Science and technology of polymer nanofibers:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Hoboken, N.J.
Wiley
2008
|
| Subjects: | |
| Online Access: | Publisher description Inhaltsverzeichnis |
| Item Description: | Includes bibliographical references |
| Physical Description: | XIX, 403 S. Ill., graph. Darst. |
| ISBN: | 9780471790594 |
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| 100 | 1 | |a Andrady, Anthony L. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Science and technology of polymer nanofibers |c Anthony L. Andrady |
| 264 | 1 | |a Hoboken, N.J. |b Wiley |c 2008 | |
| 300 | |a XIX, 403 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
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| 500 | |a Includes bibliographical references | ||
| 650 | 4 | |a Nanofibers | |
| 650 | 4 | |a Electrospinning | |
| 650 | 4 | |a Synthetic products | |
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Record in the Search Index
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| adam_text | CONTENTS
Preface xiü
Acknowledgments xix
1 Introduction 1
1.1 Historical Background 3
1.2 Basic Experimental Approach 7
1.3 Description of Electrostatic Spinning 9
1.3.1 Droplet Generation 10
1.3.2 Taylor s Cone Formation 13
1.3.3 Launching of the Jet 14
1.3.4 Elongation of Straight Segment 16
1.3.5 Whipping Instability Region 18
1.3.6 Solidification into Nanofiber 22
1.4 Nanofiber Application Areas 23
1.4.1 Filtration and Protective Apparel 24
1.4.2 Tissue Scaffolding and Drug Delivery 25
1.4.3 Nanocomposites 25
1.4.4 Sensor Applications 26
2 Introduction to Polymer Solutions 27
2.1 Average Molecular Weight 28
2.2 Selecting Solvents: Solubility Parameter 31
2.3 Thermodynamic Criterion for Solubility 35
2.3.1 Change in Entropy 36
2.3.2 Change in Enthalpy (A//mix) 39
2.4 Macromolecular Models 41
2.5 Viscosity of Dilute Polymer Solutions 45
2.6 Concentrated Polymer Solutions 50
vii
VIII
CONTENTS
Electrospinning Basics 55
3.1 Molecular Weight Effects 56
3.1.1 The Simha-Frisch Parameter, [tj]c 56
3.1.2 Solution Entanglement Number ne 63
3.2 Electrical Charge 68
3.3 Bead Formation in Electrospinning 71
3.4 Introduction to Electrospinning Practice 76
Factors Affecting Nanofiber Quality 81
4.1 The Polymer Solution 83
4.1.1 Concentration Effects 83
4.1.2 Solvent System 86
4.1.3 Conductivity 88
4.1.4 Surface Tension 91
4.1.5 Dielectric Constant e 93
4.1.6 Volatility 96
4.2 Environment 97
4.3 Collector 99
4.3.1 Collector Geometry 99
4.3.2 Collector Material 101
4.4 Applied Potential 102
4.4.1 Applied Voltage V 102
4.4.2 Polarity of the Tip 103
4.5 Feed Rate 105
4.6 Capillary Tip 106
4.7 Gap Distance 108
4.8 Relative Importance of Variables 108
4.9 Examples of Reported Data 109
Characterization of Nanofibers and Mats 111
5.1 Mat Porosity and Pore Size Distribution 115
5.1.1 Mercury Intrusion Porosimetry 117
5.1.2 Liquid Extrusion Porosimetry 119
5.1.3 Capillary Flow Porometry 121
5.1.4 Brunauer, Emmett, and Teller (BET)
Surface Area 123
5.1.5 Other Approaches 125
CONTENTS ¡X
5.2 Nanofiber Diameters and Pore Sizes
by Microscopy 126
5.2.1 Atomic Force Microscopy Technique 129
5.3 Mechanical Properties of Mats 133
5.3.1 Mat-Related Variables 135
5.4 Single-Fiber Characterization 139
5.4.1 Using the AFM for Single-Nanofiber
Measurement 141
5.4.1.1 Nanoindentation 142
