Dynamic mechanical analysis: a practical introduction
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| Main Author: | |
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| Format: | Book |
| Language: | English |
| Published: |
Boca Raton, FL [u.a.]
CRC Press
2008
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| Edition: | 2. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Includes bibliographical references and index |
| Physical Description: | XIX, 218 S. Ill., graph. Darst. |
| ISBN: | 1420053124 9781420053128 |
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| 245 | 1 | 0 | |a Dynamic mechanical analysis |b a practical introduction |c Kevin P. Menard |
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| 264 | 1 | |a Boca Raton, FL [u.a.] |b CRC Press |c 2008 | |
| 300 | |a XIX, 218 S. |b Ill., graph. Darst. | ||
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| adam_text | Titel: Dynamic mechanical analysis
Autor: Menard, Kevin P
Jahr: 2008
Contents
Author s Preface.....................................................................................................xi
Foreword to the First Edition.............................................................................xiii
Foreword to the Second Edition...........................................................................xv
Acknowledgments................................................................................................xvii
Author....................................................................................................................xix
Chapter 1 An Introduction to Dynamic Mechanical Analysis.............................1
1.1 A Brief History of DMA...................................................................................1
1.2 Basic Principles.................................................................................................2
1.3 Sample Applications..........................................................................................4
1.4 Creep-Recovery Testing...................................................................................9
1.5 Aggressive Environments................................................................................10
Notes........................................................................................................................12
Chapter 2 Basic Rheological Concepts
Stress, Strain, and Flow.....................................................................15
2.1 Force, Stress, and Deformation.......................................................................15
2.2 Applying the Stress..........................................................................................12
2.3 Hooke s Law: Defining the Elastic Response..................................................20
2.4 Geometry, Sample Shape, and Aspect Ratio...................................................24
2.5 Liquid-Like Flow or the Viscous Limit...........................................................25
2.6 Another Look at Stress-Strain Curves............................................................28
2.7 Appendix: Conversion Factors........................................................................32
Notes........................................................................................................................35
Chapter 3 Rheology Basics
Creep-Recovery and Stress Relaxation............................................37
3.1 Creep-Recovery Testing.................................................................................37
3.2 Models to Describe Creep-Recovery Behavior..............................................40
3.3 Analyzing a Creep-Recovery Curve to Fit the Four-Element Model.............41
3.4 Analyzing a Creep Experiment for Practical Use...........................................44
3.5 Creep Ringing.................................................................................................45
3.6 Other Variations on Creep Tests......................................................................45
3.7 Superposition: The Boltzmann Principle........................................................48
3.8 Retardation and Relaxation Times..................................................................49
3.9 Structure-Property Relationships in Creep-Recovery Tests..........................50
vii
viii
Contents
3.10 Stress Relaxation Experiments........................................................................
3.11 Constant Gauge Length Tests..........................................................................^3
Notes........................................................................................................................
Chapter 4 Thermomechanical Analysis..............................................................57
4.1 Theory of Thermomechanical Analysis..........................................................57
4.2 Experimental Considerations with TMA Samples..........................................59
4.3 Expansion and ............................................................................................61
4.4 Flexure and Penetration...................................................................................64
4.5 Dilatometry and Bulk Measurements.............................................................65
4.6 Mechanical Tests.............................................................................................65
4.7 PVT Relationship Studies................................................................................67
Notes........................................................................................................................68
Chapter 5 Dynamic Testing and Instrumentation...............................................71
5.1 Applying a Dynamic Stress to a Sample.........................................................71
5.2 Calculating Various Dynamic Properties........................................................74
5.2.1 Calculation from Deformation and Phase Lag....................................75
5.2.2 Calculating Properties from a Measured Stiffness.............................76
5.3 Instrumentation for DMA Tests......................................................................76
5.3.1 Forced Resonance Analyzers..............................................................76
5.3.2 Stress and Strain Control.....................................................................77
5.3.3 Axial and Torsional Deformation........................................................79
5.3.4 Free Resonance Analyzers..................................................................79
5.4 Fixtures or Testing Geometries.......................................................................81
5.4.1 Axial....................................................................................................83
5.4.1.1 Three-Point and Four-Point Bending....................................84
5.4.1.2 Dual and Single Cantilever...................................................85
5.4.1.3 Parallel Plate and Variants....................................................86
5.4.1.4 Bulk.......................................................................................87
5.4.1.5 Extension/Tensile..................................................................87
5.4.1.6 Shear Plates and Sandwiches................................................87
5.4.2 Torsional..............................................................................................88
5.4.2.1 Parallel Plates........................................................................88
5.4.2.2 Cone-and-Plate......................................................................89
5.4.2.3 Couette..................................................................................89
5.4.2.4 Torsional Beam and Braid.....................................................90
5.5 Sample Handling Issues.................................................................................90
5.6 Calibration Issues..........................................................................................................................................91
5.7 Dynamic Experiments........................................................................ 92
Notes............................................................................
