NMR for physical and biological scientists:
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
New York [u.a.]
Taylor & Francis
2007
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXII, 372 S. Ill., graph. Darst. |
| ISBN: | 9780815341031 0815341032 |
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| adam_text | CONTENTS
Preface
Symbols and fundamental
1.
A semiclassical description of spectroscopy
Damped harmonics
Quantum oscillators
The spectroscopic experiment
Ensembles and coherence
Types of spectroscopy
Practical considerations in spectroscopy
Acquiring a spectrum
Resolution: the problem of line width
Line shape
Problems
2.
ensemble behavior and coupling
Nuclear and electronic spin
The quantum picture of nuclear spin
The spinning top model of nuclear spin
Spin-state populations in ensembles
Information available from NMR:
and chemical shift
Information available from NMR:
Information available from NMR:
Information available from NMR:
/-coupling time scale, decoupling experiments and exchange
decoupling
Interaction between nuclear spins and radio-frequency (RF)
E
Problems
viii Contents
3.
Interaction between nuclear spins and RF:
A single spin in the rotating frame of reference
Interaction between nuclear spins and RF:
An ensemble of spins in the rotating frame of reference
Detection of an NMR signal
Time-domain detection in the NMR experiment: the
free induction decay and quadrature detection
Digitization of the free induction decay
Fourier transformation: time-domain FID to frequency-domain
spectrum
Discrete Fourier transformation
Spectral phasing
RF pulses and pulse phase
Pulse power and off-resonance effects from RF pulses
Phase cycling: improved quadrature detection using CYCLOPS
Factors affecting spectral quality and appearance: shimming,
window functions and apodization
After the fact: window functions and zero filling
Linear prediction
Problems
References
4.
Longitudinal (Tt) relaxation and the sensitivity of the
NMR experiment
Transverse
Chemical shift and/-coupling evolution during the spin echo
Mechanisms of nuclear spin relaxation in liquids and the spectral
density function
Dipolar relaxation and the nuclear Overhauser effect
NOE
Heteronuclear
Other contributions to
spin-rotation and paramagnetic effects
Quadrapolar relaxation
Selective and nonselective Tl measurement and multi-exponential
decay of coherence
Problems
References
5.
in liquids
The classical approach: the Rloch equations of motion for
macroscopic magnetization
Classical description of a pulsed NMR experiment
A quantum mechanical description of NMR of a single spin in an
isotropie
Contents
A quantum mechanical description of NMR of coupled spins in an
isotropie
The time-dependent nuclear spin Hamiltonian operator and
solutions to the time-dependent
Problems
References
6.
NMR experiments in liquids
An ensemble of identical spins at equilibrium: an introduction to
the density matrix formalism
Expansion of the density matrix for an uncoupled spin in terms
of Cartesian angular momentum operators
Weakly coupled ensembles and the weak-coupling approximation
Single-element operators for a two-spin system
Interconversion
operator bases
Evolution of Cartesian operators under the influence of pulses,
chemical shift and /-coupling
Evolution of operators with weak/-coupling
Analysis of a simple NMR spectrum using product operators
Problems
References
7.
coherence selection
A simple two-dimensional NMR experiment
Coherence transfer in multidimensional NMR
The COSY experiment
Quadrature detection in multidimensional NMR
Axial peaks
Phase cycling and coherence order selection: the DQF-COSY
experiment
Other multiple-quantum filters in COSY
Multiple-quantum spectroscopy
Effect of n pulses on coherence
Pulsed-field gradients for coherence selection
The gradient COSY experiment
Zero-quantum filtered COSY : NOESY and incoherent transfer
Rotating frame NOEs: CAMELSPIN and ROESY
Spin-locking experiments for coherence transfer: TOCSY and
composite pulse decoupling
Problems
References
8.
Heteronuclear polarization transfer and the INEPT experiment
Refocused INEPT
Contents
Two-dimensional polarization transfer: HETCOR
Sensitive nucleus (inverse) detection of an insensitive nucleus:
the double INEPT or HSQC experiment
Multiple-quantum approaches to heteronuclear correlation:
DEPT
Gradient coherence selection in heteronuclear correlation NMR
Phase-sensitive gradient coherence selection experiments for
heteronuclear correlations
Sensitivity enhancement in gradient coherence selection experiments
Problems
References
9.
considerations for biological applications of NMR
Polarization transfer
Solvent suppression
Frequency-labeling periods and constant time NMR experiments
Shaped and selective pulses
Composite pulse decoupling and spin-locking
Dealing with very large biomolecules in solution: deuteration and
direct 13C detection
Interference patterns in heteronuclear relaxation: TROSY
Problems
References
10.
and ordered fluids
Anisotropy in NMR: chemical shielding and dipolar coupling
Resolving the solid-state NMR spectrum: magic angle spinning
(MAS) and high-power XH decoupling
Cross-polarization for signal enhancement of dilute spins and
spin—spin correlations
Selective
rotational resonance, RFDR, and
Heteronuclear two-dimensional techniques in solid-state NMR
Solid-state NMR using oriented samples: PISEMA
Bringing a little order to solution NMR: residual dipolar couplings
and CSA in ordered fluids
Analysis of residual dipolar couplings
Problems
References
11.
