Chemorheology of polymers: from fundamental principles to reactive processing
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Cambridge [u.a.]
Cambridge Univ. Press
2009
|
| Edition: | 1. publ. |
| Subjects: | |
| Online Access: | Klappentext Inhaltsverzeichnis |
| Item Description: | graph. Darst. |
| Physical Description: | VIII, 443 S. |
| ISBN: | 9780521807197 0521807190 |
Staff View
MARC
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| 100 | 1 | |a George, Graeme A. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Chemorheology of polymers |b from fundamental principles to reactive processing |c Peter J. Halley ; Graeme A. George |
| 250 | |a 1. publ. | ||
| 264 | 1 | |a Cambridge [u.a.] |b Cambridge Univ. Press |c 2009 | |
| 300 | |a VIII, 443 S. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a graph. Darst. | ||
| 650 | 4 | |a Polymers |x Rheology | |
| 650 | 4 | |a Polymers |x Viscosity | |
| 650 | 4 | |a Polymers |x Thermal properties | |
| 700 | 1 | |a Halley, Peter J. |d 1966- |e Sonstige |0 (DE-588)138352518 |4 oth | |
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| 856 | 4 | 2 | |m Digitalisierung UB Bayreuth |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016391112&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
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Record in the Search Index
| _version_ | 1804137483488722944 |
|---|---|
| adam_text | chemorheology
of Polymers
Peter
j.
Halley
is a Professor in
the School of Engineering and a
Group Leader in the Australian
institute for
Bioengineering
and
NanotechnologyiAlBNjatthe
university of Queensland. He is a
Fellow ofthe institute of Chemical
Engineering (FichemE) and a Fellow
ofthe Royal Australian chemical
institute (FRACI).
Graeme A. George is Professor of
Polymer Science in the School of
Physical and chemical sciences,
Queensland university of
Technology,
не
is a Fellow and Past-
president of the Royal Australian
chemical
institute and
a Member
of the Orderof Australia. He has
received several awards recognizing
his contribution to international
polymer science.
Understandingthe dynamics of reactive polymer processes
allows scientists to create new, high value, high performance
polymers. Chemorheoiogy of Polymers provides an
indispensable resource for researchers and practitioners
working in this area, describingtheoretical and industrial
approaches to characterizing the flow and gelation of
reactive polymers. Beginning with an in-depth treatment
ofthe chemistry and physics of thermoplastics,
thermosets
and reactive polymers, the core ofthe book focuses on
fundamental characterization of
reattive
polymers, Theological
(flow characterization) techniques and the kinetic and
chemorheological models of these systems. Uniquely, the
coverage extends to a com
plete
review ofthe practical industrial
processes used forthese polymers and provides an insight into
the current chemorheological models and tools used to describe
and control each process. This book will appeal to polymer
scientists workingon reactive polymers within materials
science, chemistry and chemical engineering departments
as well as to polymer process engineers in industry.
Contents
Preface
page ¡x
Chemistry and structure of reactive polymers
1
1.1
The physical structure of polymers
1
1.1.1
Linear polymers as freely jointed chains
2
1.1.2
Conformations of linear hydrocarbon polymers
5
1.1.3
Molar mass and molar-mass distribution
8
1.1.4
Development of the solid state from the melt
11
1.2
Controlled molecular architecture
23
1.2.1
Stepwise polymerization
24
.2.2
Different polymer architectures achieved by step polymerization
36
.2.3
Addition polymerization
59
.2.4
Obtaining different polymer architectures by addition polymerization
85
.2.5
Networks from addition polymerization
99
1.3
Polymer blends and composites
105
.3.1
Miscibility of polymers
106
.3.2
Phase-separation phenomena 111
.3.3
Interpenetrating networks
126
1.4
Degradation and stabilization
127
.4.1
Free-radical formation during melt processing
128
.4.2
Free-radical formation in the presence of oxygen
139
.4.3
