Isobutene dimerisation in a flow-through catalytic membrane reactor:
Saved in:
| Main Author: | |
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| Format: | Book |
| Language: | English |
| Published: |
2004
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Hamburg-Harburg, Techn. Univ., Diss., 2004 |
| Physical Description: | III, 172 S. Ill., graph. Darst. 30 cm |
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Record in the Search Index
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| adam_text | ISOBUTENE DIMERISATION IN A FLOW-THROUGH CATALYTIC MEMBRANE REACTOR VOM
PROMOTIONSAUSSCHUSS DER TECHNISCHEN UNIVERSITAT HAMBURG - HARBURG ZUR
ERLANGUNG DES AKADEMISCHES GRADES DOKTOR-INGENIEUR GENEHMIGTE
DISSERTATION VON IGOR RANDJELOVIC AUS BELGRAD 2004 TABLE OF CONTENTS
CHAPTER 1 INTRODUCTION CHAPTER 2 THEORETICAL 3 2.1 CATALYSIS 3 2.1.1
CATALYST 3 2.1.2 CATALYST PROPERTIES 5 2.1.3 PRINCIPLE OF HETEROGENEOUS
CATALYSIS 6 2.2 CATALYTIC MEMBRANE REACTORS 8 2.2.1 BASICS 8 2.2.2
CHARACTERISTICS OF THE MEMBRANES 8 2.2.3 THE MEMBRANE FUNCTIONS IN A
MEMBRANE REACTOR 10 2.2.4 CATALYTIC MEMBRANE DESIGN 13 CHAPTER 3 THIN
INORGANIC FILM DEPOSITION ON POLYMER SUBSTRATE 15 3.1 BACKGROUND 15 3.2
SOL-GEL PROCESSING 16 3.2.1 BACKGROUND 16 3.2.2 EXPERIMENTAL 19 3.2.3
RESULTS AND DISCUSSION 22 3.3 LIQUID PHASE DEPOSITION (LPD) 40 3.3.1
BACKGROUND 40 3.3.2 EXPERIMENTAL AND RESULTS 41 3.4 BIOMIMETIC
PROCESSING 41 3.4.1 BACKGROUND 41 3.4.2 EXPERIMENTAL 42 3.4.3 RESULTS
AND DISCUSSION 43 3.5 CONCLUSIONS 46 CHAPTER 4 EXPERIMENTAL APPARATUS
AND MEMBRANE REACTOR 47 4.1 BACKGROUND 47 4.2 EXPERIMENTAL 50 4.2.1
MATERIALS 50 4.2.2 CATALYST PREPARATION 50 4.2.3 MEMBRANE PREPARATION 51
4.2.4 APPARATUS AND PROCEDURE 52 4.3 RESULTS AND DISCUSSION 57 4.3.1
ISOBUTENE OLIGOMERISATION 57 4.3.2 MATERIAL SELECTION 58 4.3.3 MEMBRANE
CHARACTERISATION 64 4.3.3.1 MORPHOLOGY OF THE COMPOSITE CATALYTIC
MEMBRANES 64 4.3.3.2 POROUS CATALYST LAYER 76 4.3.3.2.1 BACKGROUND 76
4.3.3.2.2 POROSITY MEASUREMENT 79 4.3.3.2.3 CAPILLARY FLOW POROMETRY
TEST 81 4.3.3.3 CATALYST PARTICLE DISTRIBUTION AND SIZE MEASUREMENT 85
4.3.3.4 MASS TRANSPORT THROUGH DENSE MEMBRANES 88 4.3.3.4.1 BACKGROUND
88 4.3.3.4.2 GAS AND VAPOR PERMEABILITY MEASUREMENT 91 4.3.3.4.3 LIQUID
MIXTURE PERMEABILITY MEASUREMENT 95 4.3.3.5 ACIDITY MEASUREMENTS 99
4.3.3.5.1 BACKGROUND 99 4.3.3.5.2 EXPERIMENTAL 99 4.3.3.5.3 RESULTS AND
DISCUSSION 101 4.3.4 PERFORMANCE OF ISOBUTENE DIMERISATION IN THE
FLOW-THROUGH MEMBRANE REACTOR 106 4.3.4.1 INFLUENCE OF THE CONVERSION ON
THE FEED PRESSURE 107 4.3.4.2 CATALYST PERFORMANCE 109 4.3.4.2.1 EFFECT
OF TEMPERATURE 109 II 4.3.4.2.2 EFFECT OF SPACE VELOCITY 113 4.3.4.3
EFFECT OF BINDER 120 4.3.4.3.1 EFFECT OF TEMPERATURE TO VARIOUS BINDERS
120 4.3.4.3.2 EFFECT OF SPACE VELOCITY TO VARIOUS BINDERS 123 4.3.4.4
EFFECT OF INTERMEDIATE THIN FILM 127 4.3.4.5 EFFECT OF PARTICLE SIZE 132
4.3.4.6 EFFECT OF INERT GAS 133 A3 A.I CATALYST DEACTIVATION 134 4.3.4.8
EFFECT OF MATERIAL 136 CHAPTER 5 DESIGN OF FLOW-THROUGH CATALYTIC
MEMBRANE REACTOR 138 5.1 INTRODUCTION 138 5.2 REACTION SCHEME AND
KINETICS 138 5.3 KINETIC EXPERIMENT 144 5.3.1 EXPERIMENTAL 144 5.3.2
RESULTS AND DISCUSSION 145 5.4 DEVELOPMENT OF A MODEL FOR THE MEMBRANE
REACTOR 147 5.4.1 THE MATERIAL BALANCE 147 5.4.2 THE ENERGY BALANCE 151
5.4.3 PRESSURE DROP 152 5.4.4 BOUNDARY CONDITIONS 153 CHAPTER 6
CONCLUSIONS AND OUTLOOK 155 CHAPTER 7 LITERATURE CITED 158 NOTATION 169
III
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| any_adam_object | 1 |
