Analytical electrochemistry:
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| Format: | Electronic eBook |
|---|---|
| Language: | English |
| Published: |
Hoboken, NJ
Wiley-VCH
2006
|
| Edition: | 3. ed. |
| Subjects: | |
| Online Access: | FRO01 TUM01 UBR01 Volltext Inhaltsverzeichnis |
| Physical Description: | 1 Online-Ressource |
| ISBN: | 0471678791 0471790303 9780471678793 9780471790303 |
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| adam_text | CONTENTS
Preface xi
Abbreviations and Symbols xiii
1 Fundamental Concepts 1
1.1 Why Electroanalysis?, 1
1.2 Faradaic Processes, 3
1.2.1 Mass Transport Controlled Reactions, 4
1.2.1.1 Potential Step Experiment, 7
1.2.1.2 Potential Sweep Experiments, 9
1.2.2 Reactions Controlled by the Rate of Electron Transfer, 12
1.2.2.1 Activated Complex Theory, 16
1.3 Electrical Double Layer, 19
1.4 Electrocapillary Effect, 23
1.5 Supplementary Reading, 25
Problems, 27
References, 28
2 Study of Electrode Reactions and Interfacial Properties 29
2.1 Cyclic Voltammetry, 29
2.1.1 Data Interpretation, 32
2.1.1.1 Reversible Systems, 32
2.1.1.2 Irreversible and Quasi reversible Systems, 34
2.1.2 Study of Reaction Mechanisms, 35
vii
yj„ CONTENTS
2.1.3 Study of Adsorption Processes, 37
2.1.4 Quantitative Applications, 41
2.2 Spectroelectrochemistry, 42 I
2.2.1 Experimental Arrangement, 43 I
2.2.2 Principles and Applications, 44 ¦
2.2.3 Electrochemiluminescence, 47
2.2.4 Optical Probing of Electrode Solution Interfaces, 48
2.3 Scanning Probe Microscopy, 49
2.3.1 Scanning Tunneling Microscopy, 50
2.3.2 Atomic Force Microscopy, 51
2.3.3 Scanning Electrochemical Microscopy, 53
2.4 Electrochemical Quartz Crystal Microbalance, 57
2.5 Impedance Spectroscopy, 58
Examples, 61
Problems, 63
References, 64
3 Controlled Potential Techniques 67
3.1 Chronoamperometry, 67
3.2 Polarography, 69
3.3 Pulse Voltammetry, 76
3.3.1 Normal Pulse Voltammetry, 76
3.3.2 Differential Pulse Voltammetry, 77
3.3.3 Square Wave Voltammetry, 80
3.3.4 Staircase Voltammetry, 82
3.4 AC Voltammetry, 84
3.5 Stripping Analysis, 85
3.5.1 Anodic Stripping Voltammetry, 86
3.5.2 Potentiometric Stripping Analysis, 89
3.5.3 Adsorptive Stripping Voltammetry and Potentiometry, 91
3.5.4 Cathodic Stripping Voltammetry, 94
3.5.5 Abrasive Stripping Voltammetry, 94
3.5.6 Applications, 94
3.6 Flow Analysis, 98
3.6.1 Principles, 98
3.6.2 Cell Design, 100
3.6.3 Mass Transport and Current Response, 103
3.6.4 Detection Modes, 105
Examples, 108
Problems, 111
References, 112
4 Practical Considerations 115
4.1 Electrochemical Cells, 115
4.2 Solvents and Supporting Electrolytes, 117
CONTENTS jx
4.3 Oxygen Removal, 118
4.4 Instrumentation, 119
4.5 Working Electrodes, 123
4.5.1 Mercury Electrodes, 123
4.5.2 Solid Electrodes, 127
4.5.2.1 Rotating Disk and Rotating Ring Disk Electrodes, 128
4.5.2.2 Carbon Electrodes, 130
4.5.2.2.1 Glassy Carbon Electrodes, 131
4.5.2.2.2 Carbon Paste Electrodes, 131
4.5.2.2.3 Carbon Fiber Electrodes, 133
4.5.2.2.4 Diamond Electrodes, 133
