 1.5.1 MATERIAL PROPERTIES 13* 1.5.2 PROCESSES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16* 1.5.3 DEVICES............................................ 25* 1.6 ACTUA1 APP1ICATIONS AND ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . .. 30* 1.6.1 EUROPEAN ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 30* 1.6.2 ACTIVITIES IN THE US 33* 1.6.3 ACTIVITIES IN THE FAR EAST . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 34* 1.7 BARRIERS AND CHALLENGES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 38* 2 FUNDAMENTALS, BALANCES, AND TRANSPORT PROCESSES . . . . . . . . . . . . . . . .. 41* 2.1 INTRODUCTION............................................... 41* 2.2 UNIT OPERATIONS AND PROCESS DESIGN. . . . . . . . . . . . . . . . . . . . . . . . . .. 43* 2.2.1 PROCESS SIMULATION, SCA1E-UP, AND EQUA1-UP . . . . . . . . . . . . . .. 43* 2.2.2 METHOD OF PROCESS, EQUIPMENT, AND PLANT DESIGN 45* 2.2.3 DESIGN PRINCIP1ES FOR PROCESS EQUIPMENT . . . . . . . . . . . . . . . . . 50* 2.3 BALANCES AND TRANSPORT EQUATIONS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52* 2.3.1 STATISTICA1 MECHANICS AND MEAN FREE PATH. . . . . . . . . . . . . . . . . 52* 2.3.2 THE BO1TZMANN EQUATION AND BALANCE EQUATIONS . . . . . . . . . .. 58* X CONTENTS 2.3.3 MACROSCOPIE BALANCE EQUATIONS 61* 2.3.4 ELEMENTARY TRANSPORT PROCESSES AND THEIR DESCRIPTION. . . . . .. 65* 2.3.5 MOLECULAR VELOCITIES AND MACROSCOPIC FLUID PROPERTIES ..... 68* 2.3.6 LIMITS OF LINEAR TRANSPORT PROPERTIES . . . . . . . . . . . . . . . . . . . .. 71* 2.4 MODE1ING, CALCULATION METHODS, AND SIMULATION 73* 2.4.1 PHYSIEAL VARIABLES AND DIMENSIONAL ANALYSIS. . . . . . . . . . . . .. 73* 2.4.2 SIMILARITY LAWS AND SCALING LAWS . . . . . . . . . . . . . . . . . . . . . . .. 74* 2.4.3 ORDER-OF-MAGNITUDE ANALYSIS. . . . . . . . . . . . . . . . . . . . . . . . . .. 75* 2.4.4 LUMPED ELEMENT MODELING . . . . . . . . . . . . . . . . . . . . . . . . . . .. 76* 2.4.5 NUMERICAL SIMULATION AND ANALYTICAL MODELING . . . . . . . . . . .. 77* 2.5 FUTURE DIRECTIONS OF MICRO PROCESS ENGINEERING RESEARCH 78* 3 MOMENTUM TRANSFER 81* 3.1 MOMENTUM TRANSPORT OF SINGLE-PHASE FLOW 81* 3.1.1 THE MOMENTUM EQUATION AND FORCE BALANCE. . . . . . .. .. 81* 3.1.2 THE ENERGY EQUATION FOR FLUID DYNAMICS . . . . . . . . . . . . . . . . .. 83* 3.1.3 BASIC EQUATIONS FOR LONG, SMALL CHANNELS . . . . . . . . . . . . . . . .. 85* 3.1.4 COMPRESSIBLE FLOW 89* 3.1.5 VISCOUS HEATING AND ENTROPY GENERATION IN CHANNEL FLOW . . .. 92* 3.1.6 FLUID DYNAMIC ENTRANCE LENGTH . . . . . . . . . . . . . . . . . . . . . . . .. 96* 3.2 CONVECTIVE FLUID DYNAMICS IN MICROCHANNELS . . . . . . . . . . . . . . . . . .. 