| author | Randjelovic, Igor |
| author_facet | Randjelovic, Igor |
| author_role | aut |
| author_sort | Randjelovic, Igor |
| author_variant | i r ir |
| building | Verbundindex |
| bvnumber | BV019681677 |
| ctrlnum | (OCoLC)249870606 (DE-599)BVBBV019681677 |
| discipline | Chemie / Pharmazie |
| format | Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV019681677 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T20:03:41Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-013009645 |
| oclc_num | 249870606 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM DE-29T DE-706 DE-83 |
| owner_facet | DE-91 DE-BY-TUM DE-29T DE-706 DE-83 |
| physical | III, 172 S. Ill., graph. Darst. 30 cm |
| publishDate | 2004 |
| publishDateSearch | 2004 |
| publishDateSort | 2004 |
| record_format | marc |
| spelling | Randjelovic, Igor Verfasser aut Isobutene dimerisation in a flow-through catalytic membrane reactor von Igor Randjelovic 2004 III, 172 S. Ill., graph. Darst. 30 cm txt rdacontent n rdamedia nc rdacarrier Hamburg-Harburg, Techn. Univ., Diss., 2004 Heterogene Katalyse (DE-588)4123377-3 gnd rswk-swf Dimerisierung (DE-588)4251822-2 gnd rswk-swf Kompositmembran (DE-588)4302635-7 gnd rswk-swf Isobuten (DE-588)4162474-9 gnd rswk-swf Durchflussreaktor (DE-588)4284881-7 gnd rswk-swf Membranreaktor (DE-588)4555095-5 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Isobuten (DE-588)4162474-9 s Dimerisierung (DE-588)4251822-2 s Heterogene Katalyse (DE-588)4123377-3 s Durchflussreaktor (DE-588)4284881-7 s Membranreaktor (DE-588)4555095-5 s Kompositmembran (DE-588)4302635-7 s DE-604 HEBIS Datenaustausch Darmstadt application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013009645&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Randjelovic, Igor Isobutene dimerisation in a flow-through catalytic membrane reactor Heterogene Katalyse (DE-588)4123377-3 gnd Dimerisierung (DE-588)4251822-2 gnd Kompositmembran (DE-588)4302635-7 gnd Isobuten (DE-588)4162474-9 gnd Durchflussreaktor (DE-588)4284881-7 gnd Membranreaktor (DE-588)4555095-5 gnd |
| subject_GND | (DE-588)4123377-3 (DE-588)4251822-2 (DE-588)4302635-7 (DE-588)4162474-9 (DE-588)4284881-7 (DE-588)4555095-5 (DE-588)4113937-9 |
| title | Isobutene dimerisation in a flow-through catalytic membrane reactor |
| title_auth | Isobutene dimerisation in a flow-through catalytic membrane reactor |
| title_exact_search | Isobutene dimerisation in a flow-through catalytic membrane reactor |
| title_full | Isobutene dimerisation in a flow-through catalytic membrane reactor von Igor Randjelovic |
| title_fullStr | Isobutene dimerisation in a flow-through catalytic membrane reactor von Igor Randjelovic |
| title_full_unstemmed | Isobutene dimerisation in a flow-through catalytic membrane reactor von Igor Randjelovic |
| title_short | Isobutene dimerisation in a flow-through catalytic membrane reactor |
| title_sort | isobutene dimerisation in a flow through catalytic membrane reactor |
| topic | Heterogene Katalyse (DE-588)4123377-3 gnd Dimerisierung (DE-588)4251822-2 gnd Kompositmembran (DE-588)4302635-7 gnd Isobuten (DE-588)4162474-9 gnd Durchflussreaktor (DE-588)4284881-7 gnd Membranreaktor (DE-588)4555095-5 gnd |
| topic_facet | Heterogene Katalyse Dimerisierung Kompositmembran Isobuten Durchflussreaktor Membranreaktor Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=013009645&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT randjelovicigor isobutenedimerisationinaflowthroughcatalyticmembranereactor |