Time scales of molecular motion, dynamic processes and relaxation
The spectral density revisited
Experimental measurement of heteronuclear relaxation parameters
in proteins
Model-free analysis of spin relaxation
Contents
Chemical
scales
Measurement of Rex
Quadrupolar relaxation
Hyperfine interactions and paramagnetic shifts of nuclear spins
Paramagnetic relaxation of nuclear spins
Relaxation and the density matrix
Problems
References
12.
Magnetic field inhomogeneity,
measurement by NMR
Basic imaging concepts: phase and frequency encoding of
position in a macroscopic sample
Spatially selective pulses
Spatial equivalents of NMR parameters
Basic two-dimensional imaging sequences
fc-Space
Contrast and contrast agents, relaxation, and flow
Rapid-scan MRL echo-planar imaging and one-shot methods
Problems
References
Appendix A. Time-dependent perturbations
The time-dependent
states
Hilbert space, eigenvectors, and superposition of states
Perturbation theory: time-dependent perturbations of the
Hamiltonian
Semiclassical interactions between EMR and quantum oscillators
using perturbation theory
Appendix B. Density matrix formalism and the relaxation
supermatrix
A density matrix description of the H, ioN HMQC experiment
RF pulses
Time evolution of the density matrix with chemical shift and
coupling
Semiclassical relaxation theory and the Redfield relaxation matrix
Index
|
| adam_txt |
CONTENTS
Preface
Symbols and fundamental
1.
A semiclassical description of spectroscopy
Damped harmonics
Quantum oscillators
The spectroscopic experiment
Ensembles and coherence
Types of spectroscopy
Practical considerations in spectroscopy
Acquiring a spectrum
Resolution: the problem of line width
Line shape
Problems
2.
ensemble behavior and coupling
Nuclear and electronic spin
The quantum picture of nuclear spin
The "spinning top" model of nuclear spin
Spin-state populations in ensembles
Information available from NMR:
and chemical shift
Information available from NMR:
Information available from NMR:
Information available from NMR:
/-coupling time scale, decoupling experiments and exchange
decoupling
Interaction between nuclear spins and radio-frequency (RF)
E
Problems
viii Contents
3.
Interaction between nuclear spins and RF:
A single spin in the rotating frame of reference
Interaction between nuclear spins and RF:
An ensemble of spins in the rotating frame of reference
Detection of an NMR signal
Time-domain detection in the NMR experiment: the
free induction decay and quadrature detection
Digitization of the free induction decay
Fourier transformation: time-domain FID to frequency-domain
spectrum
Discrete Fourier transformation
Spectral phasing
RF pulses and pulse phase
Pulse power and off-resonance effects from RF pulses
Phase cycling: improved quadrature detection using CYCLOPS
Factors affecting spectral quality and appearance: shimming,
window functions and apodization
After the fact: window functions and zero filling
Linear prediction
Problems
References
4.
Longitudinal (Tt) relaxation and the sensitivity of the
NMR experiment
Transverse
Chemical shift and/-coupling evolution during the spin echo
Mechanisms of nuclear spin relaxation in liquids and the spectral
density function
Dipolar relaxation and the nuclear Overhauser effect
NOE
Heteronuclear
Other contributions to
spin-rotation and paramagnetic effects
Quadrapolar relaxation
Selective and nonselective Tl measurement and multi-exponential
decay of coherence
Problems
References
5.
in liquids
The classical approach: the Rloch equations of motion for
macroscopic magnetization
Classical description of a pulsed NMR experiment
A quantum mechanical description of NMR of a single spin in an
isotropie
Contents
A quantum mechanical description of NMR of coupled spins in an
isotropie
The time-dependent nuclear spin Hamiltonian operator and
solutions to the time-dependent
Problems
References
6.
NMR experiments in liquids
An ensemble of identical spins at equilibrium: an introduction to
the density matrix formalism
Expansion of the density matrix for an uncoupled spin in terms
of Cartesian angular momentum operators
Weakly coupled ensembles and the weak-coupling approximation
Single-element operators for a two-spin system
Interconversion
operator bases
Evolution of Cartesian operators under the influence of pulses,
chemical shift and /-coupling
Evolution of operators with weak/-coupling
Analysis of a simple NMR spectrum using product operators
Problems
References
7.
coherence selection
A simple two-dimensional NMR experiment
Coherence transfer in multidimensional NMR
The COSY experiment
Quadrature detection in multidimensional NMR
Axial peaks
Phase cycling and coherence order selection: the DQF-COSY
experiment
Other multiple-quantum filters in COSY
Multiple-quantum spectroscopy
Effect of n pulses on coherence
Pulsed-field gradients for coherence selection
The gradient COSY experiment
"Zero-quantum filtered COSY": NOESY and incoherent transfer
Rotating frame NOEs: CAMELSPIN and ROESY
Spin-locking experiments for coherence transfer: TOCSY and
composite pulse decoupling
Problems
References
8.