4.5.2.3 Metal Electrodes, 134
4.5.3 Chemically Modified Electrodes, 136
4.5.3.1 Self Assembled Monolayers, 136
4.5.3.2 Carbon Nanotube Modified Electrodes, 139
4.5.3.3 Sol gel Encapsulation of Reactive Species, 139
4.5.3.4 Electrocatalytically Modified Electrodes, 140
4.5.3.5 Preconcentrating Electrodes, 141
4.5.3.6 Permselective Coatings, 143
4.5.3.7 Conducting Polymers, 146
4.5.4 Microelectrodes, 149
4.5.4.1 Diffusion at Microelectrodes, 151
4.5.4.2 Microelectrode Configurations, 152
4.5.4.3 Composite Electrodes, 154
Examples, 158
Problems, 158
References, 159
5 Potentiometry 165
5.1 Principles of Potentiometric Measurements, 165
5.2 Ion Selective Electrodes, 173
5.2.1 Glass Electrodes, 173
5.2.1.1 pH Electrodes, 173
5.2.1.2 Glass Electrodes for Other Cations, 177
5.2.2 Liquid Membrane Electrodes, 177
5.2.2.1 Ion Exchanger Electrodes, 179
5.2.2.2 Neutral Carrier Electrodes, 182
5.2.3 Solid State Electrodes, 185
5.2.4 Coated Wire Electrodes and Solid State Electrodes Wjthout an
Internal Filling Solution, 188
5.3 On line, On site, and In Vivo Potentiometric Measurements, 190
Examples, 194
Problems, 196
References, 197
6 Electrochemical Sensors 201
6.1 Electrochemical Biosensors, 202
6.1.1 Enzyme Based Electrodes, 202
6.1.1.1 Practical and Theoretical Considerations, 202
6.1.1.2 Enzyme Electrodes of Analytical Significance, 208
6.1.1.2.1 Glucose Sensors, 208
6.1.1.2.2 Ethanol Electrodes, 212
6.1.1.2.3 Urea Electrodes, 213
6.1.1.2.4 Toxin (Enzyme Inhibition) Biosensors, 215
6.1.1.3 Tissue and Bacteria Electrodes, 215
6.1.2 Affinity Biosensors, 216
6.1.2.1 Immunosensors, 216
6.1.2.2 DNA Hybridization Biosensors, 218
6.1.2.2.1 Background and Principles, 218
6.1.2.2.2 Electrical Transduction of DNA
Hybridization, 219
6.1.2.2.3 Other Electrochemical DNA
Biosensors, 221
6.1.2.3 Receptor Based Sensors, 222
6.1.2.4 Electrochemical Sensors Based on Molecularly
Imprinted Polymers, 224
6.2 Gas Sensors, 224
6.2.1 Carbon Dioxide Sensors, 225
6.2.2 Oxygen Electrodes, 226
6.3 Solid State Devices, 227
6.3.1 Ion Selective Field Effect Transistors, 227
6.3.2 Microfabrication of Solid State Sensor Assemblies, 229
6.3.3 Microfabrication Techniques, 229
6.3.4 Micromachined Analytical Microsystems, 232
6.4 Sensor Arrays, 234
Examples, 237
Problems, 238
References, 239
Index 245
|
| adam_txt |
CONTENTS
Preface xi
Abbreviations and Symbols xiii
1 Fundamental Concepts 1
1.1 Why Electroanalysis?, 1
1.2 Faradaic Processes, 3
1.2.1 Mass Transport Controlled Reactions, 4
1.2.1.1 Potential Step Experiment, 7
1.2.1.2 Potential Sweep Experiments, 9
1.2.2 Reactions Controlled by the Rate of Electron Transfer, 12
1.2.2.1 Activated Complex Theory, 16
1.3 Electrical Double Layer, 19
1.4 Electrocapillary Effect, 23
1.5 Supplementary Reading, 25
Problems, 27
References, 28
2 Study of Electrode Reactions and Interfacial Properties 29
2.1 Cyclic Voltammetry, 29
2.1.1 Data Interpretation, 32
2.1.1.1 Reversible Systems, 32
2.1.1.2 Irreversible and Quasi reversible Systems, 34