97* 3.2.1 DEAN FLOW IN 90 CURVES. . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 98* 3.2.2 FLUID FORCES IN BENDS 100* 3.2.3 FLUID DYNAMIES IN T-JUNCTIONS WITH SYMMETRIE INLET CONDITIONS 102* 3.2.4 FLOW REGIMES IN T-SHAPED MICROMIXERS 107* 3.3 MULTIPHASE FLOW .. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 119* 3.3.1 GAS-LIQUID FLOW PATTERNS 120* 3.3.2 1 VO-PHASE PRESSURE LOSS 122* 3.3.3 CONTACTING AND PHASE SEPARATION. . . . . . . . . . . . . . . . . . . . . . .. 123* 3.3.4 IMMISCIBLE LIQUIDS 125* 4 HEAT TRANSFER AND MICRO HEAT EXCHANGERS . . . . . . . . . . . . . . . . . . . . . . .. 129* 4.1 HEAT TRANSFER FUNDAMENTALS 129* 4.1.1 THE ENERGY BALANCE 129* 4.1.2 HEAT CONDUCTION IN SMALL SYSTEMS 131* 4.1.3 CONVECTIVE HEAT TRANSFER IN MICROCHANNE1S 134* 4.1.4 RAREFIED GASES WITH SLIP BOUNDARY CONDITIONS . . . . . . . . . . . .. 136* 4.1.5 CONVECTIVE COOLING FOR FLOW MEASUREMENT . . . . . . . . . . . . . . .. 139* 4.2 MICROFLUIDIC NETWORKS FOR HEAT EXCHANGE 143* 4.2.1 STATUS-QUO OFMIEROFLUIDIC NETWORKS FOR DEVICE COOLING 144* 4.2.2 SINGLE CHANNEL ELEMENT CALCULATION 145* 4.2.3 COMBINED CHANNEL ELEMENTS 148* 4.2.4 HEAT EXCHANGER CHANNE1 NETWORK 150* 4.3 MICRO HEAT EXCHANGER DEVICES 152* 4.3.1 NUMBER-OF-THERMAL-UNITS (NTU) CONCEPT 154* CONTENTS XI* 4.3.2 DESIGN ISSUES FOR EXCHANGE EQUIPMENT 156* 4.3.3 FOULING AND BLOCKING OF EQUIPMENT 159* 4.3.4 PARTIC1E DEPOSITION IN MICROCHANNELS . . . . . . . . . . . . . . . . . . .. 161* 5 DIFFUSION, MIXING, AND MASS TRANSFER EQUIPMENT 163* 5.1 MIXING PROCESSES AND THEIR CHARACTERIZATION 163* 5.1.1 MIXING PRINCIPLES AND DESCRIPTION 164* 5.1.2 MIXING CHARACTERIZATION 166* 5.1.3 POTENTIAL OF DIFFUSIVE MIXING 168* 5.1.4 STOICHIOMETRIC MIXING AND DIFFUSION PROCESS 169* 5.2 DIFFUSIVE MASS TRANSPORT AND CONCENTRATION DISTRIBUTION IN FLUIDS . 172* 5.3 CONVECTIVE MASS TRANSPORT 174* 5.3.1 ANALOGY BETWEEN HEAT AND MASS TRANSFER 174* 5.3.2 MIXING TIME SCALES AND CHEMICAL REACTIONS . . . . . . . . . . . . . .. 175* 5.4 CHARACTERISTICS OF CONVECTIVE MICROMIXERS 182* 5.4.1 MIXING BEHAVIOR IN 90 0 BENDS 183* 5.4.2 MIXING BEHAVIOR OFT-SHAPED MICROMIXERS 185* 5.4.3 T-SHAPED MICROMIXERS AND COMBINATIONS 190* 5.4.4 MIXING TIMES OF CONVECTIVE MICROMIXERS . . . . . . . . . . . . . . . .. 193* 5.4.5 ENERGY DISSIPATION INTO MIXING 196* 5.4.6 MIXING EFFECTIVENESS 198* 5.4.7 SUMMARY OF CONVECTIVE MICROMIXERS 202* 5.5 MIXING AND CHAOTIC ADVECTION 203* 5.5.1 CONCEPT OF CHAOTIC ADVECTION 203* 5.5.2 GEOMETRY AND FTOW REGIMES 205* 5.5.3 FLUID LARNELLAE AND CHEMICAL REACTIONS . . . . . . . . . . . . . . . . . .. 207* 5.6 DESIGN AND FABRICATION OF SILICON MICROMIXERS. . . . . . . . . . . . . . . . .. 