Polyelectrolytes and nanoparticles: with 6 tables
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Berlin [u.a.]
Springer
2007
|
| Series: | Springer laboratory manuals in polymer science
|
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XVII, 105 S. Ill., graph. Darst. 235 mm x 155 mm |
| ISBN: | 9783540463818 354046381X |
Staff View
MARC
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| 650 | 4 | |a Nanoparticles | |
| 650 | 4 | |a Polyelectrolytes | |
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Table of Contents
1 INTRODUCTION AND OBJECTIVE 1
2 POLYELECTROLYTES 5
2.1 Macromolecular Characterization of Polyelectrolytes 5
2.1.1 Chromatography 5
2.1.2 Osmometry 6
2.1.3 Light Scattering 6
2.1.4 Ultracentrifugation 9
2.1.5 Viscometry 10
2.2 Electrochemical Characterization of Polyelectrolytes 12
2.2.1 Potentiometry 12
2.2.1.1 Acidity Constants 14
2.2.1.2 Counterion Activity Coefficients 20
2.2.2 Spectroscopy 22
2.2.2.1 NMR Spectroscopy 22
2.2.2.2 UV/VIS Spectroscopy 23
2.3 Polyelectrolyte Complex Formation 24
2.3.1 Polyelectrolyte Complex Formation
with Oppositely Charged Surfactants 25
2.3.1.1 Polyelectrolyte Complex Formation
below the Critical Micellization Concentration
of the Surfactant 26
2.3.1.1.1 Investigation Methods 26
2.3.1.1.2 Binding Isotherms
and Theoretical Treatments 28
2.3.1.1.3 The Nature of Interactions 32
2.3.1.1.4 Polyelectroly te Surfactant
Complexes in the Gel Phase 34
2.3.1.2 Polyelectrolyte Complex Formation
above the Critical Micellization Concentration
of the Surfactant 34
2.3.1.2.1 Investigation Methods 35
2.3.1.2.2 Polyelectrolyte Surfactant
Complexes in the Solid State 36
XVI Table of Contents
2.3.2 Polyelectrolyte Complex Formation
with Oppositely Charged Polyelectrolytes 36
2.3.2.1 Diluted Polyanion Polycation Systems
(Water Soluble Polyelectrolyte Complexes) 38
2.3.2.1.1 Theoretical Treatments 39
2.3.2.2 Semidiluted Polyanion Polycation Systems
(Turbid Polyelectrolyte Complexes) 41
2.3.2.2.1 Aggregation Mechanism 43
2.3.2.3 Concentrated Polyanion Polycation Systems. 44
2.3.2.3.1 Macroscopic Phase Separation 44
2.3.2.3.2 Homogeneous Systems 45
3 NANOPARTICLES AND POLYELECTROLYTES 47
3.1 Nanoparticle Formation by Nucleation Processes 47
3.1.1 Free Energy and Supersaturation 47
3.1.2 The Nucleation Process 49
3.1.3 Nanopartides Produced by Nucleation Processes 50
3.1.3.1 Colloidal Gold 51
3.1.3.1.1 Reduction by Low Molecular Salts . 51
3.1.3.1.2 Photolytic Reduction 51
3.1.3.2 Polyelectrolytes as Stabilizing Agents 52
3.1.3.3 Polyelectrolytes
as Reducing and Stabilizing Agents 54
3.2 Nanoparticle Formation in Template Phases 57
3.2.1 Miniemulsions as Templates 59
3.2.2 Microemulsions as Templates 60
3.2.2.1 Recovery of Nanopartides 63
3.2.2.2 Polyelectrolyte Modified Microemulsions
as Templates 64
3.2.3 Block Copolymers as Templates 69
4 CHARACTERIZATION
OF POLYELECTROLYTE MODIFIED NANOPARTICLES 73
4.1 Particle Charge 73
4.1.1 Zeta Potential 75
4.1.1.1 Charged Particles in the Electrical Field 76
4.1.2 Methods for Zeta Potential Determination 78
4.1.2.1 Electrophoretic Light Scattering 78
4.1.2.2 Acoustophoresis 79
4.1.2.3 Streaming Potential Measurements 83
4.2 Particle Size 85
4.2.1 Dynamic Light Scattering 85
4.2.2 Electron Microscopy 87
4.2.2.1 Transmission Electron Microscope 88
