The synthetic organic chemist's companion:
"A thorough, accessible reference for organic chemists, laboratory technicians, or students, this guide merits a prominent place in every lab. It's also a great textbook for upper-level undergraduate and graduate students studying organic chemistry, medicine, pharmaceuticals, and polymers....
Gespeichert in:
| Späterer Titel: | Pirrung, Michael C. Handbook of synthetic organic chemistry |
|---|---|
| 1. Verfasser: | |
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Hoboken, N.J.
Wiley-Interscience
2007
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Zusammenfassung: | "A thorough, accessible reference for organic chemists, laboratory technicians, or students, this guide merits a prominent place in every lab. It's also a great textbook for upper-level undergraduate and graduate students studying organic chemistry, medicine, pharmaceuticals, and polymers."--BOOK JACKET. |
| Beschreibung: | XIII, 198 S. Ill., graph. Darst. |
| ISBN: | 9780470107072 |
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| 100 | 1 | |a Pirrung, Michael C. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a The synthetic organic chemist's companion |c Michael C. Pirrung |
| 264 | 1 | |a Hoboken, N.J. |b Wiley-Interscience |c 2007 | |
| 300 | |a XIII, 198 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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Datensatz im Suchindex
| _version_ | 1804136667752169472 |
|---|---|
| adam_text | CONTENT!
PREFACE
xi
ACKNOWLEt
ЮМЕ
NTS
* » *
XIII
CHAPTER
1
SEARCHING THE LITERATUME
1
U
Commercial Availability
1
1.2
Literature Preparations
3
CHAPTER
2
REAGENTS
7
2.1
Short Path Distillation
7
2,2
Ampules
11
23
Reagent Solutions
12
2.4
Titration
13
2.5
Reagent Storage
16
2.6
Subtle Reagent Variations
• 17
2.7
Dangerous Reagents
18
2.8
Reagent Properties
18
CHAPTER
3
GASES
19
3.1
Lecture Bottles
19
3.2
Tanks or Cylinders
19
3.3
Gas Safety
22
CHAPTER
4
REACTIONS ON A SMALL
SCALE—
1
TO
25
mmol
23
4.1
Reaction Flasks
24
4.2
Stirring
26
VI
CONTENTS
4.3
Glass Joints
29
4.4
Inert Atmosphere-
30
4.5
Apparatus for Addition
36
4.6
Condensers
41
4.7
Other Equipment and
Considérations
43
CHAPTER
5
TEMPERATURE CONTROL
4$
51
Heating
45
5,2
Cooling
49
CHAPTER
6
SOLVENTS
53
6.1
Selection
53
6.2
Purity
53
6,3
Degassing
58
6.4
Ammonia
60
CHAPTER
7
THE RESEARCH NOTEBOOK
CHAPTER
і
CONDUCTING THE REACTION
ITSELF
8.1
Reagents Supplied as Dispersions
69
.8.2
Azeotropic Drying
69
8.3
Stoicbiometry
70
S.4
Syringe and Inert Atmosphere
Techniques
74
8.5
General.