209* 5.6.1 MICROSTRUCTURED MIXERS FOR LIQUID PHASE PRECIPITATION 211* 5.6.2 MICROSTRUCTURED MIXERS FOR AEROSOL GENERATION 212* 5.6.3 MICROSTRUCTURED MIXERS WITH TWO WAFERS 214* 5.7 HIGH THROUGHPUT MIXING DEVICES WITH MICROCHANNELS 215* 5.7.1 NUMERICAL SIMULATION OFMIXING ELEMENTS 218* 5.7.2 EXPERIMENTAL RESULTS AND DISCUSSION 220* 5.7.3 PERFORMANCE INVESTIGATION . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 223* 5.7.4 INJECTION MICROMIXERS 224* 6 CHEMICAL REACTIONS AND REACTIVE PRECIPITATION . . . . . . . . . . . . . . . . . . .. 225* 6.1 CHEMICAL REACTOR ENGINEERING 225* 6.1.1 HEAT AND MASS TRANSFER WITH CHEMICAL REACTIONS . . . . . . . . . .. 228* 6.1.2 CHARACTERISTICS OF CONTINUOUS FTOW REACTORS . . . . . . . . . . . . . .. 229* 6.1.3 TEMPERATURE CONTROL IN MICROCHANNEL REACTORS 233* 6.2 WALL MASS TRANSFER AND SURFACE REACTIONS IN MICROFTUIDIC SYSTEMS 236* 6.2.1 CONTINUUM TRANSPORT MODEL. 237* 6.2.2 PHYSICAL MEANING OF DIMENSIONLESS PARAMETERS 240* 6.2.3 GRAETZ PROBLEM AND WALL MASS TRANSFER 240* XII CONTENTS 6.2.4 WALL MASS TRANSFER IN RNICROCHANNEL REACTORS . . . . . . . . . . . . .. 242* 6.2.5 WALL ADSORPTION AND SATURATION TIME SCALES 244* 6.3 DESIGN CRITERIA FOR MICROCHANNEL REACTORS 248* 6.3.1 EQUIPMENT DESIGN PROCESS . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 248* 6.3.2 REACTION KINETICS AND TRANSPORT PROCESSES 251* 6.3.3 HETEROGENEOUS CATALYTIC REACTIONS IN RNICROCHANNEL REACTORS. 253* 6.3.4 SCALE-UP AND ECONORNIC SITUATION 255* 6.3.5 SCALE-UP METHOD WITH EQUAL-UP PRINCIPLE 258* 6.3.6 IODIDE-IODATE REACTION FOR SELECTIVITY ENGINEERING 261* 6.3.7 COMPETITIVE-CONSECUTIVE REACTIONS 264* 6.4 MICROREACTORS FOR AEROSOL GENERATION 267* 6.4.1 NANOPARTICLE GENERATION 267* 6.4.2 ASYRNRNETRICAL RNIXING IN RNICROCHANNELS 268* 6.4.3 EXPERIMENTAL CHARACTERIZATION OF RNIXING REGIMES , 272* 6.4.4 AEROSOL GENERATION BY HOMOGENEOUS CONDENSATION . . . . . . .. 272* 6.5 MIXING AND DEFINED PRECIPITATION IN LIQUID PHASE 275* 6.5.1 MODELING AND SIMULATION OF PARTICLE PRECIPITATION 277* 6.5.2 THE POPULATION BALANCE EQUATION 278* 6.5.3 PRECIPITATION IN THE INTERDIFFUSION ZONE 280* 6.5.4 BINARY COMPOUND PRECIPITATION IN CONVECTIVE RNICRORNIXERS .. 282* 6.5.5 EXPERIMENTAL INVESTIGATIONS OF BARIUM SULFATE PRECIPITATION . 286* 6.5.6 EXPERIMENTAL INVESTIGATION OF PIGMENT SYNTHESIS 290* 7 COUPLED TRANSPORT PROCESSES 293* 7.1 THERMODYNARNICS OFIRREVERSIBLE PROCESSES 294* 7.2 THERMOELECTRIC ENERGY CONVERSION 297* 7.2.1 MICROSCALE THERMOELECTRIC ENERGY CONVERSION . . . . . . . . . . . .. 299* 7.2.2 DESIGN AND FABRICATION OF THE GENERATOR. . . . . . . . . . . . . . . . .. 