2.1.2 Study of Reaction Mechanisms, 35
vii
yj„ CONTENTS
2.1.3 Study of Adsorption Processes, 37
2.1.4 Quantitative Applications, 41
2.2 Spectroelectrochemistry, 42 I
2.2.1 Experimental Arrangement, 43 I
2.2.2 Principles and Applications, 44 ¦
2.2.3 Electrochemiluminescence, 47
2.2.4 Optical Probing of Electrode Solution Interfaces, 48
2.3 Scanning Probe Microscopy, 49
2.3.1 Scanning Tunneling Microscopy, 50
2.3.2 Atomic Force Microscopy, 51
2.3.3 Scanning Electrochemical Microscopy, 53
2.4 Electrochemical Quartz Crystal Microbalance, 57
2.5 Impedance Spectroscopy, 58
Examples, 61
Problems, 63
References, 64
3 Controlled Potential Techniques 67
3.1 Chronoamperometry, 67
3.2 Polarography, 69
3.3 Pulse Voltammetry, 76
3.3.1 Normal Pulse Voltammetry, 76
3.3.2 Differential Pulse Voltammetry, 77
3.3.3 Square Wave Voltammetry, 80
3.3.4 Staircase Voltammetry, 82
3.4 AC Voltammetry, 84
3.5 Stripping Analysis, 85
3.5.1 Anodic Stripping Voltammetry, 86
3.5.2 Potentiometric Stripping Analysis, 89
3.5.3 Adsorptive Stripping Voltammetry and Potentiometry, 91
3.5.4 Cathodic Stripping Voltammetry, 94
3.5.5 Abrasive Stripping Voltammetry, 94
3.5.6 Applications, 94
3.6 Flow Analysis, 98
3.6.1 Principles, 98
3.6.2 Cell Design, 100
3.6.3 Mass Transport and Current Response, 103
3.6.4 Detection Modes, 105
Examples, 108
Problems, 111
References, 112
4 Practical Considerations 115
4.1 Electrochemical Cells, 115
4.2 Solvents and Supporting Electrolytes, 117
CONTENTS jx
4.3 Oxygen Removal, 118
4.4 Instrumentation, 119
4.5 Working Electrodes, 123
4.5.1 Mercury Electrodes, 123
4.5.2 Solid Electrodes, 127
4.5.2.1 Rotating Disk and Rotating Ring Disk Electrodes, 128
4.5.2.2 Carbon Electrodes, 130
4.5.2.2.1 Glassy Carbon Electrodes, 131
4.5.2.2.2 Carbon Paste Electrodes, 131
4.5.2.2.3 Carbon Fiber Electrodes, 133
4.5.2.2.4 Diamond Electrodes, 133
4.5.2.3 Metal Electrodes, 134
4.5.3 Chemically Modified Electrodes, 136
4.5.3.1 Self Assembled Monolayers, 136
4.5.3.2 Carbon Nanotube Modified Electrodes, 139
4.5.3.3 Sol gel Encapsulation of Reactive Species, 139
4.5.3.4 Electrocatalytically Modified Electrodes, 140
4.5.3.5 Preconcentrating Electrodes, 141
4.5.3.6 Permselective Coatings, 143
4.5.3.7 Conducting Polymers, 146
4.5.4 Microelectrodes, 149
4.5.4.1 Diffusion at Microelectrodes, 151
4.5.4.2 Microelectrode Configurations, 152
4.5.4.3 Composite Electrodes, 154
Examples, 158
Problems, 158
References, 159
5 Potentiometry 165
5.1 Principles of Potentiometric Measurements, 165
5.2 Ion Selective Electrodes, 173
5.2.1 Glass Electrodes, 173
5.2.1.1 pH Electrodes, 173
5.2.1.2 Glass Electrodes for Other Cations, 177
5.2.2 Liquid Membrane Electrodes, 177
5.2.2.1 Ion Exchanger Electrodes, 179
5.2.2.2 Neutral Carrier Electrodes, 182
5.2.3 Solid State Electrodes, 185
5.2.4 Coated Wire Electrodes and Solid State Electrodes Wjthout an
Internal Filling Solution, 188
5.3 On line, On site, and In Vivo Potentiometric Measurements, 190
Examples, 194
