Separation process principles:
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| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Hoboken, NJ
Wiley
2006
|
| Edition: | 2. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | XXXIV, 756 S. graph. Darst. |
| ISBN: | 0471464805 9780471464808 |
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MARC
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| 245 | 1 | 0 | |a Separation process principles |c J. D. Seader ; Ernest J. Henley |
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Record in the Search Index
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|---|---|
| adam_text | Contents
About the Authors v
Preface to the Second Edition vii
Nomenclature xxi
Dimensions and Units xxxi
PART 1 FUNDAMENTAL CONCEPTS 1
Chapter 1 Separation Processes 3
1.0 Instructional Objectives 3
1.1 Industrial Chemical Processes 4
1.2 Mechanism of Separation 6
1.3 Separation by Phase Addition or Creation 8
1.4 Separation by Barrier 14
1.5 Separation by Solid Agent 15
1.6 Separation by External Field or Gradient 16
1.7 Component Recoveries and Product Purities 17
1.8 Separation Power 19
1.9 Selection of Feasible Separation Processes 21
Summary 23 References 24 Exercises 24
Chapter 2 Thermodynamics of Separation Operations 27
2.0 Instructional Objectives 27
2.1 Energy, Entropy, and Availability Balances 27
2.2 Phase Equilibria 30
Fugacities and Activity Coefficients 31
/^ Values 32
2.3 Ideal Gas, Ideal Liquid Solution Model 34
2.4 Graphical Correlations of Thermodynamic Properties 37
2.5 Nonideal Thermodynamic Property Models 42
P v T Equation of State Models 42
Derived Thermodynamic Properties from P v T Models 44
2.6 Activity Coefficient Models for the Liquid Phase 47
Activity Coefficients from Gibbs Free Energy 48
Regular Solution Model 48
Nonideal Liquid Solutions 49
Margules Equations 52
van Laar Equation 52
Local Composition Concept and the Wilson Model 53
xi
xii Contents
NRTL Model 55
UNIQUAC Model 56
UNIFAC Model 57
Liquid Liquid Equilibria 58
2.7 Difficult Mixtures 58
Predictive Soave Redlich Kwong (PSRK) Model 59
Electrolyte Solution Models 59
Polymer Solution Models 59
2.8 Selecting an Appropriate Model 59
Summary 60 References 60 Exercises 61
Chapter 3 Mass Transfer and Diffusion 66
3.0 Instructional Objectives 67
3.1 Steady State, Ordinary Molecular Diffusion 67
Fick s Law of Diffusion 68
Velocities in Mass Transfer 68
Equimolar Counterdiffusion 69
Unimolecular Diffusion 70
3.2 Diffusion Coefficients 72
Diffusivity in Gas Mixtures 72
Diffusivity in Liquid Mixtures 74
Diffusivities of Electrolytes 77
Diffusivity of Biological Solutes in Liquids 78
Diffusivity in Solids 78
3.3 One Dimensional, Steady State and Unsteady State, Molecular Diffusion
Through Stationary Media 84
Steady State 84
Unsteady State 85
3.4 Molecular Diffusion in Laminar Flow 90
Falling Liquid Film 90
Boundary Layer Flow on a Flat Plate 93
Fully Developed Flow in a Straight, Circular Tube 95
3.5 Mass Transfer in Turbulent Flow 97
Reynolds Analogy 99
Chilton Colburn Analogy 99
Other Analogies 100
Theoretical Analogy of Churchill and Zajic 100
3.6 Models for Mass Transfer at a Fluid Fluid Interface 103
Film Theory 103
Penetration Theory 104
Surface Renewal Theory 105
Film Penetration Theory 106
3.7 Two Film Theory and Overall Mass Transfer Coefficients 107
Gas Liquid Case 107
Liquid Liquid Case 109
Case of Large Driving Forces for Mass Transfer 109