301* 7.2.3 EXPERIMENTAL CHARACTERIZATION AND DISCUSSION 306* 7.2.4 THERMOCOUPLES AND RNICROFLUIDIC CHIPS 308* 7.3 ELECTRO-OSMOTIC AND ELECTRO-KINETIC EFFECTS . . . . . . . . . . . . . . . . . . . .. 311* 7.4 THERMODIFFUSION 312* 7.4.1 DESIGN AND FABRICATION OF THERMODIFFUSION DEVICES. . . . . . . .. 312* 7.4.2 EXPERIMENTAL INVESTIGATIONS WITH THERMODIFFUSION CHIPS 315* 7.4.3 IMPROVEMEM OF THERMODIFFUSION DEVICES 317* 7.4.4 KNUDSEN PUMP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 318* 7.5 PRESSURE DIFFUSION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 319* 8 CONCLUSION AND FINAL REMARKS 321* A COLOR FIGURES 323* REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 339* INDEX 361*
adam_txt	CONTENTS PREFACE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . VII* CONTENTS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . XII* NOMENC1ATURE XIII* 1 MICRO PROCESS ENGINEERING - AN INTERDISCIPLINARY APPROACH. . . . . . . . I* 1.1 INTRODUCTION AND MOTIVATION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1* 1.2 ORIENTATION OF MICRO PROCESS ENGINEERING . . . . . . . . . . . . . . . . . . . . . . 2* 1.3 THE RO1E OF TRANSPORT PROCESSES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3* 1.4 MAIN ISSUES OF SUCCESSFU1 MICROSTRUCTURES. . . . . . . . . . . . . . . . . . . . . . 9* 1.4.1 WALL HEAT CONDUCTIVITY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10* 1.4.2 PRESSURE 10SS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10* 1.4.3 CORROSION, FOULING, AND CATA1YST DEACTIVATION. . . . . . . . . . . . . . 12* 1.5 SCALING DIMENSIONS AND ISSUES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13* 1.5.1 MATERIAL PROPERTIES 13* 1.5.2 PROCESSES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16* 1.5.3 DEVICES. 25* 1.6 ACTUA1 APP1ICATIONS AND ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . . 30* 1.6.1 EUROPEAN ACTIVITIES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30* 1.6.2 ACTIVITIES IN THE US 33* 1.6.3 ACTIVITIES IN THE FAR EAST . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34* 1.7 BARRIERS AND CHALLENGES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38* 2 FUNDAMENTALS, BALANCES, AND TRANSPORT PROCESSES . . . . . . . . . . . . . . . . 41* 2.1 INTRODUCTION. 41* 2.2 UNIT OPERATIONS AND PROCESS DESIGN. . . . . . . . . . . . . . . . . . . . . . . . . . 43* 2.2.1 PROCESS SIMULATION, SCA1E-UP, AND EQUA1-UP . . . . . . . . . . . . . . 43* 2.2.2 METHOD OF PROCESS, EQUIPMENT, AND PLANT DESIGN 45* 2.2.3 DESIGN PRINCIP1ES FOR PROCESS EQUIPMENT . . . . . . . . . . . . . . . . . 50* 2.3 BALANCES AND TRANSPORT EQUATIONS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52* 2.3.1 STATISTICA1 MECHANICS AND MEAN FREE PATH. . . . . . . . . . . . . . . . . 