Problems, 196
References, 197
6 Electrochemical Sensors 201
6.1 Electrochemical Biosensors, 202
6.1.1 Enzyme Based Electrodes, 202
6.1.1.1 Practical and Theoretical Considerations, 202
6.1.1.2 Enzyme Electrodes of Analytical Significance, 208
6.1.1.2.1 Glucose Sensors, 208
6.1.1.2.2 Ethanol Electrodes, 212
6.1.1.2.3 Urea Electrodes, 213
6.1.1.2.4 Toxin (Enzyme Inhibition) Biosensors, 215
6.1.1.3 Tissue and Bacteria Electrodes, 215
6.1.2 Affinity Biosensors, 216
6.1.2.1 Immunosensors, 216
6.1.2.2 DNA Hybridization Biosensors, 218
6.1.2.2.1 Background and Principles, 218
6.1.2.2.2 Electrical Transduction of DNA
Hybridization, 219
6.1.2.2.3 Other Electrochemical DNA
Biosensors, 221
6.1.2.3 Receptor Based Sensors, 222
6.1.2.4 Electrochemical Sensors Based on Molecularly
Imprinted Polymers, 224
6.2 Gas Sensors, 224
6.2.1 Carbon Dioxide Sensors, 225
6.2.2 Oxygen Electrodes, 226
6.3 Solid State Devices, 227
6.3.1 Ion Selective Field Effect Transistors, 227
6.3.2 Microfabrication of Solid State Sensor Assemblies, 229
6.3.3 Microfabrication Techniques, 229
6.3.4 Micromachined Analytical Microsystems, 232
6.4 Sensor Arrays, 234
Examples, 237
Problems, 238
References, 239
Index 245 |
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| publishDateSearch | 2006 |
| publishDateSort | 2006 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Analytical electrochemistry Joseph Wang 3. ed. Hoboken, NJ Wiley-VCH 2006 1 Online-Ressource txt rdacontent c rdamedia cr rdacarrier Electrochemical analysis Elektroanalyse (DE-588)4014237-1 gnd rswk-swf Elektrochemie (DE-588)4014241-3 gnd rswk-swf Elektroanalyse (DE-588)4014237-1 s Elektrochemie (DE-588)4014241-3 s 1\p DE-604 Wang, Joseph 1948- Sonstige (DE-588)13216292X oth https://onlinelibrary.wiley.com/doi/book/10.1002/0471790303 Verlag Volltext HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014997131&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Analytical electrochemistry Electrochemical analysis Elektroanalyse (DE-588)4014237-1 gnd Elektrochemie (DE-588)4014241-3 gnd |
| subject_GND | (DE-588)4014237-1 (DE-588)4014241-3 |
| title | Analytical electrochemistry |
| title_auth | Analytical electrochemistry |
| title_exact_search | Analytical electrochemistry |
| title_exact_search_txtP | Analytical electrochemistry |
| title_full | Analytical electrochemistry Joseph Wang |
| title_fullStr | Analytical electrochemistry Joseph Wang |
| title_full_unstemmed | Analytical electrochemistry Joseph Wang |
| title_short | Analytical electrochemistry |
| title_sort | analytical electrochemistry |
| topic | Electrochemical analysis Elektroanalyse (DE-588)4014237-1 gnd Elektrochemie (DE-588)4014241-3 gnd |
| topic_facet | Electrochemical analysis Elektroanalyse Elektrochemie |
| url | https://onlinelibrary.wiley.com/doi/book/10.1002/0471790303 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014997131&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT wangjoseph analyticalelectrochemistry |