Stabilization of organic matter in the acid soil environment: importance of mineral phases and involved mechanisms
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Tönning [u.a.]
<<Der>> Andere Verl.
2007
|
| Schriftenreihe: | Hallenser bodenwissenschaftliche Abhandlungen
11 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXI, 183 S. Ill., graph. Darst., Tab. |
| ISBN: | 9783899596045 |
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| 245 | 1 | 0 | |a Stabilization of organic matter in the acid soil environment |b importance of mineral phases and involved mechanisms |c von Robert Mikutta |
| 264 | 1 | |a Tönning [u.a.] |b <<Der>> Andere Verl. |c 2007 | |
| 300 | |a XXI, 183 S. |b Ill., graph. Darst., Tab. | ||
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Datensatz im Suchindex
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| adam_text | TABLE OF CONTENTS
Table of contents I
List of figures V
List of tables XI
List of abbreviations XIV
Summary XV
Kurzfassung XVIII
1. Scientific Background and Research Objectives 1
1.1 Global change and soils 2
1.2 Concepts of organic matter stabilization in soils 3
1.3 Chemical protection 5
1.3.1 Metal-organic complexes 6
1.3.2 Presence of minerals capable for sorbing organic matter 6
1.3.3 Surface reactivity of mineral phases 7
1.3.4 Pore architecture 8
1.3.5 Mechanisms of sorptive interactions 9
1.4 Methodological approaches to assess stable organic matter 12
1.5 Objectives and outline 13
2. Review: Organic Matter Removal from Soils using Hydrogen Peroxide,
Sodium Hypochlorite, and Disodium Peroxodisulfate 16
2.1 Abstract 17
2.2 Introduction 17
2.3 Procedures, reaction conditions and application 18
2.3.1 Hydrogen peroxide 18
2.3.2 Sodium hypochlorite 20
2.3.3 Disodium peroxodisulfate 20
2.4 Reaction of oxidants with inorganic and organic matter 23
2.4.1 Hydrogen peroxide 23
2.4.2 Sodium hypochlorite 25
2.4.3 Disodium peroxodisulfate 25
2.5 Efficiency of organic matter removal 26
2.5.1 Hydrogen peroxide 26
2.5.2 Sodium hypochlorite 27
2.5.3 Disodium peroxodisulfate 27
2.6 Efficiency of organic carbon removal depends on sample properties 28
2.6.1 Composition of organic matter 28
2.6.2 Protection of organic matter by soil minerals 29
2.7 Treatments induce modifications of mineral constituents 31
2.7.1 Thermal effect on minerals
2.7.2 Hydrogen peroxide
2.7.3 Sodium hypochlorite
2.7.4 Disodium peroxodisulfate
2.8 Metal precipitation
2.9 Synthesis
2.10 Implications
31
31
35
37
37
38
39
3. Poorly-crystalline Mineral Phases protect Organic Matter in acid
Subsoil Horizons 42
3.1 Abstract 43
3.2 Introduction 43
3.3 Materials and methods 44
3.4 Results 49
3.4.1 Organic carbon removal 49
3.4.2 Chemical degradation and sample properties 49
3.4.3 Isolation of stable organic carbon 51
3.4.4 Linear regression analysis - untreated samples 51
3.4.5 Linear regression analysis - stable organic carbon 51
3.5 Discussion 55
3.6 Conclusions 57
4. Stabilization of Soil Organic Matter: Association with Minerals
or Chemical Recalcitrance? 57
4.1 Abstract 58
4.2 Introduction 58
4.3 Materials and methods 60
4.4 Results 64
4.4.1 Mineral-protected organic matter 64
4.4.2 Chemically resistant organic matter 70
4.4.3 Radiocarbon content of organic matter pools 70
4.4.4 13C signatures 73
4.4.5 Contribution of lignin to stable organic matter 73
4.4.6 Cross-polarization magic-angle spinning carbon-13 NMR 75
4.5 Discussion 77
4.5.1 Mineral-protected organic matter 77
4.5.2 Chemically resistant organic matter 79
4.6 Conclusions 80
5. Poorly-crystalline Minerals protect Organic Carbon in Clay
Subfractions from acid Subsoil Horizons 82
5.1 Abstract 83
5.2 Introduction 83
5.3 Materials and methods 84
5.4 Results and discussion 87
5.4.1 Initial and stable organic matter 87
5.4.2 Crystallinity of mineral phases 87