52* 2.3.2 THE BO1TZMANN EQUATION AND BALANCE EQUATIONS . . . . . . . . . . 58* X CONTENTS 2.3.3 MACROSCOPIE BALANCE EQUATIONS 61* 2.3.4 ELEMENTARY TRANSPORT PROCESSES AND THEIR DESCRIPTION. . . . . . 65* 2.3.5 MOLECULAR VELOCITIES AND MACROSCOPIC FLUID PROPERTIES . 68* 2.3.6 LIMITS OF LINEAR TRANSPORT PROPERTIES . . . . . . . . . . . . . . . . . . . . 71* 2.4 MODE1ING, CALCULATION METHODS, AND SIMULATION " 73* 2.4.1 PHYSIEAL VARIABLES AND DIMENSIONAL ANALYSIS. . . . . . . . . . . . . 73* 2.4.2 SIMILARITY LAWS AND SCALING LAWS . . . . . . . . . . . . . . . . . . . . . . . 74* 2.4.3 ORDER-OF-MAGNITUDE ANALYSIS. . . . . . . . . . . . . . . . . . . . . . . . . . 75* 2.4.4 LUMPED ELEMENT MODELING . . . . . . . . . . . . . . . . . . . . . . . . . . . 76* 2.4.5 NUMERICAL SIMULATION AND ANALYTICAL MODELING . . . . . . . . . . . 77* 2.5 FUTURE DIRECTIONS OF MICRO PROCESS ENGINEERING RESEARCH 78* 3 MOMENTUM TRANSFER 81* 3.1 MOMENTUM TRANSPORT OF SINGLE-PHASE FLOW 81* 3.1.1 THE MOMENTUM EQUATION AND FORCE BALANCE. . . . . . . . 81* 3.1.2 THE ENERGY EQUATION FOR FLUID DYNAMICS . . . . . . . . . . . . . . . . . 83* 3.1.3 BASIC EQUATIONS FOR LONG, SMALL CHANNELS . . . . . . . . . . . . . . . . 85* 3.1.4 COMPRESSIBLE FLOW 89* 3.1.5 VISCOUS HEATING AND ENTROPY GENERATION IN CHANNEL FLOW . . . 92* 3.1.6 FLUID DYNAMIC ENTRANCE LENGTH . . . . . . . . . . . . . . . . . . . . . . . . 96* 3.2 CONVECTIVE FLUID DYNAMICS IN MICROCHANNELS . . . . . . . . . . . . . . . . . . 97* 3.2.1 DEAN FLOW IN 90 CURVES. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98* 3.2.2 FLUID FORCES IN BENDS 100* 3.2.3 FLUID DYNAMIES IN T-JUNCTIONS WITH SYMMETRIE INLET CONDITIONS 102* 3.2.4 FLOW REGIMES IN T-SHAPED MICROMIXERS 107* 3.3 MULTIPHASE FLOW . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 119* 3.3.1 GAS-LIQUID FLOW PATTERNS 120* 3.3.2 1\VO-PHASE PRESSURE LOSS 122* 3.3.3 CONTACTING AND PHASE SEPARATION. . . . . . . . . . . . . . . . . . . . . . . 123* 3.3.4 IMMISCIBLE LIQUIDS 125* 4 HEAT TRANSFER AND MICRO HEAT EXCHANGERS . . . . . . . . . . . . . . . . . . . . . . . 129* 4.1 HEAT TRANSFER FUNDAMENTALS 129* 4.1.1 THE ENERGY BALANCE 129* 4.1.2 HEAT CONDUCTION IN SMALL SYSTEMS 131* 4.1.3 CONVECTIVE HEAT TRANSFER IN MICROCHANNE1S 134* 4.1.4 RAREFIED GASES WITH SLIP BOUNDARY CONDITIONS . . . . . . . . . . . . 136* 4.1.5 CONVECTIVE COOLING FOR FLOW MEASUREMENT . . . . . . . . . . . . . . . 139* 4.2 MICROFLUIDIC NETWORKS FOR HEAT EXCHANGE 143* 4.2.1 STATUS-QUO OFMIEROFLUIDIC NETWORKS FOR DEVICE COOLING 144* 4.2.2 SINGLE CHANNEL ELEMENT CALCULATION 145* 4.2.3 COMBINED CHANNEL ELEMENTS 148* 4.2.4 HEAT EXCHANGER CHANNE1 NETWORK 150* 4.3 MICRO HEAT EXCHANGER DEVICES " 152* 4.3.1 NUMBER-OF-THERMAL-UNITS (NTU) CONCEPT 154* CONTENTS XI* 4.3.2 DESIGN ISSUES FOR EXCHANGE EQUIPMENT 156* 4.3.3 FOULING AND BLOCKING OF EQUIPMENT 159* 4.3.4 PARTIC1E DEPOSITION IN MICROCHANNELS . . . . . . . . . . . . . . . . . . . 