Summary 111 References 112 Exercises 113
Contents xiii
Chapter 4 Single Equilibrium Stages and Flash Calculations 117
4.0 Instructional Objectives 117
4.1 The Gibbs Phase Rule and Degrees of Freedom 117
Degrees of Freedom Analysis 118
4.2 Binary Vapor Liquid Systems 119
4.3 Azeotropic Systems 123
4.4 Multicomponent Flash, Bubble Point, and Dew Point Calculations 126
Isothermal Flash 126
Bubble and Dew Points 128
Adiabatic Flash 130
4.5 Ternary Liquid Liquid Systems 131
4.6 Multicomponent Liquid Liquid Systems 137
4.7 Solid Liquid Systems 138
Leaching 138
Crystallization 141
Liquid Adsorption 142
4.8 Gas Liquid Systems 144
4.9 Gas Solid Systems 146
Sublimation and Desublimation 146
Gas Adsorption 146
4.10 Multiphase Systems 147
Approximate Method for a Vapor Liquid Solid System 148
Approximate Method for a Vapor Liquid Liquid System 149
Rigorous Method for a Vapor Liquid Liquid System 150
Summary 151 References 152 Exercises 152
Chapter 5 Cascades and Hybrid Systems 161
5.0 Instructional Objectives 161
5.1 Cascade Configurations 161
5.2 Solid Liquid Cascades 163
5.3 Single Section, Liquid Liquid Extraction Cascades 165
Cocurrent Cascade 165
Crosscurrent Cascade 165
Countercurrent Cascade 166
5.4 Multicomponent Vapor Liquid Cascades 167
Single Section Cascades by Group Methods 167
Two Section Cascades 171
5.5 Membrane Cascades 175
5.6 Hybrid Systems 176
5.7 Degrees of Freedom and Specifications for Countercurrent Cascades 177
Stream Variables 178
Adiabatic or Nonadiabatic Equilibrium Stage 178
Single Section, Countercurrent Cascade 179
Two Section, Countercurrent Cascades 179
Summary 184 References 185 Exercises 185
xiv Contents
PART 2 SEPARATIONS BY PHASE ADDITION OR CREATION 191
Chapter 6 Absorption and Stripping of Dilute Mixtures 193
6.0 Instructional Objectives 193
Industrial Example 194
6.1 Equipment 196
6.2 General Design Considerations 200
6.3 Graphical Equilibrium Stage Method for Trayed Towers 201
Minimum Absorbent Flow Rate 202
Number of Equilibrium Stages 203
6.4 Algebraic Method for Determining the Number of Equilibrium Stages 205
6.5 Stage Efficiency 207
Performance Data 208
Empirical Correlations 208
Semitheoretical Models 212
Scale up from Laboratory Data 214
6.6 Tray Diameter, Pressure Drop, and Mass Transfer 215
Tray Diameter 215
High Capacity Trays 218
Tray Vapor Pressure Drop 219
Mass Transfer Coefficients and Transfer Units 220
Weeping, Entrainment, and Downcomer Backup 222
6.7 Rate Based Method for Packed Columns 223
6.8 Packed Column Efficiency, Capacity, and Pressure Drop 228
Liquid Holdup 228
Column Diameter and Pressure Drop 233
Mass Transfer Efficiency 237
6.9 Concentrated Solutions in Packed Columns 242
Summary 244 References 244 Exercises 246
Chapter 7 Distillation of Binary Mixtures 252
7.0 Instructional Objectives 252
Industrial Example 253
7.1 Equipment and Design Considerations 255
7.2 McCabe Thiele Graphical Equilibrium Stage Method for Trayed Towers 255
Rectifying Section 257
Stripping Section 259
Feed Stage Considerations 259
Determination of Number of Equilibrium Stages and Feed Stage Location 261
Limiting Conditions 261
Column Operating Pressure and Condenser Type 265
Subcooled Reflux 266
Reboiler Type 268
Condenser and Reboiler Duties 269
Feed Preheat 270
Contents xv
Optimal Reflux Ratio 270
Large Number of Stages 271
Use of Murphree Efficiency 272
Multiple Feeds, Side Streams, and Open Steam 273
7.3 Estimation of Stage Efficiency 275
Performance Data 275
Empirical Correlations 276