ix Contents
Chapter 6 Time and Temperature Scans Part I
Transitions in Polymers......................................................................95
6.1 Time and Temperature Scanning in the DMA................................................95
6.2 Transitions in Polymers: Overview.................................................................98
6.3 Sub-Tg Transitions..........................................................................................101
6.4 The Glass Transition (Tg or 7......................................................................103
6.5 The Rubbery Plateau, Ta* and Tn..................................................................106
6.6 The Terminal Region.....................................................................................110
6.7 Frequency Dependencies in Transition Studies.............................................112
6.8 Applications...................................................................................................114
6.9 Time-Based Studies.......................................................................................117
6.10 Conclusions....................................................................................................118
Notes......................................................................................................................119
Chapter 7 Time and Temperature Scans Part II
Thermosets.......................................................................................123
7.1 Thermosetting Materials: A Review.............................................................123
7.2 Studying Curing Behavior in the DMA: Cure Profiles.................................127
7.3 Photocuring...................................................................................................132
7.4 Modeling Cure Cycles...................................................................................133
7.5 Isothermal Curing Studies.............................................................................133
7.6 Kinetics by DMA: The Roller Model and Other Approaches.......................134
7.7 Mapping Thermoset Behavior: The Gillham-Enns Diagram.......................137
7.8 Quality Control Approaches to Thermoset Characterization.......................138
7.9 Postcure Studies.............................................................................................140
7.10 Conclusions....................................................................................................141
Notes......................................................................................................................142
Chapter 8 Frequency Scans...............................................................................145
8.1 Methods of Performing a Frequency Scan....................................................145
8.2 Frequency Effects on Materials.....................................................................147
8.3 The Deborah Number....................................................................................155
8.4 Frequency Effects on Solid Polymers...........................................................155
8.5 Frequency Effects During Curing Studies....................................................158
8.6 Frequency Studies on Polymer Melts............................................................158
8.7 Normal Forces and Elasticity........................................................................159
8.8 Master Curves and Time-Temperature Superposition..................................161
8.9 Transformations of Data................................................................................167
8.10 Molecular Weight and Molecular Weight Distributions...............................169
8.11 Conclusions....................................................................................................121
Notes......................................................................................................................121
Contents
x *
Chapter 9 Unusual Conditions and Specialized Tests......................................175
9.1 UV Studies....................................................................................................175
9.1.1 UV Photocures..................................................................................^77
9.1.2 UV Photodegradations...................................................................... 78
9.2 Humidity Studies...........................................................................................^
9.2.1 Equilibration Times...........................................................................*81
9.2.2 Effects of Humidity in the DMA......................................................182
9.3 Immersion......................................................................................................182
9.3.1 Effects of Solvent on Instrumentation and Measurement.................183
9.3.2 DMA in Solution...............................................................................184
9.4 Hyphenated Techniques.................................................................................186
9.5 Modeling Other Mechanical Tests................................................................187