161* 5 DIFFUSION, MIXING, AND MASS TRANSFER EQUIPMENT 163* 5.1 MIXING PROCESSES AND THEIR CHARACTERIZATION 163* 5.1.1 MIXING PRINCIPLES AND DESCRIPTION 164* 5.1.2 MIXING CHARACTERIZATION 166* 5.1.3 POTENTIAL OF DIFFUSIVE MIXING 168* 5.1.4 STOICHIOMETRIC MIXING AND DIFFUSION PROCESS 169* 5.2 DIFFUSIVE MASS TRANSPORT AND CONCENTRATION DISTRIBUTION IN FLUIDS . 172* 5.3 CONVECTIVE MASS TRANSPORT 174* 5.3.1 ANALOGY BETWEEN HEAT AND MASS TRANSFER 174* 5.3.2 MIXING TIME SCALES AND CHEMICAL REACTIONS . . . . . . . . . . . . . . 175* 5.4 CHARACTERISTICS OF CONVECTIVE MICROMIXERS 182* 5.4.1 MIXING BEHAVIOR IN 90 0 BENDS 183* 5.4.2 MIXING BEHAVIOR OFT-SHAPED MICROMIXERS 185* 5.4.3 T-SHAPED MICROMIXERS AND COMBINATIONS 190* 5.4.4 MIXING TIMES OF CONVECTIVE MICROMIXERS . . . . . . . . . . . . . . . . 193* 5.4.5 ENERGY DISSIPATION INTO MIXING 196* 5.4.6 MIXING EFFECTIVENESS 198* 5.4.7 SUMMARY OF CONVECTIVE MICROMIXERS 202* 5.5 MIXING AND CHAOTIC ADVECTION 203* 5.5.1 CONCEPT OF CHAOTIC ADVECTION 203* 5.5.2 GEOMETRY AND FTOW REGIMES 205* 5.5.3 FLUID LARNELLAE AND CHEMICAL REACTIONS . . . . . . . . . . . . . . . . . . 207* 5.6 DESIGN AND FABRICATION OF SILICON MICROMIXERS. . . . . . . . . . . . . . . . . 209* 5.6.1 MICROSTRUCTURED MIXERS FOR LIQUID PHASE PRECIPITATION 211* 5.6.2 MICROSTRUCTURED MIXERS FOR AEROSOL GENERATION 212* 5.6.3 MICROSTRUCTURED MIXERS WITH TWO WAFERS 214* 5.7 HIGH THROUGHPUT MIXING DEVICES WITH MICROCHANNELS 215* 5.7.1 NUMERICAL SIMULATION OFMIXING ELEMENTS 218* 5.7.2 EXPERIMENTAL RESULTS AND DISCUSSION 220* 5.7.3 PERFORMANCE INVESTIGATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . 223* 5.7.4 INJECTION MICROMIXERS 224* 6 CHEMICAL REACTIONS AND REACTIVE PRECIPITATION . . . . . . . . . . . . . . . . . . . 225* 6.1 CHEMICAL REACTOR ENGINEERING 225* 6.1.1 HEAT AND MASS TRANSFER WITH CHEMICAL REACTIONS . . . . . . . . . . 228* 6.1.2 CHARACTERISTICS OF CONTINUOUS FTOW REACTORS . . . . . . . . . . . . . . 229* 6.1.3 TEMPERATURE CONTROL IN MICROCHANNEL REACTORS 233* 6.2 WALL MASS TRANSFER AND SURFACE REACTIONS IN MICROFTUIDIC SYSTEMS 236* 6.2.1 CONTINUUM TRANSPORT MODEL. 237* 6.2.2 PHYSICAL MEANING OF DIMENSIONLESS PARAMETERS 240* 6.2.3 GRAETZ PROBLEM AND WALL MASS TRANSFER 240* XII CONTENTS 6.2.4 WALL MASS TRANSFER IN RNICROCHANNEL REACTORS . . . . . . . . . . . . . 242* 6.2.5 WALL ADSORPTION AND SATURATION TIME SCALES 244* 6.3 DESIGN CRITERIA FOR MICROCHANNEL REACTORS 248* 6.3.1 EQUIPMENT DESIGN PROCESS . . . . . . . . . . . . . . . . . . . . . . . . . . . . 