4.2.2.2 Preparation of Specimen Support Films 89
Table of Contents XVII
4.2.2.3 Preparation of Suspensions 90
4.2.2.4 Preparation of Bulk Material 90
4.2.2.5 Preparation of Microemulsions 91
5 FIELDS OF APPLICATION 93
6 REFERENCES 97
SUBJECT INDEX 103 |
| adam_txt |
Table of Contents
1 INTRODUCTION AND OBJECTIVE 1
2 POLYELECTROLYTES 5
2.1 Macromolecular Characterization of Polyelectrolytes 5
2.1.1 Chromatography 5
2.1.2 Osmometry 6
2.1.3 Light Scattering 6
2.1.4 Ultracentrifugation 9
2.1.5 Viscometry 10
2.2 Electrochemical Characterization of Polyelectrolytes 12
2.2.1 Potentiometry 12
2.2.1.1 Acidity Constants 14
2.2.1.2 Counterion Activity Coefficients 20
2.2.2 Spectroscopy 22
2.2.2.1 NMR Spectroscopy 22
2.2.2.2 UV/VIS Spectroscopy 23
2.3 Polyelectrolyte Complex Formation 24
2.3.1 Polyelectrolyte Complex Formation
with Oppositely Charged Surfactants 25
2.3.1.1 Polyelectrolyte Complex Formation
below the Critical Micellization Concentration
of the Surfactant 26
2.3.1.1.1 Investigation Methods 26
2.3.1.1.2 Binding Isotherms
and Theoretical Treatments 28
2.3.1.1.3 The Nature of Interactions 32
2.3.1.1.4 Polyelectroly te Surfactant
Complexes in the Gel Phase 34
2.3.1.2 Polyelectrolyte Complex Formation
above the Critical Micellization Concentration
of the Surfactant 34
2.3.1.2.1 Investigation Methods 35
2.3.1.2.2 Polyelectrolyte Surfactant
Complexes in the Solid State 36
XVI Table of Contents
2.3.2 Polyelectrolyte Complex Formation
with Oppositely Charged Polyelectrolytes 36
2.3.2.1 Diluted Polyanion Polycation Systems
(Water Soluble Polyelectrolyte Complexes) 38
2.3.2.1.1 Theoretical Treatments 39
2.3.2.2 Semidiluted Polyanion Polycation Systems
(Turbid Polyelectrolyte Complexes) 41
2.3.2.2.1 Aggregation Mechanism 43
2.3.2.3 Concentrated Polyanion Polycation Systems. 44
2.3.2.3.1 Macroscopic Phase Separation 44
2.3.2.3.2 Homogeneous Systems 45
3 NANOPARTICLES AND POLYELECTROLYTES 47
3.1 Nanoparticle Formation by Nucleation Processes 47
3.1.1 Free Energy and Supersaturation 47
3.1.2 The Nucleation Process 49
3.1.3 Nanopartides Produced by Nucleation Processes 50
3.1.3.1 Colloidal Gold 51
3.1.3.1.1 Reduction by Low Molecular Salts . 51
3.1.3.1.2 Photolytic Reduction 51
3.1.3.2 Polyelectrolytes as Stabilizing Agents 52
3.1.3.3 Polyelectrolytes
as Reducing and Stabilizing Agents 54
3.2 Nanoparticle Formation in Template Phases 57
3.2.1 Miniemulsions as Templates 59
3.2.2 Microemulsions as Templates 60
3.2.2.1 Recovery of Nanopartides 63
3.2.2.2 Polyelectrolyte Modified Microemulsions
as Templates 64
3.2.3 Block Copolymers as Templates 69
4 CHARACTERIZATION
OF POLYELECTROLYTE MODIFIED NANOPARTICLES 73
4.1 Particle Charge 73
4.1.1 Zeta Potential 75
4.1.1.1 Charged Particles in the Electrical Field 76
4.1.2 Methods for Zeta Potential Determination 78
4.1.2.1 Electrophoretic Light Scattering 78
4.1.2.2 Acoustophoresis 79
4.1.2.3 Streaming Potential Measurements 83
4.2 Particle Size 85
4.2.1 Dynamic Light Scattering 85
4.2.2 Electron Microscopy 87
4.2.2.1 Transmission Electron Microscope 88
4.2.2.2 Preparation of Specimen Support Films 89
Table of Contents XVII
4.2.2.3 Preparation of Suspensions 90
4.2.2.4 Preparation of Bulk Material 90
4.2.2.5 Preparation of Microemulsions 91
5 FIELDS OF APPLICATION 93
6 REFERENCES 97
SUBJECT INDEX 103 |