Procedute
for Transfer of
Materials
by Syringe
75
8.6
Addition
77
8,7
Special Techniques
79
8:7.1
Water Removal
79
8.7.2
Reactions above
.Atmospheric Pressure
81
8.7.3
Reagent Gases
83
8.7.4
Ultrásonicatioxi
86
■CHAPTER
9
CONTENTS
VII
8.8
Quenching
86
8.9
Specialized Reagents
87
8.9.1
Diazomethane
87
8.9,2
Lithium Aluminum
Hydride
89
8.9.3
Hydrogen Peroxide
89
8.10
Reaction Time
versas
Purification
Time
91
FOLLOWING THE REACTION
93
9.1
Thin Layer Chromatography
(TLC)
93
9.1.1
Cutting. Glass
TLC
Plates
94
9.1.2
Spotting
TLC
Plates
94
9.13
Eluting
TLC
Plates
96
9.14
Visualizing
TLC
Plates
98
9.2
Gas Chromatography (GC)
103
9.3
High-Pressure Liquid
Chromatography (H.PLC)
104
9.4
NMR Spectroscopy
105
WORKING UP REACTIONS
107
10.1
Solvent Extraction
108
10.2
Drying Organic Solutions
112
10.3
Specialized Workups
114
1.0.3,1
.Reactions Producing
Triphenylphosphine Oxide
.114
10.3.2
Reactions Involving Boron
Compounds
114
10.3.3
Reactions Involving Copper
Salts
114
10.3.4
Reactions Involving
Aluminum Reagents
114
10.3.5
Reactions Involving Tin
Reagents
115
F.VA
.PORATION
117
Vill
CONTENTS
CHAPTER
12
VACUUM SYSTEMS
12.1
Vacuum Sources
12.2
Vacuum Manifolds
12.3
Vacuum. Gauges
123
123
124
126
CHAPTER
13
PURIFICATION OF PRODUCTS
131
13.1
Distillation
131
13.2
Silica
Gei
Chromatography
132
13.3
Flash Column Chromatography
133
13.4
Gradients
136
13.5
Special Absorbents
136
13.5.1
Triethylamine-Treated
Silica Gel
136
13.5.2
Oxalic Acid-Coated Silica
Gel
136
13.5.3
Silver Nitrate-Impregnated.
Silica Gel
137
13.5.4
Other Sorbents
138
13.6
Preparative Gas Chromatography
139
CHAPTER
14
METHODS
FÖR
STRUCTURE
ELUCIDATION
141
14.1
Nuclear Magnetic Resonance
Spectroscopy (NMR)
141
14.2
Infrared Spectroscopy
(IR)
146
14.3
Ultraviolet Spectroscopy (UV)
147
14.4
Combustion Analysis
149
14,5
Mass Spectrometry
1.50
14.6
Crystallography
151
CHAPTER
15
CLE.
¿NING
UP AFTER THE
REACTION
153
CONTENTS
¡χ
chapter;» specific examples
155
16.1
The Experimental
Î55
16.2
The Org.
Syn.
Prep
155
16.3
Comparison
, 156
CHAPTER
17
STRATEGIES FOR REACTION
OPTIMIZATION
■ 157
APPENDICES
1
NMR SPECTRAL DATA OF COMMON
CONTAMINANTS
OF ORGANIC REACTION
PRODUCTS
■ ig!
2
SYNTHETIC SOLVENT SELECTION CHART
169
3
RECIPES FOR
TLC
STAINS
■■
m
4
MIXOTROPIC SERIES
173
5
STUCK JOINTS
.
І75
6
ACIDITIES OF ORGANIC FUNCTIONAL
GROUPS 177
7
ACIDITIES OF ORGANIC
FU
NCTION
AL
GROUPS IN DMSO Igj
Ш
WEE RESOURCES FOE SYNTHETIC
CHEMISTRY lg5
BIBLIOGRAPHY
187
INDEX 189
|
| adam_txt |
CONTENT!
PREFACE
xi
ACKNOWLEt
ЮМЕ
NTS
* » *
XIII
CHAPTER
1
SEARCHING THE LITERATUME
1
U
Commercial Availability
1
1.2
Literature Preparations
3
CHAPTER
2
REAGENTS
7
2.1
Short Path Distillation
7
2,2
Ampules
11
23
Reagent Solutions
12
2.4
Titration
13
2.5
Reagent Storage
16
2.6
Subtle Reagent Variations
• 17
2.7
Dangerous Reagents
18
2.8
Reagent Properties
18
CHAPTER
3
GASES
19
3.1
Lecture Bottles
19
3.2
Tanks or Cylinders
19
3.3
Gas Safety
22
CHAPTER
4
REACTIONS ON A SMALL
SCALE—
1
TO
25
mmol
23
4.1
Reaction Flasks
24
4.2
Stirring
26
VI
CONTENTS
4.3
Glass Joints
29
4.4
Inert Atmosphere-
30
4.5
Apparatus for Addition
36
4.6
Condensers
41
4.7
Other Equipment and
Considérations
43
CHAPTER
5
TEMPERATURE CONTROL
4$
51
Heating
45
5,2
Cooling
49
CHAPTER
6
SOLVENTS
53
6.1
Selection
53
6.2
Purity
53
6,3
Degassing
58
6.4
Ammonia
60
CHAPTER
7
THE RESEARCH NOTEBOOK
CHAPTER
і
CONDUCTING THE REACTION
ITSELF
8.1
Reagents Supplied as Dispersions
69
.8.2
Azeotropic Drying
69
8.3
Stoicbiometry
70
S.4
Syringe and Inert Atmosphere
Techniques
74
8.5
General.