248* 6.3.2 REACTION KINETICS AND TRANSPORT PROCESSES 251* 6.3.3 HETEROGENEOUS CATALYTIC REACTIONS IN RNICROCHANNEL REACTORS. 253* 6.3.4 SCALE-UP AND ECONORNIC SITUATION 255* 6.3.5 SCALE-UP METHOD WITH EQUAL-UP PRINCIPLE 258* 6.3.6 IODIDE-IODATE REACTION FOR SELECTIVITY ENGINEERING 261* 6.3.7 COMPETITIVE-CONSECUTIVE REACTIONS 264* 6.4 MICROREACTORS FOR AEROSOL GENERATION 267* 6.4.1 NANOPARTICLE GENERATION 267* 6.4.2 ASYRNRNETRICAL RNIXING IN RNICROCHANNELS 268* 6.4.3 EXPERIMENTAL CHARACTERIZATION OF RNIXING REGIMES , 272* 6.4.4 AEROSOL GENERATION BY HOMOGENEOUS CONDENSATION . . . . . . . 272* 6.5 MIXING AND DEFINED PRECIPITATION IN LIQUID PHASE 275* 6.5.1 MODELING AND SIMULATION OF PARTICLE PRECIPITATION 277* 6.5.2 THE POPULATION BALANCE EQUATION 278* 6.5.3 PRECIPITATION IN THE INTERDIFFUSION ZONE 280* 6.5.4 BINARY COMPOUND PRECIPITATION IN CONVECTIVE RNICRORNIXERS . 282* 6.5.5 EXPERIMENTAL INVESTIGATIONS OF BARIUM SULFATE PRECIPITATION . 286* 6.5.6 EXPERIMENTAL INVESTIGATION OF PIGMENT SYNTHESIS 290* 7 COUPLED TRANSPORT PROCESSES " 293* 7.1 THERMODYNARNICS OFIRREVERSIBLE PROCESSES 294* 7.2 THERMOELECTRIC ENERGY CONVERSION 297* 7.2.1 MICROSCALE THERMOELECTRIC ENERGY CONVERSION . . . . . . . . . . . . 299* 7.2.2 DESIGN AND FABRICATION OF THE GENERATOR. . . . . . . . . . . . . . . . . 301* 7.2.3 EXPERIMENTAL CHARACTERIZATION AND DISCUSSION 306* 7.2.4 THERMOCOUPLES AND RNICROFLUIDIC CHIPS 308* 7.3 ELECTRO-OSMOTIC AND ELECTRO-KINETIC EFFECTS . . . . . . . . . . . . . . . . . . . . 311* 7.4 THERMODIFFUSION 312* 7.4.1 DESIGN AND FABRICATION OF THERMODIFFUSION DEVICES. . . . . . . . 312* 7.4.2 EXPERIMENTAL INVESTIGATIONS WITH THERMODIFFUSION CHIPS 315* 7.4.3 IMPROVEMEM OF THERMODIFFUSION DEVICES 317* 7.4.4 KNUDSEN PUMP . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 318* 7.5 PRESSURE DIFFUSION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 319* 8 CONCLUSION AND FINAL REMARKS 321* A COLOR FIGURES 323* REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 339* INDEX 361*
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author_facet	Kockmann, Norbert
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author_sort	Kockmann, Norbert
author_variant	n k nk
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dewey-tens	660 - Chemical engineering
discipline	Chemie / Pharmazie Elektrotechnik / Elektronik / Nachrichtentechnik
discipline_str_mv	Chemie / Pharmazie Elektrotechnik / Elektronik / Nachrichtentechnik
format	Book
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illustrated	Illustrated
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physical	XX, 365 S. Ill., graph. Darst.