Notes......................................................................................................................188
Chapter 10 DMA Applications to Real Problems
Guidelines........................................................................................191
10.1 The Problem: Material Characterization or Performance...........................191
10.2 Performance Tests: To Model or to Copy....................................................191
10.3 Choosing a Type of Test..............................................................................192
10.4 Characterization..........................................................................................194
10.5 Choosing the Fixture...................................................................................194
10.6 Checking the Response to Loads................................................................197
10.7 Checking the Response to Frequency.........................................................197
10.8 Checking the Response to Time..................................................................197
10.9 Checking the Temperature Response..........................................................198
10.11 Putting It Together.......................................................................................199
10.12 Verify the Results........................................................................................199
10.13 Supporting Data from Other Methods........................................................200
10.14 Appendix: Sample Experiments for the DMA............................................201
10.14.1 TMA Experiments........................................................................201
10.14.2 Stress-Strain Scans......................................................................201
10.14.3 Creep-Recovery Experiments......................................................201
10.14.4 Stress Relaxation..........................................................................202
10.14.5 Dynamic Strain Sweeps................................................................202
10.14.6 Dynamic Temperature Scans........................................................202
10.14.7 Curing Studies.............................................................................202
10.14.8 Frequency Scans.....................................................................202
Notes........................................................................... ZZZIZZZZZ Zzn
Index......................................................................................................................205
|
| adam_txt |
Titel: Dynamic mechanical analysis
Autor: Menard, Kevin P
Jahr: 2008
Contents
Author's Preface.xi
Foreword to the First Edition.xiii
Foreword to the Second Edition.xv
Acknowledgments.xvii
Author.xix
Chapter 1 An Introduction to Dynamic Mechanical Analysis.1
1.1 A Brief History of DMA.1
1.2 Basic Principles.2
1.3 Sample Applications.4
1.4 Creep-Recovery Testing.9
1.5 Aggressive Environments.10
Notes.12
Chapter 2 Basic Rheological Concepts
Stress, Strain, and Flow.15
2.1 Force, Stress, and Deformation.15
2.2 Applying the Stress.12
2.3 Hooke's Law: Defining the Elastic Response.20
2.4 Geometry, Sample Shape, and Aspect Ratio.24
2.5 Liquid-Like Flow or the Viscous Limit.25
2.6 Another Look at Stress-Strain Curves.28
2.7 Appendix: Conversion Factors.32
Notes.35
Chapter 3 Rheology Basics
Creep-Recovery and Stress Relaxation.37
3.1 Creep-Recovery Testing.37
3.2 Models to Describe Creep-Recovery Behavior.40
3.3 Analyzing a Creep-Recovery Curve to Fit the Four-Element Model.41
3.4 Analyzing a Creep Experiment for Practical Use.44
3.5 Creep Ringing.45
3.6 Other Variations on Creep Tests.45
3.7 Superposition: The Boltzmann Principle.48
3.8 Retardation and Relaxation Times.49
3.9 Structure-Property Relationships in Creep-Recovery Tests.50
vii
viii
Contents
3.10 Stress Relaxation Experiments.
3.11 Constant Gauge Length Tests.^3
Notes.
Chapter 4 Thermomechanical Analysis.57
4.1 Theory of Thermomechanical Analysis.57
4.2 Experimental Considerations with TMA Samples.59
4.3 Expansion and .61
4.4 Flexure and Penetration.64
4.5 Dilatometry and Bulk Measurements.65
4.6 Mechanical Tests.65
4.7 PVT Relationship Studies.67
Notes.68
Chapter 5 Dynamic Testing and Instrumentation.71
5.1 Applying a Dynamic Stress to a Sample.71
5.2 Calculating Various Dynamic Properties.74
5.2.1 Calculation from Deformation and Phase Lag.75
5.2.2 Calculating Properties from a Measured Stiffness.76
5.3 Instrumentation for DMA Tests.76
5.3.1 Forced Resonance Analyzers.76
5.3.2 Stress and Strain Control.77
5.3.3 Axial and Torsional Deformation.79
5.3.4 Free Resonance Analyzers.79
5.4 Fixtures or Testing Geometries.81
5.4.1 Axial.83
5.4.1.1 Three-Point and Four-Point Bending.84
5.4.1.2 Dual and Single Cantilever.85
5.4.1.3 Parallel Plate and Variants.86
5.4.1.4 Bulk.87
5.4.1.5 Extension/Tensile.87
5.4.1.6 Shear Plates and Sandwiches.87
5.4.2 Torsional.88
5.4.2.1 Parallel Plates.88
5.4.2.2 Cone-and-Plate.89
5.4.2.3 Couette.89
5.4.2.4 Torsional Beam and Braid.90
5.5 Sample Handling Issues.90
5.6 Calibration Issues.91
5.7 Dynamic Experiments. 92
Notes.