5.4.3 Relation between mineral and stable organic matter 89
5.4.4 Mineral surfaces and organic matter 91
5.5 Conclusions 94
6. Stabilization of Organic Matter at Micropores ( 2 nm) in Acid Forest
Subsoils 95
6.1 Abstract . 96
6.2 Introduction 96
6.3 Materials and methods 98
6.4 Results and discussion 100
6.4.1 Micro- and mesoporosity in relation to mineralogical properties 101
6.4.2 Association of stable OM with mineral micro- and small mesopores 102
7. Microbial Mineralization of Forest Floor Organic Matter bound
to Minerals via different Binding Mechanisms 108
7.1 Abstract 109
7.2 Introduction 109
7.3 Materials and methods 111
7.3.1 Minerals and their properties 111
7.3.2 Organic matter 112
7.3.3 SoTption experiments and isotherm modelling 113
7.3.4 Sorptive fractionation of organic matter 116
7.3.5 Organic matter flocculation by Ca2+ 116
7.3.6 Desorption of sorbed organic matter into diluted solutions 116
7.3.7 Biodegradation of sorbed organic matter 117
7.3.8 Statistics 118
7.4 Results and discussion 118
7.4.1 Properties of test minerals and organic matter 118
7.4.2 Sorption of organic matter 121
7.4.2.1 Effect of background electrolytes 121
7.4.2.2 Ca-induced flocculation of organic matter 126
7.4.2.3 Contribution of individual binding mechanisms to the
III
sorption of organic matter 126
7.4.2.4 Organic matter affinity related to the estimated
contribution of binding mechanisms 128
7.4.2.5 Sorptive fractionation of organic matter 128
7.4.3 Stability of sorbed organic matter against desorption 131
7.4.4 Stability of sorbed organic matter against biodegradation 133
7.4.4.1 Microbial mineralization as related to binding mechanisms 133
7.4.4.2 Mineralization of sorbed organic matter as related to
sorption affinity, sorptive fractionation, and sorption reversibility 138
7.4.4.3 Degradation rates of sorbed organic matter 142
7.5 Synthesis 143
7.6 Conclusions 144
8. Synopsis 146
8.1 Methodological aspects in assessment of stable organic matter 147
8.2 Organic matter stabilization in acidic subsoil horizons 147
8.3 Importance of micropores for the stabilization of organic matteT 150
8.4 Impact of binding mechanisms on the stability of sorbed organic matter 151
8.5 Conclusions 153
8.6 Prospective 155
9. References 157
10. Acknowledgments (Danksagung) 182
IV
|
| adam_txt |
TABLE OF CONTENTS
Table of contents I
List of figures V
List of tables XI
List of abbreviations XIV
Summary XV
Kurzfassung XVIII
1. Scientific Background and Research Objectives 1
1.1 Global change and soils 2
1.2 Concepts of organic matter stabilization in soils 3
1.3 Chemical protection 5
1.3.1 Metal-organic complexes 6
1.3.2 Presence of minerals capable for sorbing organic matter 6
1.3.3 Surface reactivity of mineral phases 7
1.3.4 Pore architecture 8
1.3.5 Mechanisms of sorptive interactions 9
1.4 Methodological approaches to assess stable organic matter 12
1.5 Objectives and outline 13
2. Review: Organic Matter Removal from Soils using Hydrogen Peroxide,
Sodium Hypochlorite, and Disodium Peroxodisulfate 16
2.1 Abstract 17
2.2 Introduction 17
2.3 Procedures, reaction conditions and application 18
2.3.1 Hydrogen peroxide 18
2.3.2 Sodium hypochlorite 20
2.3.3 Disodium peroxodisulfate 20
2.4 Reaction of oxidants with inorganic and organic matter 23
2.4.1 Hydrogen peroxide 23
2.4.2 Sodium hypochlorite 25
2.4.3 Disodium peroxodisulfate 25
2.5 Efficiency of organic matter removal 26
2.5.1 Hydrogen peroxide 26
2.5.2 Sodium hypochlorite 27
2.5.3 Disodium peroxodisulfate 27
2.6 Efficiency of organic carbon removal depends on sample properties 28
2.6.1 Composition of organic matter 28
2.6.2 Protection of organic matter by soil minerals 29
2.7 Treatments induce modifications of mineral constituents 31
2.7.1 Thermal effect on minerals
2.7.2 Hydrogen peroxide
2.7.3 Sodium hypochlorite
2.7.4 Disodium peroxodisulfate