5.4.1.2 Bending Test 143
5.4.1.3 Uniaxial Extension 145
5.5 Nanofiber Crystallinity 146
5.5.1 Differential Scanning Calorimetry
(DSC) Technique 146
5.5.2 X-ray Diffraction Methods 148
6 Composite Nanofibers 153
6.1 Carbon Nanotubes in Nanofibers 156
6.1.1 Dispersion of Nanotubes 158
6.1.2 Orientation of Nanotubes 164
6.1.3 Other Carbons 168
6.2 Metal-Nanofiber Composites 169
6.2.1 Direct Electrospinning 169
6.2.2 Reductive Post-Reaction 171
6.2.3 Gas-Phase Post-Reaction 172
6.3 Polymer-Clay Composites 173
6.4 Decorated or Exocomposite Nanofibers 177
6.4.1 Nanofiber-Nanoparticle Composites 177
6.4.1.1 Dry Methods 177
6.4.1.2 Wet Methods 180
6.4.2 Nanofiber-Nanotube Composites 180
7 Biomédical Applications of Nanofibers 183
7.1 Drug Delivery Applications 184
7.1.1 Drug-Loaded Fibers 186
7.1.2 Controlled Delivery of Macromolecules 191
7.2 Scaffolding Applications of Nanofibers 194
7.2.1 Natural Biopolymers 198
X CONTENTS
7.2.1.1 Collagen and Elastin 199
7.2.1.2 Fibrinogen 202
7.2.1.3 Silk 203
7.2.1.4 Chitin/Chitosan 206
7.2.1.5 Poly(3-hydroxybutyrate-co-3-hydroxyvalerate)
(PHBV) 208
7.2.2 Synthetic Polymers 208
7.2.2.1 Polyglycolides (PGA) 209
7.2.2.2 Polylactide (PLA) 210
7.2.2.3 PolyCe-caprolactone) (PCL) 211
7.2.3 Scaffolding with Stem Cells 216
7.3 Other Applications 218
7.3.1 Wound Care Applications 218
7.3.2 Immobilized Bioactive Moieties on Nanofibers 220
7.4 Future Directions 222
8 Applications of Nanofiber Mats 225
8.1 Introduction to Air Filtration 225
8.1.1 Nanofiber Filter Performance 232
8.1.2 Filters with Nanofibers 233
8.2 Nanofiber Sensors 235
8.2.1 Gravimetric Sensors 236
8.2.2 Conductivity Sensors 237
8.2.3 Optical Sensors 240
8.3 Inorganic Nanofibers 241
8.3.1 Sol-Gel Chemistry 241
8.3.2 Oxide Nanofibers 242
9 Recent Developments in Electrospinning 249
9.1 Nanofibers with Surface Porosity 249
9.1.1 Extraction of a Component from
Bicomponent Nanofibers 250
9.1.2 Phase Separation During Electrospinning 252
9.2 Core-Shell Nanofibers 257
9.2.1 Coaxial Electrospinning 258
9.2.2 Core-Shell Geometry by Post-Treatment
of Nanofibers 263
CONTENTS
XI
9.3 Highly Aligned Nanofiber Mats 265
9.3.1 Parallel Electrode Collector 266
9.3.2 Rotating Cylinder Collectors 267
9.3.3 Chain Orientation During Fiber Alignment 271
9.3.4 Infrared Dichroism 272
9.4 Mixed Polymer Nanofibers and Nanofiber Mats 274
9.5 Crosslinked Nanofibers 277
9.5.1 Photocrosslinked Nanofibers 277
9.5.2 Crosslinking Agents 279
Appendix I Electrospun Polymers Used in Tissue
Engineering and Biomédical Applications 283
Appendix II Summary Table of Electrospun Polymer
Nanofibers 291
References 329
Index 389
|
| adam_txt |
CONTENTS
Preface xiü
Acknowledgments xix
1 Introduction 1
1.1 Historical Background 3
1.2 Basic Experimental Approach 7
1.3 Description of Electrostatic Spinning 9
1.3.1 Droplet Generation 10
1.3.2 Taylor's Cone Formation 13
1.3.3 Launching of the Jet 14
1.3.4 Elongation of Straight Segment 16
1.3.5 Whipping Instability Region 18
1.3.6 Solidification into Nanofiber 22
1.4 Nanofiber Application Areas 23
1.4.1 Filtration and Protective Apparel 24
1.4.2 Tissue Scaffolding and Drug Delivery 25
1.4.3 Nanocomposites 25
1.4.4 Sensor Applications 26
2 Introduction to Polymer Solutions 27
2.1 Average Molecular Weight 28
2.2 Selecting Solvents: Solubility Parameter 31
2.3 Thermodynamic Criterion for Solubility 35