Control of free-radical reactions during processing
149
References
162
Physics and dynamics of reactive polymers
2.1
Chapter rationale
2.2
Polymer physics and dynamics
2.2.1
Polymer physics and motion
-
early models
2.2.2
Theories of polymer dynamics
2.3
Introduction to the physics of reactive polymers
2.3.1
Network polymers
2.3.2
Reactively modified polymers
2.4
Physical transitions in curing systems
2.4.1
Gelation and vitrification
2.4.2
Phase separation
2.4.3
Time-temperature-transformation (TTT) diagrams
169
169
169
169
170
175
176
177
179
180
181
181
Contents
2.4.4
Reactive
systems without major
transitions
186
2.5
Physicochemical models of reactive polymers
186
2.5.1
Network models
187
2.5.2
Reactive polymer models
191
References
192
Chemical and physical analyses for reactive polymers
195
3.1
Monitoring physical and chemical changes during reactive processing
195
3.2
Differential scanning calorimetry (DSC)
196
3.2.1
An outline of DSC theory
196
3.2.2
Isothermal DSC experiments for polymer chemorheology
197
3.2.3
Modulated DSC experiments for chemorheology
202
3.2.4
Scanning DSC experiments for chemorheology
203
3.2.5
Process-control parameters from time-temperature superposition
206
3.2.6
Kinetic models for network-formation from DSC
207
3.3
Spectroscopie
methods of analysis
208
3.3.1
Information from
spectroscopie
methods
208
3.3.2
Magnetic resonance spectroscopy
209
3.3.3
Vibrational spectroscopy overview
-
selection rules
213
3.3.4
Fourier-transform infrared (FT-IR) and sampling methods:
transmission, reflection, emission, excitation
216
3.3.5
Mid-infrared (MIR) analysis of polymer reactions
222
3.3.6
Near-infrared (NIR) analysis of polymer reactions
235
3.3.7
Raman-spectral analysis of polymer reactions
240
3.3.8
UV-visible spectroscopy and fluorescence analysis of polymer reactions
244
3.3.9
Chemiluminescence and charge-recombination luminescence
255
3.4
Remote spectroscopy
259
3.4.1
Principles of fibre-optics
259
3.4.2
Coupling of fibre-optics to reacting systems
263
3.5
Chemometrics and statistical analysis of spectral data
271
3.5.1
Multivariate curve resolution
272
3.5.2
Multivariate calibration
275
3.5.3
Other curve-resolution and calibration methods
280
3.6
Experimental techniques for determining physical properties during cure
282
3.6.1
Torsionai
braid analysis
282
3.6.2
Mechanical properties
283
3.6.3
Dielectric properties
287
3.6.4
Rheology
292
3.6.5
Other techniques
305
3.6.6
Dual physicochemical analysis
311
References
312
Chemorheological techniques for reactive polymers
321
4.1
Introduction
321
4.2
Chemorheology
321
4.2.1
Fundamental chemorheology
321
Contents
VII
4.3 Chemoviscosity
profiles
327
4.3.1 Chemoviscosity 327
4.3.2 Gel
effects
336
4.4
Chemorheological techniques
336
4.4.1
Standards
338
4.4.2
Chemoviscosity profiles
-
shear-rate effects,
η3 = ηΒ(γ, Τ)
338
4.4.3
Chemoviscosity profiles
-
cure effects,
η€ = ηο(α, Τ)
342
4.4.4
Filler effects on viscosity: ^sr(F) and ^(F)
343
4.4.5
Chemoviscosity profiles
-
combined effects,
ηΜ = ηΜ(γ, α, Τ)
344
4.4.6
Process parameters
344
4.5
Gelation techniques
345
References
347
Chemorheology and chemorheological modelling
351
5.1
Introduction
351
5.2
Chemoviscosity and chemorheological models
351
5.2.1
Neat systems
351
5.2.2
Filled systems
357
5.2.3
Reactive-extrusion systems and elastomer/rabber-processing systems
370
5.3
Chemorheological models and process modelling
370
References
371
Industrial technologies, chemorheological modelling and process modelling
for processing reactive polymers
375
6.1
Introduction
375
6.2
Casting
375
6.2.1
Process diagram and description
375
6.2.2
Quality-control tests and important process variables
375
6.2.3
Typical systems
376
6.2.4
Chemorheological and process modelling
376
6.3
Potting, encapsulation, sealing and foaming
378
6.3.1
Process diagram and description
378
6.3.2
Quality-control tests and important process variables
379
6.3.3
Typical systems
379
6.3.4
Chemorheological and process modelling
380
6.4
Thermoset extrusion
380
6.4.1
Extrusion
380
6.4.2
Pultrasion
382
6.5
Reactive extrusion
385
6.5.1
Process diagram and description