Semi Theoretical Models 278
Scale up from Laboratory Data 278
7.4 Diameter of Trayed Towers and Reflux Drums 279
Reflux Drums 279
7.5 Rate Based Method for Packed Columns 280
HETP Method 280
HTU Method 281
7.6 Ponchon Savarit Graphical Equilibrium Stage Method for Trayed Towers 283
Summary 284 References 285 Exercises 285
Chapter 8 Liquid Liquid Extraction with Ternary Systems 295
8.0 Instructional Objectives 295
Industrial Example 296
8.1 Equipment 298
Mixer Settlers 299
Spray Columns 299
Packed Columns 300
Plate Columns 300
Columns with Mechanically Assisted Agitation 300
8.2 General Design Considerations 305
8.3 Hunter Nash Graphical Equilibrium Stage Method 309
Number of Equilibrium Stages 310
Minimum and Maximum Solvent to Feed Flow Rate Ratios 313
Use of Right Triangle Diagrams 315
Use of an Auxiliary Distribution Curve with a McCabe Thiele Diagram 317
Extract and Raffinate Reflux 318
8.4 Maloney Schubert Graphical Equilibrium Stage Method 322
8.5 Theory and Scale Up of Extractor Performance 325
Mixer Settler Units 325
Multicompartment Columns 332
Axial Dispersion 334
Summary 337 References 338 Exercises 339
Chapter 9 Approximate Methods for Multicomponent,
Multistage Separations 344
9.0 Instructional Objectives 344
9.1 Fenske Underwood Gilliland Method 344
Selection of Two Key Components 345
Column Operating Pressure 347
xvi Contents
Fenske Equation for Minimum Equilibrium Stages 347
Distribution of Nonkey Components at Total Reflux 349
Underwood Equations for Minimum Reflux 349
Gilliland Correlation for Actual Reflux Ratio and Theoretical Stages 353
Feed Stage Location 355
Distribution of Nonkey Components at Actual Reflux 356
9.2 Kremser Group Method 356
Strippers 357
Liquid Liquid Extraction 358
Summary 360 References 360 Exercises 360
Chapter 10 Equilibrium Based Methods for Multicomponent Absorption,
Stripping, Distillation, and Extraction 364
10.0 Instructional Objectives 364
10.1 Theoretical Model for an Equilibrium Stage 365
10.2 General Strategy of Mathematical Solution 366
10.3 Equation Tearing Procedures 367
Tridiagonal Matrix Algorithm 367
Bubble Point (BP) Method for Distillation 369
Sum Rates Method for Absorption and Stripping 374
Isothermal Sum Rates Method for Liquid Liquid Extraction 378
10.4 Newton Raphson Method 380
10.5 Inside Out Method 388
MESH Equations 389
Rigorous and Complex Thermodynamic Property Models 390
Approximate Thermodynamic Property Models 390
Inside Out Algorithm 391
Summary 393 References 394 Exercises 394
Chapter 11 Enhanced Distillation and Supercritical Extraction 401
11.0 Instructional Objectives 402
11.1 Use of Triangular Graphs 402
Residue Curve Maps 405
Distillation Curve Maps 410
Product Composition Regions at Total Reflux (Bow Tie Regions) 411
11.2 Extractive Distillation 413
11.3 Salt Distillation 417
11.4 Pressure Swing Distillation 419
11.5 Homogeneous Azeotropic Distillation 421
11.6 Heterogeneous Azeotropic Distillation 425
Multiplicity of Solutions 429
11.7 Reactive Distillation 432
11.8 Supercritical Fluid Extraction 439
Summary 445 References 445 Exercises 447
Contents xvii
Chapter 12 Rate Based Models for Distillation 449
12.0 Instructional Objectives 451
12.1 Rate Based Model 451
12.2 Thermodynamic Properties and Transport Rate Expressions 454
12.3 Methods for Estimating Transport Coefficients and Interfacial Area 456
12.4 Vapor and Liquid Flow Patterns 457
12.5 Method of Calculation 457
ChemSep Program 457
RATEFRAC Program 461
