The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Aachen
Shaker
2004
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| Series: | Berichte aus der Materialwissenschaft
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | 107 S. graph. Darst. 21 cm, 162 gr. |
| ISBN: | 3832230483 |
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Record in the Search Index
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| adam_text | THE EXPERIMENTAL AND THEORETICAL DETERMINATION OF THE THERMODYNAMIC
PROPERTIES OF MELTS AND GLASSES FROM THE SYSTEM CAO-MGO-AI 2 O 3 -SIO 2
VON DER FAKULTAT FUR GEORESSOURCEN UND MATERIALTECHNIK DER RHEINISCH
-WESTFALISCHEN TECHNISCHEN HOCHSCHULE AACHEN ZUR ERLANGUNG DES
AKADEMISCHEN GRADES EINES DOKTORS DER INGENIEURWISSENSCHAFTEN GENEHMIGTE
DISSERTATION VORGELEGT VON M.SC. JIN-WOOK SHIN AUS YECHON, KOREA
BERICHTER: UNIV.-PROF. DR.RER.NAT. REINHARD CONRADT UNIV.-PROF. JOCHEN
M. SCHNEIDER, PH. D. TAG DER MUNDLICHEN PRUFUNG: 29. JUNI 2004 CONTENTS
CONTENTS 1. INTRODUCTION 2. THEORY 2.1 THE GLASS TRANSITION AND THE
GLASSY STATE 2.1.1 THE GLASS TRANSITION 2.1.1.1 PHENOMENOLOGICAL ASPECTS
2.1.1.2 THERMODYNAMIC ASPECTS 2.2 EXPERIMENTAL METHODS IN
THERMOCHEMISTRY 2.2.1 ELECTROCHEMICAL METHODS 2.2.2 CALORIMETRIC METHODS
9 9 9 11 14 14 17 3. EXPERIMENTAL 22 3.1 PREPARATION OF GLASSY SAMPLES
22 3.1.1 SELECTION OF COMPOSITIONS 22 3.1.2 CALCULATION OF
CONSTITUTIONAL COMPOUNDS 26 3.1.3 SAMPLE PREPARATION 30 3.1.4
CHARACTERIZATION OF SAMPLES 30 3.2 DETERMINATION OF CAO ACTIVITIES IN
THE MELT 31 3.2.1 ASSEMBLY OF EQUIPMENT 33 3.2.2 DESCRIPTION AND
CHARACTERIZATION OF THE ELECTROLYTE 35 3.3 DETERMINATION OF AC P AND T G
BY DIFFERENTIAL SCANNING CALORIMETER 45 3.3.1 DESCRIPTION OF A DYNAMIC
CALORIMETER 45 3.3.2 CALIBRATION OF A DYNAMIC CALORIMETER 46 3.3.3
MEASUREMENT OF T G AND AC P 47 3.4 DETERMINATION OF IT AND AH MIXCA O
BY ISOTHERMAL DROP CALORIMETER 48 3.4.1 DESCRIPTION OF AN ISOTHERMAL
DROP CALORIMETER 48 3.4.2 CALIBRATION OF AN ISOTHERMAL DROP CALORIMETER
51 3.4.3 MEASUREMENT OF H VIT AND AH 54 4.1 4.2 THERMODYNAMIC MODELING
CONSTITUTIONAL MODEL MODIFIED QUASICHEMICAL MODEL 58 58 63 CONTENTS 5.
RESULTS AND DISCUSSION 68 5.1 RESULTS OF CALCULATION AND EMF MEASUREMENT
68 5.1.1 CALCULATION OF OXIDE ACTIVITIES IN THE MELTS 68 5.1.2
EXPERIMENTAL RESULTS 71 5.2 RESULTS OF CALCULATION AND CALORIMETRIC
MEASUREMENT 82 5.2.1 CALCULATION OF H VIT AND AH MIX CAO 82 5.2.2
EXPERIMENTAL RESULTS OF CALORIMETRIC MEASUREMENT 85 6. SUMMARY 92 7.
REFERENCES 95 8. APPENDICES 103 8.1 DATA FOR CONSTITUTIONAL COMPOUNDS
103 8.2 FORMATION ENTHALPY OF CONSTITUTIONAL COMPOUNDS 107
|
| any_adam_object | 1 |
| author | Shin, Jin-Wook 1970- |
| author_GND | (DE-588)129393762 |
| author_facet | Shin, Jin-Wook 1970- |
| author_role | aut |
| author_sort | Shin, Jin-Wook 1970- |
| author_variant | j w s jws |
| building | Verbundindex |
| bvnumber | BV019784860 |
| classification_tum | IND 200d |
| ctrlnum | (OCoLC)71746774 (DE-599)BVBBV019784860 |
| dewey-full | 620 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 620 - Engineering and allied operations |
| dewey-raw | 620 |
| dewey-search | 620 |
| dewey-sort | 3620 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Maschinenbau / Maschinenwesen Industrien, sonstige |
| format | Thesis Book |
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| indexdate | 2024-07-09T20:06:03Z |
| institution | BVB |
| isbn | 3832230483 |
| language | English |
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| physical | 107 S. graph. Darst. 21 cm, 162 gr. |
| publishDate | 2004 |
| publishDateSearch | 2004 |
| publishDateSort | 2004 |
| publisher | Shaker |
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| series2 | Berichte aus der Materialwissenschaft |
| spelling | Shin, Jin-Wook 1970- Verfasser (DE-588)129393762 aut The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 Jin-Wook Shin Aachen Shaker 2004 107 S. graph. Darst. 21 cm, 162 gr. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Materialwissenschaft Zugl.: Aachen, Techn. Hochsch., Diss., 2004 Calciumoxid (DE-588)4069810-5 gnd rswk-swf Zustandsgröße (DE-588)4068159-2 gnd rswk-swf Glasschmelze (DE-588)4122177-1 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Glasschmelze (DE-588)4122177-1 s Calciumoxid (DE-588)4069810-5 s Zustandsgröße (DE-588)4068159-2 s DE-604 HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013110727&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Shin, Jin-Wook 1970- The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 Calciumoxid (DE-588)4069810-5 gnd Zustandsgröße (DE-588)4068159-2 gnd Glasschmelze (DE-588)4122177-1 gnd |
| subject_GND | (DE-588)4069810-5 (DE-588)4068159-2 (DE-588)4122177-1 (DE-588)4113937-9 |
| title | The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 |
| title_auth | The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 |
| title_exact_search | The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 |
| title_full | The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 Jin-Wook Shin |
| title_fullStr | The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 Jin-Wook Shin |
| title_full_unstemmed | The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 Jin-Wook Shin |
| title_short | The experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system CaO-MgO-Al 2 O 3 -SiO 2 |
| title_sort | the experimental and theoretical determination of the thermodynamic properties of melts and glasses from the system cao mgo al 2 o 3 sio 2 |
| topic | Calciumoxid (DE-588)4069810-5 gnd Zustandsgröße (DE-588)4068159-2 gnd Glasschmelze (DE-588)4122177-1 gnd |
| topic_facet | Calciumoxid Zustandsgröße Glasschmelze Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013110727&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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