X-Ray crystallography of biomacromolecules: a practical guide
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Weinheim
WILEY-VCH
2007
|
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XIII, 304 S. Ill., graph. Darst. 240 mm x 170 mm |
| ISBN: | 9783527313969 3527313966 |
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Record in the Search Index
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VII
Contents
Preface
Part I
Principles and Methods
1
1.1
1.2
1.2.1
1.2.1.1
1.2.1.2
1.2.2 pH
1.2.3
1.2.4
1.3
1.3.1
1.3.2
1.3.3
1.4
1.5
References
2
2.1
2.1.1
2.1.2
2.1.3
2.2
2.2.1
2.2.2
2.2.3
2.2.4
2.3
X-Ray Crystallography of Biomacromolecuks.
Copyright
ISBN:
VIII Contents
2.3.1
2.3.2
2.3.3
2.4
2.4.1
2.4.2
References
3
3.1
3.1.1
3.1.2
3.2
3.2.1
3.2.2
3.2.3
3.2.4
3.2.5
3.2.5.1
3.2.5.2
3.2.6
3.2.7
3.2.8
3.2.9
3.2.10
3.2.11
3.2.12
3.2.13
References
4
4.1
4.2
with Normal Flat Detector
4.3
4.4
4.5
4.6
References
5
5.1
5.1.1
5.1.2
5.1.3
Contents
5.2
5.2.1
5.2.2
5.2.3
5.2.4
5.2.5
5.2.6
5.2.7
5.3
5.3.1
5.3.2
5.4
5.4.1
5.4.2
5.4.3
and Phase Calculation
5.4.4
Data
5.5
5.5.1
5.5.2
5.5.3
5.5.3.1
5.5.3.2
5.5.3.3
5.5.4
References
6
and Phase Combination
6.1
6.2
6.3
6.4
6.5
6.6
6.7
6.8
References
7
7.1
7.2
7.2.1
7.2.2
X
7.2.3
7.2.4
7.2.5
7.2.6
7.3
7.3.1
7.3.2
7.3.2.
1
7.3.2.
2
7.3.2.
3
7.3.2.
3.1
7.3.2.
3.2
7.3.2.
3.3
7.3.3
Constraints and Restraints in Refinement
Refinement by Simulated Annealing
The Maximum Likelihood Method
Refinement at Atomic Resolution
Verification and Accuracy of Structure Determination
Free R-Factor as a Tool for Cross-Validation
in Structure Determination
Determination of Coordinate Uncertainty
Unrestrained Least-Squares Refinement
Restrained Least-Squares Refinement
Rough Estimation of Coordinate Uncertainties
Luzzati Plot
ffA-Plot
The Diffraction-Component Precision Index
Validation of the Geometric and Stereochemical Parameters
of the Structural Model
7.3.4
Experimental Data
7.3.5
References
8
Crystal Structure Determination of the Time-Course of Reactions
and of Unstable Species
8.1
Introduction
8.2
Triggering Methods
8.2.1
Photolysis
8.2.2
Diffusion
8.2.3
Radiolysis
8.3
Trapping Methods
8.3.1
Physical Trapping
8.3.2
Chemical Trapping
8.4
Laue
8.4.1
Principles of the
8.4.2
Advantages and Disadvantages
8.4.3
Practical Aspects
References
9
Structural Genomics
9.1
Introduction
9.2
Target Selection
9.3
Production of
9.3.1
Introduction
9.3.2
Engineering an Appropriate Expression Construct
9.3.3
Expression Systems
9.3.3.1
E. coli
Contents
9.3.3.2 Eukaryotic Expression Systems 222
9.3.3.2.1
9.3.3.2.2 Baculovirus 213
9.3.3.2.3
9.3.4 Protein
9.3.4.1
9.3.4.2
9.3.5
9.4
References
Part II Practical Examples
Introductory Remarks
10
10.1
and Reflection Integration
10.2
10.3
References
11
11.1
11.2
11.3
References
12 MIRAS
12.1
References
13
13.1
References
14
for 4-BUDH
14.1
14.2
References
XII Contents
15 Model Building
15.1
to the Computer Graphics Modeling Program "O"
15.2
and New SHARP-Phasing for 4-BUDH
15.3
References
Subject Index |
| adam_txt |
VII
Contents
Preface
Part I
Principles and Methods
1
1.1
1.2
1.2.1
1.2.1.1
1.2.1.2
1.2.2 pH
1.2.3
1.2.4
1.3
1.3.1
1.3.2
1.3.3
1.4
1.5
References
2
2.1
2.1.1
2.1.2
2.1.3
2.2
2.2.1
2.2.2
2.2.3
2.2.4
2.3
X-Ray Crystallography of Biomacromolecuks.
Copyright
ISBN:
VIII Contents
2.3.1
2.3.2
2.3.3
2.4
2.4.1
2.4.2
References
3
3.1
3.1.1
3.1.2
3.2
3.2.1
3.2.2
3.2.3
3.2.4
3.2.5
3.2.5.1
3.2.5.2
3.2.6
3.2.7
3.2.8
3.2.9
3.2.10
3.2.11
3.2.12
3.2.13
References
4
4.1
4.2
with Normal Flat Detector
4.3
4.4
4.5
4.6
References
5
5.1
5.1.1
5.1.2
5.1.3
Contents
5.2
5.2.1
5.2.2
5.2.3
5.2.4
5.2.5
5.2.6
5.2.7
5.3
5.3.1
5.3.2
5.4
5.4.1
5.4.2
5.4.3
and Phase Calculation
5.4.4
Data
5.5
5.5.1
5.5.2
5.5.3
5.5.3.1
5.5.3.2
5.5.3.3
5.5.4
References
6
and Phase Combination
6.1
6.2
6.3
6.4
6.5
6.6
6.7
6.8
References
7
7.1
7.2
7.2.1
7.2.2
X
7.2.3
7.2.4
7.2.5
7.2.6
7.3
7.3.1
7.3.2
7.3.2.