Summary 462 References 463 Exercises 463
Chapter 13 Batch Distillation 466
13.0 Instructional Objectives 466
13.1 Differential Distillation 466
13.2 Binary Batch Rectification with Constant Reflux
and Variable Distillate Composition 469
13.3 Binary Batch Rectification with Constant Distillate Composition
and Variable Reflux 470
13.4 Batch Stripping and Complex Batch Distillation 471
13.5 Effect of Liquid Holdup 472
13.6 Shortcut Method for Multicomponent Batch Rectification
with Constant Reflux 472
13.7 Stage by Stage Methods for Multicomponent, Batch Rectification 474
Rigorous Model 474
Rigorous Integration Method 476
Rapid Solution Method 480
13.8 Optimal Control 482
Slop Cuts 482
Optimal Control by Variation of Reflux Ratio 484
Summary 486 References 487 Exercises 487
PART 3 SEPARATIONS BY BARRIERS AND SOLID AGENTS 491
Chapter 14 Membrane Separations 493
14.0 Instructional Objectives 493
Industrial Example 494
14.1 Membrane Materials 496
14.2 Membrane Modules 499
14.3 Transport in Membranes 502
Porous Membranes 502
Bulk Flow 503
Liquid Diffusion in Pores 504
Gas Diffusion 505
Nonporous Membranes 505
Solution Diffusion for Liquid Mixtures 506
xviii Contents
Solution Diffusion for Gas Mixtures 507
Module Flow Patterns 510
Cascades 512
External Mass Transfer Resistances 513
Concentration Polarization and Fouling 515
14.4 Dialysis and Electrodialysis 516
Electrodialysis 518
14.5 Reverse Osmosis 521
14.6 Gas Permeation 525
14.7 Pervaporation 527
14.8 Ultrafiltration 531
Process Configurations 532
14.9 Microfiltration 540
Constant Flux Operation 541
Constant Pressure Operation 542
Combined Operation 542
Summary 543 References 544 Exercises 545
Chapter 15 Adsorption, Ion Exchange, and Chromatography 548
15.0 Instructional Objectives 549
Industrial Example 550
15.1 Sorbents 551
Adsorbents 551
Ion Exchangers 555
Sorbents for Chromatography 557
15.2 Equilibrium Considerations 559
Pure Gas Adsorption 559
Liquid Adsorption 563
Ion Exchange Equilibria 565
Equilibria in Chromatography 568
15.3 Kinetic and Transport Considerations 568
External Transport 568
Internal Transport 571
Mass Transfer in Ion Exchange and Chromatography 572
15.4 Sorption Systems 573
Adsorption 573
Ion Exchange 576
Chromatography 577
Slurry Adsorption (Contact Filtration) 577
Fixed Bed Adsorption (Percolation) 580
Thermal Swing Adsorption 587
Pressure Swing Adsorption 590
Continuous, Countercurrent Adsorption Systems 596
Simulated Moving Bed Systems 598
Ion Exchange Cycle 607
Chromatographic Separations 608
Summary 612 References 613 Exercises 615
Contents xix
PART 4 SEPARATIONS THAT INVOLVE A SOLID PHASE 621
Chapter 16 Leaching and Washing 623
16.0 Instructional Objectives 623
Industrial Example 623
16.1 Equipment for Leaching 624
Batch Extractors 625
Espresso Machine 626
Continuous Extractors 627
Continuous, Countercurrent Washing 629
16.2 Equilibrium Stage Model for Leaching and Washing 631
McCabe Smith Algebraic Method 633
Variable Underflow 635
16.3 Rate Based Model for Leaching 637
Food Processing 637
Mineral Processing 639
Summary 641 References 641 Exercises 642
Chapter 17 Crystallization, Desublimation, and Evaporation 644
17.0 Instructional Objectives 644
Industrial Example 645
17.1 Crystal Geometry 648
Crystal Size Distributions 648
Differential Screen Analysis 651
Cumulative Screen Analysis 651
Surface Mean Diameter 652
Mass Mean Diameter 652
Arithmetic Mean Diameter 652
Volume Mean Diameter 653