385
6.5.2
Quality-control tests and important process variables
387
6.5.3
Typical systems
388
6.5.4
Chemorheological and process modelling
389
6.6
Moulding processes
391
6.6.1
Open-mould processes
391
6.6.2
Resin-transfer moulding
393
viii Contents
6.6.3
Compression, SMC, DMC
and BMC moulding
395
6.6.4
Transfer moulding
397
6.6.5
Reaction injection moulding
400
6.6.6
Thermoset injection moulding
403
6.6.7
Press moulding (prepreg)
405
6.6.8
Autoclave moulding (prepreg)
406
6.7
Rubber mixing and processing
407
6.7.1
Rubber mixing processes
407
6.7.2
Rubber processing
409
6.8
High-energy processing
413
6.8.1
Microwave processing
413
6.8.2
Ultraviolet processing
415
6.8.3
Gamma-irradiation processing
416
6.8.4
Electron-beam-irradiation processing
417
6.9
Novel processing
420
6.9.1
Rapid prototyping and manufacturing
420
6.9.2
Microlithography
424
6.10
Real-time monitoring
426
6.10.1
Sensors for real-time process monitoring
426
6.10.2
Real-time monitoring using fibre optics
429
References
431
Glossary of commonly used terms
435
Index
440
|
| adam_txt |
chemorheology
of Polymers
Peter
j.
Halley
is a Professor in
the School of Engineering and a
Group Leader in the Australian
institute for
Bioengineering
and
NanotechnologyiAlBNjatthe
university of Queensland. He is a
Fellow ofthe institute of Chemical
Engineering (FichemE) and a Fellow
ofthe Royal Australian chemical
institute (FRACI).
Graeme A. George is Professor of
Polymer Science in the School of
Physical and chemical sciences,
Queensland university of
Technology,
не
is a Fellow and Past-
president of the Royal Australian
chemical
institute and
a Member
of the Orderof Australia. He has
received several awards recognizing
his contribution to international
polymer science.
Understandingthe dynamics of reactive polymer processes
allows scientists to create new, high value, high performance
polymers. Chemorheoiogy of Polymers provides an
indispensable resource for researchers and practitioners
working in this area, describingtheoretical and industrial
approaches to characterizing the flow and gelation of
reactive polymers. Beginning with an in-depth treatment
ofthe chemistry and physics of thermoplastics,
thermosets
and reactive polymers, the core ofthe book focuses on
fundamental characterization of
reattive
polymers, Theological
(flow characterization) techniques and the kinetic and
chemorheological models of these systems. Uniquely, the
coverage extends to a com
plete
review ofthe practical industrial
processes used forthese polymers and provides an insight into
the current chemorheological models and tools used to describe
and control each process. This book will appeal to polymer
scientists workingon reactive polymers within materials
science, chemistry and chemical engineering departments
as well as to polymer process engineers in industry.
Contents
Preface
page ¡x
Chemistry and structure of reactive polymers
1
1.1
The physical structure of polymers
1
1.1.1
Linear polymers as freely jointed chains
2
1.1.2
Conformations of linear hydrocarbon polymers
5
1.1.3
Molar mass and molar-mass distribution
8
1.1.4
Development of the solid state from the melt
11
1.2
Controlled molecular architecture
23
1.2.1
Stepwise polymerization
24
.2.2
Different polymer architectures achieved by step polymerization
36
.2.3
Addition polymerization
59
.2.4
Obtaining different polymer architectures by addition polymerization
85
.2.5
Networks from addition polymerization
99
1.3
Polymer blends and composites
105
.3.1
Miscibility of polymers
106
.3.2
Phase-separation phenomena 111
.3.3
Interpenetrating networks
126
1.4
Degradation and stabilization
127
.4.1
Free-radical formation during melt processing
128
.4.2
Free-radical formation in the presence of oxygen
139
.4.3
Control of free-radical reactions during processing
149
References
162
Physics and dynamics of reactive polymers
2.1
Chapter rationale
2.2
Polymer physics and dynamics
2.2.1
Polymer physics and motion
-
early models
2.2.2
Theories of polymer dynamics
2.3
Introduction to the physics of reactive polymers
2.3.1
Network polymers
2.3.2
Reactively modified polymers