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| illustrated | Illustrated |
| index_date | 2024-07-02T16:29:48Z |
| indexdate | 2024-07-20T09:10:44Z |
| institution | BVB |
| isbn | 9783540463818 354046381X |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-015434044 |
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| owner | DE-91G DE-BY-TUM DE-20 DE-703 DE-11 |
| owner_facet | DE-91G DE-BY-TUM DE-20 DE-703 DE-11 |
| physical | XVII, 105 S. Ill., graph. Darst. 235 mm x 155 mm |
| publishDate | 2007 |
| publishDateSearch | 2007 |
| publishDateSort | 2007 |
| publisher | Springer |
| record_format | marc |
| series2 | Springer laboratory manuals in polymer science |
| spelling | Kötz, Joachim Verfasser aut Polyelectrolytes and nanoparticles with 6 tables Joachim Koetz ; Sabine Kosmella Berlin [u.a.] Springer 2007 XVII, 105 S. Ill., graph. Darst. 235 mm x 155 mm txt rdacontent n rdamedia nc rdacarrier Springer laboratory manuals in polymer science Electrolytes chemistry Nanoparticles Polyelectrolytes Polymers chemistry Nanostrukturiertes Material (DE-588)4342626-8 gnd rswk-swf Nanopartikel (DE-588)4333369-2 gnd rswk-swf Polyelektrolyt (DE-588)4175165-6 gnd rswk-swf Polyelektrolyt (DE-588)4175165-6 s DE-604 Nanopartikel (DE-588)4333369-2 s Nanostrukturiertes Material (DE-588)4342626-8 s Kosmella, Sabine Verfasser aut text/html http://deposit.dnb.de/cgi-bin/dokserv?id=2850668&prov=M&dok_var=1&dok_ext=htm Inhaltstext HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015434044&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kötz, Joachim Kosmella, Sabine Polyelectrolytes and nanoparticles with 6 tables Electrolytes chemistry Nanoparticles Polyelectrolytes Polymers chemistry Nanostrukturiertes Material (DE-588)4342626-8 gnd Nanopartikel (DE-588)4333369-2 gnd Polyelektrolyt (DE-588)4175165-6 gnd |
| subject_GND | (DE-588)4342626-8 (DE-588)4333369-2 (DE-588)4175165-6 |
| title | Polyelectrolytes and nanoparticles with 6 tables |
| title_auth | Polyelectrolytes and nanoparticles with 6 tables |
| title_exact_search | Polyelectrolytes and nanoparticles with 6 tables |
| title_exact_search_txtP | Polyelectrolytes and nanoparticles with 6 tables |
| title_full | Polyelectrolytes and nanoparticles with 6 tables Joachim Koetz ; Sabine Kosmella |
| title_fullStr | Polyelectrolytes and nanoparticles with 6 tables Joachim Koetz ; Sabine Kosmella |
| title_full_unstemmed | Polyelectrolytes and nanoparticles with 6 tables Joachim Koetz ; Sabine Kosmella |
| title_short | Polyelectrolytes and nanoparticles |
| title_sort | polyelectrolytes and nanoparticles with 6 tables |
| title_sub | with 6 tables |
| topic | Electrolytes chemistry Nanoparticles Polyelectrolytes Polymers chemistry Nanostrukturiertes Material (DE-588)4342626-8 gnd Nanopartikel (DE-588)4333369-2 gnd Polyelektrolyt (DE-588)4175165-6 gnd |
| topic_facet | Electrolytes chemistry Nanoparticles Polyelectrolytes Polymers chemistry Nanostrukturiertes Material Nanopartikel Polyelektrolyt |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=2850668&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=015434044&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT kotzjoachim polyelectrolytesandnanoparticleswith6tables AT kosmellasabine polyelectrolytesandnanoparticleswith6tables |