Procedute
for Transfer of
Materials
by Syringe
75
8.6
Addition
77
8,7
Special Techniques
79
8:7.1
Water Removal
79
8.7.2
Reactions above
.Atmospheric Pressure
81
8.7.3
Reagent Gases
83
8.7.4
Ultrásonicatioxi
86
■CHAPTER
9
CONTENTS
VII
8.8
Quenching
86
8.9
Specialized Reagents
87
8.9.1
Diazomethane
87
8.9,2
Lithium Aluminum
Hydride
89
8.9.3
Hydrogen Peroxide
89
8.10
Reaction Time
versas
Purification
Time
91
FOLLOWING THE REACTION
93
9.1
Thin Layer Chromatography
(TLC)
93
9.1.1
Cutting. Glass
TLC
Plates
94
9.1.2 '
Spotting
TLC
Plates
94
9.13
Eluting
TLC
Plates
96
9.14
Visualizing
TLC
Plates
98
9.2
Gas Chromatography (GC)
103
9.3
High-Pressure Liquid
Chromatography (H.PLC)
' 104
9.4
NMR Spectroscopy
105
WORKING UP REACTIONS
107
10.1
Solvent Extraction
108
10.2
Drying Organic Solutions
112
10.3
Specialized Workups
114
1.0.3,1
.Reactions Producing
Triphenylphosphine Oxide
.114
10.3.2
Reactions Involving Boron
Compounds
114
10.3.3
Reactions Involving Copper
Salts
114
10.3.4
Reactions Involving
Aluminum Reagents
114
10.3.5
Reactions Involving Tin
Reagents
115
F.VA
.PORATION
117
Vill
CONTENTS
CHAPTER
12
VACUUM SYSTEMS
12.1
Vacuum Sources
12.2
Vacuum Manifolds
12.3
Vacuum. Gauges
123
123
124
126
CHAPTER
13
PURIFICATION OF PRODUCTS
131
13.1
Distillation
131
13.2
Silica
Gei
Chromatography
132
13.3
Flash Column Chromatography
133
13.4
Gradients
136
13.5
Special Absorbents
136
13.5.1
Triethylamine-Treated
Silica Gel
136
13.5.2
Oxalic Acid-Coated Silica
Gel
136
13.5.3
Silver Nitrate-Impregnated.
Silica Gel
137
13.5.4
Other Sorbents
138
13.6
Preparative Gas Chromatography
139
CHAPTER
14
METHODS
FÖR
STRUCTURE
ELUCIDATION
141
14.1
Nuclear Magnetic Resonance
Spectroscopy (NMR)
141
14.2
Infrared Spectroscopy
(IR)
146
14.3
Ultraviolet Spectroscopy (UV)
147
14.4
Combustion Analysis
149
14,5
Mass Spectrometry
1.50
14.6
Crystallography
151
CHAPTER
15
CLE.
¿NING
UP AFTER THE
REACTION
153
CONTENTS
¡χ
chapter;» specific examples
155
16.1
The Experimental
Î55
16.2
The Org.
Syn.
Prep
155
16.3
Comparison
, 156
CHAPTER
17
STRATEGIES FOR REACTION
OPTIMIZATION
■ 157
APPENDICES
1
NMR SPECTRAL DATA OF COMMON
CONTAMINANTS
OF ORGANIC REACTION
PRODUCTS
■ ig!