17.2 Thermodynamic Considerations 653
Solubility and Material Balances 653
Enthalpy Balances 656
17.3 Kinetic and Transport Considerations 658
Supersaturation 658
Nucleation 659
Crystal Growth 660
17.4 Equipment for Solution Crystallization 663
Circulating, Batch Crystallizers 664
Continuous, Cooling Crystallizers 665
Continuous, Vacuum, Evaporating Crystallizers 665
17.5 The MSMPR Crystallization Model 666
Crystal Population Balance 667
17.6 Precipitation 671
17.7 Melt Crystallization 673
Equipment for Melt Crystallization 674
17.8 Zone Melting 677
xx Contents
17.9 Desublimation 679
Desublimation in a Heat Exchanger 680
17.10 Evaporation 681
Evaporator Model 683
Multiple Effect Evaporator Systems 685
Overall Heat Transfer Coefficients in Evaporators 688
Summary 688 References 689 Exercises 690
Chapter 18 Drying of Solids 695
18.0 Instructional Objectives 695
Industrial Example 696
18.1 Drying Equipment 696
Batch Operation 697
Continuous Operation 699
18.2 Psychrometry 711
Wet Bulb Temperature 713
Adiabatic Saturation Temperature 715
Moisture Evaporation Temperature 716
18.3 Equilibrium Moisture Content of Solids 719
18.4 Drying Periods 721
Constant Rate Drying Period 722
Falling Rate Drying Period 724
18.5 Dryer Models 734
Material and Energy Balances for Direct Heat Dryers 734
Belt Dryer with Through Circulation 735
Direct Heat Rotary Dryer 738
Fluidized Bed Dryer 739
Summary 742 References 742 Exercises 743
Index 748
|
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| id | DE-604.BV020822732 |
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| indexdate | 2024-07-09T20:14:06Z |
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| isbn | 0471464805 9780471464808 |
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| spelling | Seader, Junior D. Verfasser aut Separation process principles J. D. Seader ; Ernest J. Henley 2. ed. Hoboken, NJ Wiley 2006 XXXIV, 756 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Trennverfahren Separation (Technology) Textbooks Trennverfahren (DE-588)4078395-9 gnd rswk-swf Trennverfahren (DE-588)4078395-9 s DE-604 Henley, Ernest J. Verfasser aut http://www3.ub.tu-berlin.de/ihv/001714186.pdf Inhaltsverzeichnis HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013528069&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Seader, Junior D. Henley, Ernest J. Separation process principles Trennverfahren Separation (Technology) Textbooks Trennverfahren (DE-588)4078395-9 gnd |
| subject_GND | (DE-588)4078395-9 |
| title | Separation process principles |
| title_auth | Separation process principles |
| title_exact_search | Separation process principles |
| title_full | Separation process principles J. D. Seader ; Ernest J. Henley |
| title_fullStr | Separation process principles J. D. Seader ; Ernest J. Henley |
| title_full_unstemmed | Separation process principles J. D. Seader ; Ernest J. Henley |
| title_short | Separation process principles |
| title_sort | separation process principles |
| topic | Trennverfahren Separation (Technology) Textbooks Trennverfahren (DE-588)4078395-9 gnd |
| topic_facet | Trennverfahren Separation (Technology) Textbooks |
| url | http://www3.ub.tu-berlin.de/ihv/001714186.pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013528069&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT seaderjuniord separationprocessprinciples AT henleyernestj separationprocessprinciples |
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