ix Contents
Chapter 6 Time and Temperature Scans Part I
Transitions in Polymers.95
6.1 Time and Temperature Scanning in the DMA.95
6.2 Transitions in Polymers: Overview.98
6.3 Sub-Tg Transitions.101
6.4 The Glass Transition (Tg or 7.103
6.5 The Rubbery Plateau, Ta* and Tn.106
6.6 The Terminal Region.110
6.7 Frequency Dependencies in Transition Studies.112
6.8 Applications.114
6.9 Time-Based Studies.117
6.10 Conclusions.118
Notes.119
Chapter 7 Time and Temperature Scans Part II
Thermosets.123
7.1 Thermosetting Materials: A Review.123
7.2 Studying Curing Behavior in the DMA: Cure Profiles.127
7.3 Photocuring.132
7.4 Modeling Cure Cycles.133
7.5 Isothermal Curing Studies.133
7.6 Kinetics by DMA: The Roller Model and Other Approaches.134
7.7 Mapping Thermoset Behavior: The Gillham-Enns Diagram.137
7.8 Quality Control Approaches to Thermoset Characterization.138
7.9 Postcure Studies.140
7.10 Conclusions.141
Notes.142
Chapter 8 Frequency Scans.145
8.1 Methods of Performing a Frequency Scan.145
8.2 Frequency Effects on Materials.147
8.3 The Deborah Number.155
8.4 Frequency Effects on Solid Polymers.155
8.5 Frequency Effects During Curing Studies.158
8.6 Frequency Studies on Polymer Melts.158
8.7 Normal Forces and Elasticity.159
8.8 Master Curves and Time-Temperature Superposition.161
8.9 Transformations of Data.167
8.10 Molecular Weight and Molecular Weight Distributions.169
8.11 Conclusions.121
Notes.121
Contents
x *
Chapter 9 Unusual Conditions and Specialized Tests.175
9.1 UV Studies.175
9.1.1 UV Photocures.^77
9.1.2 UV Photodegradations.'78
9.2 Humidity Studies.^
9.2.1 Equilibration Times.*81
9.2.2 Effects of Humidity in the DMA.182
9.3 Immersion.182
9.3.1 Effects of Solvent on Instrumentation and Measurement.183
9.3.2 DMA in Solution.184
9.4 Hyphenated Techniques.186
9.5 Modeling Other Mechanical Tests.187
Notes.188
Chapter 10 DMA Applications to Real Problems
Guidelines.191
10.1 The Problem: Material Characterization or Performance.191
10.2 Performance Tests: To Model or to Copy.191
10.3 Choosing a Type of Test.192
10.4 Characterization.194
10.5 Choosing the Fixture.194
10.6 Checking the Response to Loads.197
10.7 Checking the Response to Frequency.197
10.8 Checking the Response to Time.197
10.9 Checking the Temperature Response.198
10.11 Putting It Together.199
10.12 Verify the Results.199
10.13 Supporting Data from Other Methods.200
10.14 Appendix: Sample Experiments for the DMA.201
10.14.1 TMA Experiments.201
10.14.2 Stress-Strain Scans.201
10.14.3 Creep-Recovery Experiments.201
10.14.4 Stress Relaxation.202
10.14.5 Dynamic Strain Sweeps.202
10.14.6 Dynamic Temperature Scans.202
10.14.7 Curing Studies.202
10.14.8 Frequency Scans.202
Notes."ZZZIZZZZZ'Zzn
Index.205 |
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| index_date | 2024-07-02T19:40:33Z |
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| publisher | CRC Press |
| record_format | marc |
| spelling | Menard, Kevin P. Verfasser aut Dynamic mechanical analysis a practical introduction Kevin P. Menard 2. ed. Boca Raton, FL [u.a.] CRC Press 2008 XIX, 218 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Includes bibliographical references and index Materials Testing Rheology Polymere (DE-588)4046699-1 gnd rswk-swf Thermodynamische Eigenschaft (DE-588)4126056-9 gnd rswk-swf Mechanische Eigenschaft (DE-588)4217961-0 gnd rswk-swf Polymere (DE-588)4046699-1 s Mechanische Eigenschaft (DE-588)4217961-0 s DE-604 Thermodynamische Eigenschaft (DE-588)4126056-9 s HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016292789&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Menard, Kevin P. Dynamic mechanical analysis a practical introduction Materials Testing Rheology Polymere (DE-588)4046699-1 gnd Thermodynamische Eigenschaft (DE-588)4126056-9 gnd Mechanische Eigenschaft (DE-588)4217961-0 gnd |
| subject_GND | (DE-588)4046699-1 (DE-588)4126056-9 (DE-588)4217961-0 |
| title | Dynamic mechanical analysis a practical introduction |
| title_auth | Dynamic mechanical analysis a practical introduction |
| title_exact_search | Dynamic mechanical analysis a practical introduction |
| title_exact_search_txtP | Dynamic mechanical analysis a practical introduction |
| title_full | Dynamic mechanical analysis a practical introduction Kevin P. Menard |
| title_fullStr | Dynamic mechanical analysis a practical introduction Kevin P. Menard |
| title_full_unstemmed | Dynamic mechanical analysis a practical introduction Kevin P. Menard |
| title_short | Dynamic mechanical analysis |
| title_sort | dynamic mechanical analysis a practical introduction |
| title_sub | a practical introduction |
| topic | Materials Testing Rheology Polymere (DE-588)4046699-1 gnd Thermodynamische Eigenschaft (DE-588)4126056-9 gnd Mechanische Eigenschaft (DE-588)4217961-0 gnd |
| topic_facet | Materials Testing Rheology Polymere Thermodynamische Eigenschaft Mechanische Eigenschaft |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=016292789&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT menardkevinp dynamicmechanicalanalysisapracticalintroduction |