2.8 Metal precipitation
2.9 Synthesis
2.10 Implications
31
31
35
37
37
38
39
3. Poorly-crystalline Mineral Phases protect Organic Matter in acid
Subsoil Horizons 42
3.1 Abstract 43
3.2 Introduction 43
3.3 Materials and methods 44
3.4 Results 49
3.4.1 Organic carbon removal 49
3.4.2 Chemical degradation and sample properties 49
3.4.3 Isolation of stable organic carbon 51
3.4.4 Linear regression analysis - untreated samples 51
3.4.5 Linear regression analysis - stable organic carbon 51
3.5 Discussion 55
3.6 Conclusions 57
4. Stabilization of Soil Organic Matter: Association with Minerals
or Chemical Recalcitrance? 57
4.1 Abstract 58
4.2 Introduction 58
4.3 Materials and methods 60
4.4 Results 64
4.4.1 Mineral-protected organic matter 64
4.4.2 Chemically resistant organic matter 70
4.4.3 Radiocarbon content of organic matter pools 70
4.4.4 13C signatures 73
4.4.5 Contribution of lignin to stable organic matter 73
4.4.6 Cross-polarization magic-angle spinning carbon-13 NMR 75
4.5 Discussion 77
4.5.1 Mineral-protected organic matter 77
4.5.2 Chemically resistant organic matter 79
4.6 Conclusions 80
5. Poorly-crystalline Minerals protect Organic Carbon in Clay
Subfractions from acid Subsoil Horizons 82
5.1 Abstract 83
5.2 Introduction 83
5.3 Materials and methods 84
5.4 Results and discussion 87
5.4.1 Initial and stable organic matter 87
5.4.2 Crystallinity of mineral phases 87
5.4.3 Relation between mineral and stable organic matter 89
5.4.4 Mineral surfaces and organic matter 91
5.5 Conclusions 94
6. Stabilization of Organic Matter at Micropores ( 2 nm) in Acid Forest
Subsoils 95
6.1 Abstract . 96
6.2 Introduction 96
6.3 Materials and methods 98
6.4 Results and discussion 100
6.4.1 Micro- and mesoporosity in relation to mineralogical properties 101
6.4.2 Association of stable OM with mineral micro- and small mesopores 102
7. Microbial Mineralization of Forest Floor Organic Matter bound
to Minerals via different Binding Mechanisms 108
7.1 Abstract 109
7.2 Introduction 109
7.3 Materials and methods 111
7.3.1 Minerals and their properties 111
7.3.2 Organic matter 112
7.3.3 SoTption experiments and isotherm modelling 113
7.3.4 Sorptive fractionation of organic matter 116
7.3.5 Organic matter flocculation by Ca2+ 116
7.3.6 Desorption of sorbed organic matter into diluted solutions 116
7.3.7 Biodegradation of sorbed organic matter 117
7.3.8 Statistics 118
7.4 Results and discussion 118
7.4.1 Properties of test minerals and organic matter 118
7.4.2 Sorption of organic matter 121
7.4.2.1 Effect of background electrolytes 121
7.4.2.2 Ca-induced flocculation of organic matter 126
7.4.2.3 Contribution of individual binding mechanisms to the
III
sorption of organic matter 126
7.4.2.4 Organic matter affinity related to the estimated
contribution of binding mechanisms 128
7.4.2.5 Sorptive fractionation of organic matter 128
7.4.3 Stability of sorbed organic matter against desorption 131
7.4.4 Stability of sorbed organic matter against biodegradation 133
7.4.4.1 Microbial mineralization as related to binding mechanisms 133
7.4.4.2 Mineralization of sorbed organic matter as related to
sorption affinity, sorptive fractionation, and sorption reversibility 138
7.4.4.3 Degradation rates of sorbed organic matter 142
7.5 Synthesis 143
7.6 Conclusions 144
8. Synopsis 146
8.1 Methodological aspects in assessment of stable organic matter 147
8.2 Organic matter stabilization in acidic subsoil horizons 147
8.3 Importance of micropores for the stabilization of organic matteT 150
8.4 Impact of binding mechanisms on the stability of sorbed organic matter 151
8.5 Conclusions 153
8.6 Prospective 155
9. References 157
10. Acknowledgments (Danksagung) 182
IV |
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| discipline | Geowissenschaften Geologie / Paläontologie Agrar-/Forst-/Ernährungs-/Haushaltswissenschaft / Gartenbau |