2.3.1 Change in Entropy 36
2.3.2 Change in Enthalpy (A//mix) 39
2.4 Macromolecular Models 41
2.5 Viscosity of Dilute Polymer Solutions 45
2.6 Concentrated Polymer Solutions 50
vii
VIII
CONTENTS
Electrospinning Basics 55
3.1 Molecular Weight Effects 56
3.1.1 The Simha-Frisch Parameter, [tj]c 56
3.1.2 Solution Entanglement Number ne 63
3.2 Electrical Charge 68
3.3 Bead Formation in Electrospinning 71
3.4 Introduction to Electrospinning Practice 76
Factors Affecting Nanofiber Quality 81
4.1 The Polymer Solution 83
4.1.1 Concentration Effects 83
4.1.2 Solvent System 86
4.1.3 Conductivity 88
4.1.4 Surface Tension 91
4.1.5 Dielectric Constant e 93
4.1.6 Volatility 96
4.2 Environment 97
4.3 Collector 99
4.3.1 Collector Geometry 99
4.3.2 Collector Material 101
4.4 Applied Potential 102
4.4.1 Applied Voltage V 102
4.4.2 Polarity of the Tip 103
4.5 Feed Rate 105
4.6 Capillary Tip 106
4.7 Gap Distance 108
4.8 Relative Importance of Variables 108
4.9 Examples of Reported Data 109
Characterization of Nanofibers and Mats 111
5.1 Mat Porosity and Pore Size Distribution 115
5.1.1 Mercury Intrusion Porosimetry 117
5.1.2 Liquid Extrusion Porosimetry 119
5.1.3 Capillary Flow Porometry 121
5.1.4 Brunauer, Emmett, and Teller (BET)
Surface Area 123
5.1.5 Other Approaches 125
CONTENTS ¡X
5.2 Nanofiber Diameters and Pore Sizes
by Microscopy 126
5.2.1 Atomic Force Microscopy Technique 129
5.3 Mechanical Properties of Mats 133
5.3.1 Mat-Related Variables 135
5.4 Single-Fiber Characterization 139
5.4.1 Using the AFM for Single-Nanofiber
Measurement 141
5.4.1.1 Nanoindentation 142
5.4.1.2 Bending Test 143
5.4.1.3 Uniaxial Extension 145
5.5 Nanofiber Crystallinity 146
5.5.1 Differential Scanning Calorimetry
(DSC) Technique 146
5.5.2 X-ray Diffraction Methods 148
6 Composite Nanofibers 153
6.1 Carbon Nanotubes in Nanofibers 156
6.1.1 Dispersion of Nanotubes 158
6.1.2 Orientation of Nanotubes 164
6.1.3 Other Carbons 168
6.2 Metal-Nanofiber Composites 169
6.2.1 Direct Electrospinning 169
6.2.2 Reductive Post-Reaction 171
6.2.3 Gas-Phase Post-Reaction 172
6.3 Polymer-Clay Composites 173
6.4 Decorated or Exocomposite Nanofibers 177
6.4.1 Nanofiber-Nanoparticle Composites 177
6.4.1.1 Dry Methods 177
6.4.1.2 Wet Methods 180
6.4.2 Nanofiber-Nanotube Composites 180
7 Biomédical Applications of Nanofibers 183
7.1 Drug Delivery Applications 184
7.1.1 Drug-Loaded Fibers 186
7.1.2 Controlled Delivery of Macromolecules 191
7.2 Scaffolding Applications of Nanofibers 194
7.2.1 Natural Biopolymers 198
X CONTENTS
7.2.1.1 Collagen and Elastin 199
7.2.1.2 Fibrinogen 202
7.2.1.3 Silk 203
7.2.1.4 Chitin/Chitosan 206
7.2.1.5 Poly(3-hydroxybutyrate-co-3-hydroxyvalerate)
(PHBV) 208
7.2.2 Synthetic Polymers 208
7.2.2.1 Polyglycolides (PGA) 209
7.2.2.2 Polylactide (PLA) 210
7.2.2.3 PolyCe-caprolactone) (PCL) 211
7.2.3 Scaffolding with Stem Cells 216
7.3 Other Applications 218
7.3.1 Wound Care Applications 218
7.3.2 Immobilized Bioactive Moieties on Nanofibers 220
7.4 Future Directions 222
8 Applications of Nanofiber Mats 225
8.1 Introduction to Air Filtration 225
8.1.1 Nanofiber Filter Performance 232
8.1.2 Filters with Nanofibers 233
8.2 Nanofiber Sensors 235
8.2.1 Gravimetric Sensors 236
8.2.2 Conductivity Sensors 237
8.2.3 Optical Sensors 240
8.3 Inorganic Nanofibers 241
8.3.1 Sol-Gel Chemistry 241
8.3.2 Oxide Nanofibers 242