Heteronuclear polarization transfer and the INEPT experiment
Refocused INEPT
Contents
Two-dimensional polarization transfer: HETCOR
Sensitive nucleus (inverse) detection of an insensitive nucleus:
the double INEPT or HSQC experiment
Multiple-quantum approaches to heteronuclear correlation:
DEPT
Gradient coherence selection in heteronuclear correlation NMR
Phase-sensitive gradient coherence selection experiments for
heteronuclear correlations
Sensitivity enhancement in gradient coherence selection experiments
Problems
References
9.
considerations for biological applications of NMR
Polarization transfer
Solvent suppression
Frequency-labeling periods and constant time NMR experiments
Shaped and selective pulses
Composite pulse decoupling and spin-locking
Dealing with very large biomolecules in solution: deuteration and
direct 13C detection
Interference patterns in heteronuclear relaxation: TROSY
Problems
References
10.
and ordered fluids
Anisotropy in NMR: chemical shielding and dipolar coupling
Resolving the solid-state NMR spectrum: magic angle spinning
(MAS) and high-power XH decoupling
Cross-polarization for signal enhancement of dilute spins and
spin—spin correlations
Selective
rotational resonance, RFDR, and
Heteronuclear two-dimensional techniques in solid-state NMR
Solid-state NMR using oriented samples: PISEMA
Bringing a little order to solution NMR: residual dipolar couplings
and CSA in ordered fluids
Analysis of residual dipolar couplings
Problems
References
11.
Time scales of molecular motion, dynamic processes and relaxation
The spectral density revisited
Experimental measurement of heteronuclear relaxation parameters
in proteins
Model-free analysis of spin relaxation
Contents
Chemical
scales
Measurement of Rex
Quadrupolar relaxation
Hyperfine interactions and paramagnetic shifts of nuclear spins
Paramagnetic relaxation of nuclear spins
Relaxation and the density matrix
Problems
References
12.
Magnetic field inhomogeneity,
measurement by NMR
Basic imaging concepts: phase and frequency encoding of
position in a macroscopic sample
Spatially selective pulses
Spatial equivalents of NMR parameters
Basic two-dimensional imaging sequences
fc-Space
Contrast and contrast agents, relaxation, and flow
Rapid-scan MRL echo-planar imaging and one-shot methods
Problems
References
Appendix A. Time-dependent perturbations
The time-dependent
states
Hilbert space, eigenvectors, and superposition of states
Perturbation theory: time-dependent perturbations of the
Hamiltonian
Semiclassical interactions between EMR and quantum oscillators
using perturbation theory
Appendix B. Density matrix formalism and the relaxation
supermatrix
A density matrix description of the 'H, ioN HMQC experiment
RF pulses
Time evolution of the density matrix with chemical shift and
coupling
Semiclassical relaxation theory and the Redfield relaxation matrix
Index |
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| illustrated | Illustrated |
| index_date | 2024-07-02T13:47:58Z |
| indexdate | 2024-07-09T20:34:41Z |
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| language | English |
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| spelling | Pochapsky, Thomas C. Verfasser aut NMR for physical and biological scientists Thomas C. Pochapsky and Susan Sondej Pochapsky New York [u.a.] Taylor & Francis 2007 XXII, 372 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Magnetic Resonance Spectroscopy Nuclear magnetic resonance Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Biologie (DE-588)4006851-1 gnd rswk-swf Biologie (DE-588)4006851-1 s NMR-Spektroskopie (DE-588)4075421-2 s b DE-604 Pochapsky, Susan Sondej Verfasser aut Digitalisierung UB Regensburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014604965&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Pochapsky, Thomas C. Pochapsky, Susan Sondej NMR for physical and biological scientists Magnetic Resonance Spectroscopy Nuclear magnetic resonance Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd Biologie (DE-588)4006851-1 gnd |
| subject_GND | (DE-588)4075421-2 (DE-588)4006851-1 |
| title | NMR for physical and biological scientists |
| title_auth | NMR for physical and biological scientists |
| title_exact_search | NMR for physical and biological scientists |
| title_exact_search_txtP | NMR for physical and biological scientists |
| title_full | NMR for physical and biological scientists Thomas C. Pochapsky and Susan Sondej Pochapsky |
| title_fullStr | NMR for physical and biological scientists Thomas C. Pochapsky and Susan Sondej Pochapsky |
| title_full_unstemmed | NMR for physical and biological scientists Thomas C. Pochapsky and Susan Sondej Pochapsky |
| title_short | NMR for physical and biological scientists |
| title_sort | nmr for physical and biological scientists |
| topic | Magnetic Resonance Spectroscopy Nuclear magnetic resonance Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd Biologie (DE-588)4006851-1 gnd |
| topic_facet | Magnetic Resonance Spectroscopy Nuclear magnetic resonance Nuclear magnetic resonance spectroscopy NMR-Spektroskopie Biologie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=014604965&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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