1
7.3.2.
2
7.3.2.
3
7.3.2.
3.1
7.3.2.
3.2
7.3.2.
3.3
7.3.3
Constraints and Restraints in Refinement
Refinement by Simulated Annealing
The Maximum Likelihood Method
Refinement at Atomic Resolution
Verification and Accuracy of Structure Determination
Free R-Factor as a Tool for Cross-Validation
in Structure Determination
Determination of Coordinate Uncertainty
Unrestrained Least-Squares Refinement
Restrained Least-Squares Refinement
Rough Estimation of Coordinate Uncertainties
Luzzati Plot
ffA-Plot
The Diffraction-Component Precision Index
Validation of the Geometric and Stereochemical Parameters
of the Structural Model
7.3.4
Experimental Data
7.3.5
References
8
Crystal Structure Determination of the Time-Course of Reactions
and of Unstable Species
8.1
Introduction
8.2
Triggering Methods
8.2.1
Photolysis
8.2.2
Diffusion
8.2.3
Radiolysis
8.3
Trapping Methods
8.3.1
Physical Trapping
8.3.2
Chemical Trapping
8.4
Laue
8.4.1
Principles of the
8.4.2
Advantages and Disadvantages
8.4.3
Practical Aspects
References
9
Structural Genomics
9.1
Introduction
9.2
Target Selection
9.3
Production of
9.3.1
Introduction
9.3.2
Engineering an Appropriate Expression Construct
9.3.3
Expression Systems
9.3.3.1
E. coli
Contents
9.3.3.2 Eukaryotic Expression Systems 222
9.3.3.2.1
9.3.3.2.2 Baculovirus 213
9.3.3.2.3
9.3.4 Protein
9.3.4.1
9.3.4.2
9.3.5
9.4
References
Part II Practical Examples
Introductory Remarks
10
10.1
and Reflection Integration
10.2
10.3
References
11
11.1
11.2
11.3
References
12 MIRAS
12.1
References
13
13.1
References
14
for 4-BUDH
14.1
14.2
References
XII Contents
15 Model Building
15.1
to the Computer Graphics Modeling Program "O"
15.2
and New SHARP-Phasing for 4-BUDH
15.3
References
Subject Index |
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| index_date | 2024-07-02T15:26:16Z |
| indexdate | 2024-07-20T09:07:36Z |
| institution | BVB |
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| spelling | Messerschmidt, Albrecht Verfasser aut X-Ray crystallography of biomacromolecules a practical guide Albrecht Messerschmidt Weinheim WILEY-VCH 2007 XIII, 304 S. Ill., graph. Darst. 240 mm x 170 mm txt rdacontent n rdamedia nc rdacarrier Biomolecules X-ray crystallography Proteine (DE-588)4076388-2 gnd rswk-swf Kristallstruktur (DE-588)4136176-3 gnd rswk-swf Röntgenstrukturanalyse (DE-588)4137203-7 gnd rswk-swf Proteine (DE-588)4076388-2 s Kristallstruktur (DE-588)4136176-3 s Röntgenstrukturanalyse (DE-588)4137203-7 s DE-604 text/html http://deposit.dnb.de/cgi-bin/dokserv?id=2843886&prov=M&dok_var=1&dok_ext=htm Inhaltstext Digitalisierung UB Regensburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014943991&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Messerschmidt, Albrecht X-Ray crystallography of biomacromolecules a practical guide Biomolecules X-ray crystallography Proteine (DE-588)4076388-2 gnd Kristallstruktur (DE-588)4136176-3 gnd Röntgenstrukturanalyse (DE-588)4137203-7 gnd |
| subject_GND | (DE-588)4076388-2 (DE-588)4136176-3 (DE-588)4137203-7 |
| title | X-Ray crystallography of biomacromolecules a practical guide |
| title_auth | X-Ray crystallography of biomacromolecules a practical guide |
| title_exact_search | X-Ray crystallography of biomacromolecules a practical guide |
| title_exact_search_txtP | X-Ray crystallography of biomacromolecules a practical guide |
| title_full | X-Ray crystallography of biomacromolecules a practical guide Albrecht Messerschmidt |
| title_fullStr | X-Ray crystallography of biomacromolecules a practical guide Albrecht Messerschmidt |
| title_full_unstemmed | X-Ray crystallography of biomacromolecules a practical guide Albrecht Messerschmidt |
| title_short | X-Ray crystallography of biomacromolecules |
| title_sort | x ray crystallography of biomacromolecules a practical guide |
| title_sub | a practical guide |
| topic | Biomolecules X-ray crystallography Proteine (DE-588)4076388-2 gnd Kristallstruktur (DE-588)4136176-3 gnd Röntgenstrukturanalyse (DE-588)4137203-7 gnd |
| topic_facet | Biomolecules X-ray crystallography Proteine Kristallstruktur Röntgenstrukturanalyse |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=2843886&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014943991&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT messerschmidtalbrecht xraycrystallographyofbiomacromoleculesapracticalguide |