2
SYNTHETIC SOLVENT SELECTION CHART
169
3
RECIPES FOR
TLC
STAINS
■■
m
4
MIXOTROPIC SERIES
173
5
STUCK JOINTS
.
І75
6
ACIDITIES OF ORGANIC FUNCTIONAL
GROUPS 177
7
ACIDITIES OF ORGANIC
FU
NCTION
AL
GROUPS IN DMSO Igj
Ш
WEE RESOURCES FOE SYNTHETIC
CHEMISTRY lg5
BIBLIOGRAPHY
187
INDEX 189 |
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| index_date | 2024-07-02T18:13:17Z |
| indexdate | 2024-07-09T21:00:03Z |
| institution | BVB |
| isbn | 9780470107072 |
| language | English |
| lccn | 2007011296 |
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| owner | DE-703 DE-91G DE-BY-TUM DE-384 DE-19 DE-BY-UBM DE-29T DE-11 |
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| physical | XIII, 198 S. Ill., graph. Darst. |
| publishDate | 2007 |
| publishDateSearch | 2007 |
| publishDateSort | 2007 |
| publisher | Wiley-Interscience |
| record_format | marc |
| spelling | Pirrung, Michael C. Verfasser aut The synthetic organic chemist's companion Michael C. Pirrung Hoboken, N.J. Wiley-Interscience 2007 XIII, 198 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier "A thorough, accessible reference for organic chemists, laboratory technicians, or students, this guide merits a prominent place in every lab. It's also a great textbook for upper-level undergraduate and graduate students studying organic chemistry, medicine, pharmaceuticals, and polymers."--BOOK JACKET. Chemische reacties gtt Gassen gtt Organische chemie gtt Organische verbindingen gtt Reagentia gtt Synthese (chemie) gtt Zuiveringstechnieken gtt Organic compounds Synthesis Organische Synthese (DE-588)4075695-6 gnd rswk-swf (DE-588)4151278-9 Einführung gnd-content Organische Synthese (DE-588)4075695-6 s DE-604 Gefolgt von Pirrung, Michael C. Handbook of synthetic organic chemistry Second edition Amsterdam: Academic Press, 2017 (DE-604)BV044213101 Digitalisierung UB Augsburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015756638&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Pirrung, Michael C. The synthetic organic chemist's companion Chemische reacties gtt Gassen gtt Organische chemie gtt Organische verbindingen gtt Reagentia gtt Synthese (chemie) gtt Zuiveringstechnieken gtt Organic compounds Synthesis Organische Synthese (DE-588)4075695-6 gnd |
| subject_GND | (DE-588)4075695-6 (DE-588)4151278-9 |
| title | The synthetic organic chemist's companion |
| title_auth | The synthetic organic chemist's companion |
| title_exact_search | The synthetic organic chemist's companion |
| title_exact_search_txtP | The synthetic organic chemist's companion |
| title_full | The synthetic organic chemist's companion Michael C. Pirrung |
| title_fullStr | The synthetic organic chemist's companion Michael C. Pirrung |
| title_full_unstemmed | The synthetic organic chemist's companion Michael C. Pirrung |
| title_new | Pirrung, Michael C. Handbook of synthetic organic chemistry |
| title_short | The synthetic organic chemist's companion |
| title_sort | the synthetic organic chemist s companion |
| topic | Chemische reacties gtt Gassen gtt Organische chemie gtt Organische verbindingen gtt Reagentia gtt Synthese (chemie) gtt Zuiveringstechnieken gtt Organic compounds Synthesis Organische Synthese (DE-588)4075695-6 gnd |
| topic_facet | Chemische reacties Gassen Organische chemie Organische verbindingen Reagentia Synthese (chemie) Zuiveringstechnieken Organic compounds Synthesis Organische Synthese Einführung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015756638&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT pirrungmichaelc thesyntheticorganicchemistscompanion |