| discipline_str_mv | Geowissenschaften Geologie / Paläontologie Agrar-/Forst-/Ernährungs-/Haushaltswissenschaft / Gartenbau |
| format | Thesis Book |
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| index_date | 2024-07-02T20:29:57Z |
| indexdate | 2024-07-09T21:14:16Z |
| institution | BVB |
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| language | English |
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| series | Hallenser bodenwissenschaftliche Abhandlungen |
| series2 | Hallenser bodenwissenschaftliche Abhandlungen |
| spelling | Mikutta, Robert Verfasser aut Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms von Robert Mikutta Tönning [u.a.] <<Der>> Andere Verl. 2007 XXI, 183 S. Ill., graph. Darst., Tab. txt rdacontent n rdamedia nc rdacarrier Hallenser bodenwissenschaftliche Abhandlungen 11 Zugl.: Halle (Saale), Univ., Diss., 2007 Boden (DE-588)4007348-8 gnd rswk-swf Organischer Stoff (DE-588)4203832-7 gnd rswk-swf Humus (DE-588)4160800-8 gnd rswk-swf Kohlenstoffkreislauf (DE-588)4164552-2 gnd rswk-swf Paragenese (DE-588)4173268-6 gnd rswk-swf Physikochemische Bodeneigenschaft (DE-588)4311151-8 gnd rswk-swf Saurer Boden (DE-588)4051834-6 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Boden (DE-588)4007348-8 s Organischer Stoff (DE-588)4203832-7 s Kohlenstoffkreislauf (DE-588)4164552-2 s Physikochemische Bodeneigenschaft (DE-588)4311151-8 s DE-604 Saurer Boden (DE-588)4051834-6 s Humus (DE-588)4160800-8 s Paragenese (DE-588)4173268-6 s b DE-604 Hallenser bodenwissenschaftliche Abhandlungen 11 (DE-604)BV035419895 11 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016441507&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Mikutta, Robert Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms Hallenser bodenwissenschaftliche Abhandlungen Boden (DE-588)4007348-8 gnd Organischer Stoff (DE-588)4203832-7 gnd Humus (DE-588)4160800-8 gnd Kohlenstoffkreislauf (DE-588)4164552-2 gnd Paragenese (DE-588)4173268-6 gnd Physikochemische Bodeneigenschaft (DE-588)4311151-8 gnd Saurer Boden (DE-588)4051834-6 gnd |
| subject_GND | (DE-588)4007348-8 (DE-588)4203832-7 (DE-588)4160800-8 (DE-588)4164552-2 (DE-588)4173268-6 (DE-588)4311151-8 (DE-588)4051834-6 (DE-588)4113937-9 |
| title | Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms |
| title_auth | Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms |
| title_exact_search | Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms |
| title_exact_search_txtP | Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms |
| title_full | Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms von Robert Mikutta |
| title_fullStr | Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms von Robert Mikutta |
| title_full_unstemmed | Stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms von Robert Mikutta |
| title_short | Stabilization of organic matter in the acid soil environment |
| title_sort | stabilization of organic matter in the acid soil environment importance of mineral phases and involved mechanisms |
| title_sub | importance of mineral phases and involved mechanisms |
| topic | Boden (DE-588)4007348-8 gnd Organischer Stoff (DE-588)4203832-7 gnd Humus (DE-588)4160800-8 gnd Kohlenstoffkreislauf (DE-588)4164552-2 gnd Paragenese (DE-588)4173268-6 gnd Physikochemische Bodeneigenschaft (DE-588)4311151-8 gnd Saurer Boden (DE-588)4051834-6 gnd |
| topic_facet | Boden Organischer Stoff Humus Kohlenstoffkreislauf Paragenese Physikochemische Bodeneigenschaft Saurer Boden Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016441507&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV035419895 |
| work_keys_str_mv | AT mikuttarobert stabilizationoforganicmatterintheacidsoilenvironmentimportanceofmineralphasesandinvolvedmechanisms |