publishDate	2008
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publisher	Springer
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spelling	Kockmann, Norbert Verfasser aut Transport phenomena in micro process engineering with 17 tables Norbert Kockmann Berlin [u.a.] Springer 2008 XX, 365 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Heat and mass transfer Literaturverz. S. 339 - 359 Chemical engineering Microchemistry Transport theory Mikrosystemtechnik (DE-588)4221617-5 gnd rswk-swf Chemische Verfahrenstechnik (DE-588)4069941-9 gnd rswk-swf Mikroreaktor (DE-588)4786310-9 gnd rswk-swf Transportprozess (DE-588)4185932-7 gnd rswk-swf Chemieanlage (DE-588)4121084-0 gnd rswk-swf Chemische Verfahrenstechnik (DE-588)4069941-9 s Mikroreaktor (DE-588)4786310-9 s Transportprozess (DE-588)4185932-7 s DE-604 Chemieanlage (DE-588)4121084-0 s Mikrosystemtechnik (DE-588)4221617-5 s OEBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016451782&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Kockmann, Norbert Transport phenomena in micro process engineering with 17 tables Chemical engineering Microchemistry Transport theory Mikrosystemtechnik (DE-588)4221617-5 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd Mikroreaktor (DE-588)4786310-9 gnd Transportprozess (DE-588)4185932-7 gnd Chemieanlage (DE-588)4121084-0 gnd
subject_GND	(DE-588)4221617-5 (DE-588)4069941-9 (DE-588)4786310-9 (DE-588)4185932-7 (DE-588)4121084-0
title	Transport phenomena in micro process engineering with 17 tables
title_auth	Transport phenomena in micro process engineering with 17 tables
title_exact_search	Transport phenomena in micro process engineering with 17 tables
title_exact_search_txtP	Transport phenomena in micro process engineering with 17 tables
title_full	Transport phenomena in micro process engineering with 17 tables Norbert Kockmann
title_fullStr	Transport phenomena in micro process engineering with 17 tables Norbert Kockmann
title_full_unstemmed	Transport phenomena in micro process engineering with 17 tables Norbert Kockmann
title_short	Transport phenomena in micro process engineering
title_sort	transport phenomena in micro process engineering with 17 tables
title_sub	with 17 tables
topic	Chemical engineering Microchemistry Transport theory Mikrosystemtechnik (DE-588)4221617-5 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd Mikroreaktor (DE-588)4786310-9 gnd Transportprozess (DE-588)4185932-7 gnd Chemieanlage (DE-588)4121084-0 gnd
topic_facet	Chemical engineering Microchemistry Transport theory Mikrosystemtechnik Chemische Verfahrenstechnik Mikroreaktor Transportprozess Chemieanlage
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016451782&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT kockmannnorbert transportphenomenainmicroprocessengineeringwith17tables

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