9 Recent Developments in Electrospinning 249
9.1 Nanofibers with Surface Porosity 249
9.1.1 Extraction of a Component from
Bicomponent Nanofibers 250
9.1.2 Phase Separation During Electrospinning 252
9.2 Core-Shell Nanofibers 257
9.2.1 Coaxial Electrospinning 258
9.2.2 Core-Shell Geometry by Post-Treatment
of Nanofibers 263
CONTENTS
XI
9.3 Highly Aligned Nanofiber Mats 265
9.3.1 Parallel Electrode Collector 266
9.3.2 Rotating Cylinder Collectors 267
9.3.3 Chain Orientation During Fiber Alignment 271
9.3.4 Infrared Dichroism 272
9.4 Mixed Polymer Nanofibers and Nanofiber Mats 274
9.5 Crosslinked Nanofibers 277
9.5.1 Photocrosslinked Nanofibers 277
9.5.2 Crosslinking Agents 279
Appendix I Electrospun Polymers Used in Tissue
Engineering and Biomédical Applications 283
Appendix II Summary Table of Electrospun Polymer
Nanofibers 291
References 329
Index 389 |
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| illustrated | Illustrated |
| index_date | 2024-07-02T20:28:54Z |
| indexdate | 2024-07-09T21:14:12Z |
| institution | BVB |
| isbn | 9780471790594 |
| language | English |
| lccn | 2007027362 |
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| spelling | Andrady, Anthony L. Verfasser aut Science and technology of polymer nanofibers Anthony L. Andrady Hoboken, N.J. Wiley 2008 XIX, 403 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references Nanofibers Electrospinning Synthetic products Polymers Polymere (DE-588)4046699-1 gnd rswk-swf Nanostruktur (DE-588)4204530-7 gnd rswk-swf Elektrospinnen (DE-588)7543825-2 gnd rswk-swf Nanostruktur (DE-588)4204530-7 s Elektrospinnen (DE-588)7543825-2 s Polymere (DE-588)4046699-1 s DE-604 http://www.loc.gov/catdir/enhancements/fy0740/2007027362-d.html Publisher description HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016438848&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Andrady, Anthony L. Science and technology of polymer nanofibers Nanofibers Electrospinning Synthetic products Polymers Polymere (DE-588)4046699-1 gnd Nanostruktur (DE-588)4204530-7 gnd Elektrospinnen (DE-588)7543825-2 gnd |
| subject_GND | (DE-588)4046699-1 (DE-588)4204530-7 (DE-588)7543825-2 |
| title | Science and technology of polymer nanofibers |
| title_auth | Science and technology of polymer nanofibers |
| title_exact_search | Science and technology of polymer nanofibers |
| title_exact_search_txtP | Science and technology of polymer nanofibers |
| title_full | Science and technology of polymer nanofibers Anthony L. Andrady |
| title_fullStr | Science and technology of polymer nanofibers Anthony L. Andrady |
| title_full_unstemmed | Science and technology of polymer nanofibers Anthony L. Andrady |
| title_short | Science and technology of polymer nanofibers |
| title_sort | science and technology of polymer nanofibers |
| topic | Nanofibers Electrospinning Synthetic products Polymers Polymere (DE-588)4046699-1 gnd Nanostruktur (DE-588)4204530-7 gnd Elektrospinnen (DE-588)7543825-2 gnd |
| topic_facet | Nanofibers Electrospinning Synthetic products Polymers Polymere Nanostruktur Elektrospinnen |
| url | http://www.loc.gov/catdir/enhancements/fy0740/2007027362-d.html http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016438848&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT andradyanthonyl scienceandtechnologyofpolymernanofibers |