2.4
Physical transitions in curing systems
2.4.1
Gelation and vitrification
2.4.2
Phase separation
2.4.3
Time-temperature-transformation (TTT) diagrams
169
169
169
169
170
175
176
177
179
180
181
181
Contents
2.4.4
Reactive
systems without major
transitions
186
2.5
Physicochemical models of reactive polymers
186
2.5.1
Network models
187
2.5.2
Reactive polymer models
191
References
192
Chemical and physical analyses for reactive polymers
195
3.1
Monitoring physical and chemical changes during reactive processing
195
3.2
Differential scanning calorimetry (DSC)
196
3.2.1
An outline of DSC theory
196
3.2.2
Isothermal DSC experiments for polymer chemorheology
197
3.2.3
Modulated DSC experiments for chemorheology
202
3.2.4
Scanning DSC experiments for chemorheology
203
3.2.5
Process-control parameters from time-temperature superposition
206
3.2.6
Kinetic models for network-formation from DSC
207
3.3
Spectroscopie
methods of analysis
208
3.3.1
Information from
spectroscopie
methods
208
3.3.2
Magnetic resonance spectroscopy
209
3.3.3
Vibrational spectroscopy overview
-
selection rules
213
3.3.4
Fourier-transform infrared (FT-IR) and sampling methods:
transmission, reflection, emission, excitation
216
3.3.5
Mid-infrared (MIR) analysis of polymer reactions
222
3.3.6
Near-infrared (NIR) analysis of polymer reactions
235
3.3.7
Raman-spectral analysis of polymer reactions
240
3.3.8
UV-visible spectroscopy and fluorescence analysis of polymer reactions
244
3.3.9
Chemiluminescence and charge-recombination luminescence
255
3.4
Remote spectroscopy
259
3.4.1
Principles of fibre-optics
259
3.4.2
Coupling of fibre-optics to reacting systems
263
3.5
Chemometrics and statistical analysis of spectral data
271
3.5.1
Multivariate curve resolution
272
3.5.2
Multivariate calibration
275
3.5.3
Other curve-resolution and calibration methods
280
3.6
Experimental techniques for determining physical properties during cure
282
3.6.1
Torsionai
braid analysis
282
3.6.2
Mechanical properties
283
3.6.3
Dielectric properties
287
3.6.4
Rheology
292
3.6.5
Other techniques
305
3.6.6
Dual physicochemical analysis
311
References
312
Chemorheological techniques for reactive polymers
321
4.1
Introduction
321
4.2
Chemorheology
321
4.2.1
Fundamental chemorheology
321
Contents
VII
4.3 Chemoviscosity
profiles
327
4.3.1 Chemoviscosity 327
4.3.2 Gel
effects
336
4.4
Chemorheological techniques
336
4.4.1
Standards
338
4.4.2
Chemoviscosity profiles
-
shear-rate effects,
η3 = ηΒ(γ, Τ)
338
4.4.3
Chemoviscosity profiles
-
cure effects,
η€ = ηο(α, Τ)
342
4.4.4
Filler effects on viscosity: ^sr(F) and ^(F)
343
4.4.5
Chemoviscosity profiles
-
combined effects,
ηΜ = ηΜ(γ, α, Τ)
344
4.4.6
Process parameters
344
4.5
Gelation techniques
345
References
347
Chemorheology and chemorheological modelling
351
5.1
Introduction
351
5.2
Chemoviscosity and chemorheological models
351
5.2.1
Neat systems
351
5.2.2
Filled systems
357
5.2.3
Reactive-extrusion systems and elastomer/rabber-processing systems
370
5.3
Chemorheological models and process modelling
370
References
371
Industrial technologies, chemorheological modelling and process modelling
for processing reactive polymers
375
6.1
Introduction
375
6.2
Casting
375
6.2.1
Process diagram and description
375
6.2.2
Quality-control tests and important process variables
375
6.2.3
Typical systems
376
6.2.4
Chemorheological and process modelling
376
6.3
Potting, encapsulation, sealing and foaming
378
6.3.1
Process diagram and description
378
6.3.2
Quality-control tests and important process variables
379
6.3.3
Typical systems
379
6.3.4
Chemorheological and process modelling
380
6.4
Thermoset extrusion
380
6.4.1
Extrusion
380
6.4.2
Pultrasion
382
6.5
Reactive extrusion
385
6.5.1
Process diagram and description
385
6.5.2
Quality-control tests and important process variables
387
6.5.3
Typical systems
388
6.5.4
Chemorheological and process modelling
389
6.6
Moulding processes
391
6.6.1
Open-mould processes
391
6.6.2
Resin-transfer moulding
393
viii Contents
6.6.3
Compression, SMC, DMC
and BMC moulding
395
6.6.4
Transfer moulding
397
6.6.5
Reaction injection moulding
400
6.6.6
Thermoset injection moulding
403
6.6.7
Press moulding (prepreg)
405
6.6.8
Autoclave moulding (prepreg)
406
6.7
Rubber mixing and processing
407
6.7.1
Rubber mixing processes
407
6.7.2
Rubber processing
409
6.8
High-energy processing
413
6.8.1
Microwave processing
413
6.8.2
Ultraviolet processing
415
6.8.3
Gamma-irradiation processing
416
6.8.4
Electron-beam-irradiation processing
417
6.9
Novel processing
420
6.9.1
Rapid prototyping and manufacturing
420
6.9.2
Microlithography
424
6.10
Real-time monitoring
426
6.10.1
Sensors for real-time process monitoring
426
6.10.2
Real-time monitoring using fibre optics
429
References
431
Glossary of commonly used terms
435
Index
440 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | George, Graeme A. |
| author_GND | (DE-588)138352518 |
| author_facet | George, Graeme A. |
| author_role | aut |
| author_sort | George, Graeme A. |
| author_variant | g a g ga gag |
| building | Verbundindex |
| bvnumber | BV023204940 |
| classification_rvk | UV 4100 VE 8000 VN 5900 |
| ctrlnum | (OCoLC)635069291 (DE-599)HBZHT015425104 |
| discipline | Chemie / Pharmazie Physik |
| discipline_str_mv | Chemie / Pharmazie Physik |
| edition | 1. publ. |
| format | Book |
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| id | DE-604.BV023204940 |
| illustrated | Not Illustrated |
| index_date | 2024-07-02T20:09:35Z |
| indexdate | 2024-07-09T21:13:01Z |
| institution | BVB |
| isbn | 9780521807197 0521807190 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-016391112 |
| oclc_num | 635069291 |
| open_access_boolean | |
| owner | DE-703 DE-355 DE-BY-UBR DE-11 |
| owner_facet | DE-703 DE-355 DE-BY-UBR DE-11 |
| physical | VIII, 443 S. |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | Cambridge Univ. Press |
| record_format | marc |
| spelling | George, Graeme A. Verfasser aut Chemorheology of polymers from fundamental principles to reactive processing Peter J. Halley ; Graeme A. George 1. publ. Cambridge [u.a.] Cambridge Univ. Press 2009 VIII, 443 S. txt rdacontent n rdamedia nc rdacarrier graph. Darst. Polymers Rheology Polymers Viscosity Polymers Thermal properties Halley, Peter J. 1966- Sonstige (DE-588)138352518 oth Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016391112&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Klappentext Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016391112&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | George, Graeme A. Chemorheology of polymers from fundamental principles to reactive processing Polymers Rheology Polymers Viscosity Polymers Thermal properties |
| title | Chemorheology of polymers from fundamental principles to reactive processing |
| title_auth | Chemorheology of polymers from fundamental principles to reactive processing |
| title_exact_search | Chemorheology of polymers from fundamental principles to reactive processing |
| title_exact_search_txtP | Chemorheology of polymers from fundamental principles to reactive processing |
| title_full | Chemorheology of polymers from fundamental principles to reactive processing Peter J. Halley ; Graeme A. George |
| title_fullStr | Chemorheology of polymers from fundamental principles to reactive processing Peter J. Halley ; Graeme A. George |
| title_full_unstemmed | Chemorheology of polymers from fundamental principles to reactive processing Peter J. Halley ; Graeme A. George |
| title_short | Chemorheology of polymers |
| title_sort | chemorheology of polymers from fundamental principles to reactive processing |
| title_sub | from fundamental principles to reactive processing |
| topic | Polymers Rheology Polymers Viscosity Polymers Thermal properties |
| topic_facet | Polymers Rheology Polymers Viscosity Polymers Thermal properties |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016391112&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016391112&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT georgegraemea chemorheologyofpolymersfromfundamentalprinciplestoreactiveprocessing AT halleypeterj chemorheologyofpolymersfromfundamentalprinciplestoreactiveprocessing |